The aim of studying and bibliography

The main aim of study: To provide a student a knowledge on electrochemical technology, production of various chemical compounds by electrochemical means and application of electrochemical techniques in industrial processes.

The general information about the module: The module is realized in the 6-th semester for Chemical Technology students.

Teaching materials: Instrukcje do ćwiczeń laboratoryjnych

Bibliography required to complete the module

Bibliography used during lectures

1	Aleksander Ciszewski	Technologia chemiczna. Procesy elektrochemiczne	Wyd. Politechniki Poznańskiej, Poznań .	2008
2	Andrzej Czerwiński	Akumulatory, baterie, ogniwa.	WKŁ, Warszawa .	2012

Bibliography to self-study

1	K. Schmidt – Szałowski, J. Sentek, J. Raabe, E. Bobryk	Podstawy technologii chemicznej – procesy w przemyśle nieorganicznym	Oficyna Wydawnicza Politechniki Warszawskiej, Warszawa.	2004
2	R. Dylewski, W. Gnot, M. Gonet	Elektrochemia przemysłowa – Wybrane procesy i zagadnienia	Wydawnictwo Politechniki Śląskiej, Gliwice .	2002

Basic requirements in category knowledge/skills/social competences

Formal requirements: Active 1-st degree course student status.

Basic requirements in category knowledge: The student should have knowledge on physical chemistry within the scope of electrochemistry and basic knowledge on chemical technology

Basic requirements in category skills: The student should be ready to work in a team environment.

Basic requirements in category social competences: is responsible, displays maturity indispensable for a job in chemistry

Module outcomes

MEK	The student who completed the module	Types of classes / teaching methods leading to achieving a given outcome of teaching	Methods of verifying every mentioned outcome of teaching	Relationships with KEK	Relationships with PRK
01	has a knowledge in the area of electrochemistry of chemical compounds	lecture	written tests, laboratory reports	K_W08+++ K_U21+	P6S_UW P6S_WG
02	has a knowledge on industrial electrochemical technologies	lecture	written tests, laboratory reports	K_W08+++ K_W13+++ K_U17+++	P6S_UW P6S_WG
03	can plan and perform a simple laboratory experiment in the area of electrochemical technology and can properly interpret the results and write a report.	laboratory	performance observation, laboratory report	K_W08+ K_W13+ K_U10+++ K_U17+	P6S_UW P6S_WG
04	can work in a team performing experiments, calculations and can interpret the results	laboratory	performance observation, laboratory report	K_U10++ K_K03+++	P6S_KR P6S_UW

Attention: Depending on the epidemic situation, verification of the achieved learning outcomes specified in the study program, in particular credits and examinations at the end of specific classes, can be implemented remotely (real-time meetings).

The syllabus of the module

Sem.	TK	The content	realized in	MEK
6	TK01	Electrolysis process - general definitions. Area of electro-chemical engineering. Industrial electrochemical processes of inorganic compounds. Chloralkali industry processes. Electrolytic production of aluminium and magnesium. Hydrometallurgical processes. Electrochemical production of zinc. Electrolytic refining of copper. Industrial electrochemical processes of organic compounds. Electrohydro - dimerization of acetonitrile. Electrolytic production of sebacic acid. Electrochemical production of aromatic aldehydes. Application of electrochemical methods in waste recycling. Principles of electroplating processer. Batteries and fuel – cells.	W01-W15	MEK01 MEK02
6	TK02	Electroreffining of copper. Galvanic cells. Characteystic of charging and discharging of the cell. Electrolytic manganese dioxide. Electrochemical oxidation of aniline.	L01-L15	MEK03 MEK04

The student's effort

The type of classes	The work before classes	The participation in classes	The work after classes
Lecture (sem. 6)	The preparation for a test: 10.00 hours/sem.	contact hours: 15.00 hours/sem.	complementing/reading through notes: 1.00 hours/sem. Studying the recommended bibliography: 2.00 hours/sem.
Laboratory (sem. 6)	The preparation for a Laboratory: 8.00 hours/sem.	contact hours: 15.00 hours/sem.	Finishing/Making the report: 9.00 hours/sem.
Advice (sem. 6)
Credit (sem. 6)

The way of giving the component module grades and the final grade

The type of classes	The way of giving the final grade
Lecture	A written test including the content of the lectures. An examination mark depends on the score gained: 3.0 (50.0%-60.0%) MP ; 3.5 (60.1%-70.0%) MP; 4.0 (70.1%-80.0%) MP; 4,5 (80.1%-90.0%) MP; 5.0 (90.1%-100%) MP. MP denotes the full score.
Laboratory	The necessary condition for receiving a credit for laboratory is obtaining at least a pass mark in every exercise included in the schedule. The mark in a single unit corresponds to the mark obtained for a written/oral test. The necessary condition to pass the unit is also correct performance of the laboratory work and correct/individual preparation of a report. The mark in laboratory is an arithmetic mean of the marks obtained for every exercise included in the schedule. The final mark in laboratory is rounded according to WKZJK.
The final grade	A final mark (K): K= 0.5 w L + 0.5 w E; where: L, W denote respectively a positive mark in the laboratory and the lecture. w – a coefficient for a resit, w = 1.0 for a regular term, w = 0.9 for a first resit, w = 0.8 for a second resit. A final mark is rounded according to WKZJK.

Sample problems

Required during the exam/when receiving the credit
(-)

Realized during classes/laboratories/projects
(-)

Others
(-)

Can a student use any teaching aids during the exam/when receiving the credit : no

The contents of the module are associated with the research profile: yes

1	P. Chmielarz; T. Pacześniak; K. Rydel-Ciszek; A. Sobkowiak	Bio-Inspired Iron Pentadentate Complexes as Dioxygen Activators in the Oxidation of Cyclohexene and Limonene	2023
2	P. Błoniarz; D. Maksym; J. Muzart; T. Pacześniak; A. Pokutsa; A. Zaborovskyi	Cyclohexane oxidation: relationships of the process efficiency with electrical conductance, electronic and cyclic voltammetry spectra of the reaction mixture	2021
3	P. Chmielarz; A. Miłaczewska; T. Pacześniak; K. Rydel-Ciszek; A. Sobkowiak	‘Oxygen-Consuming Complexes’–Catalytic Effects of Iron–Salen Complexes with Dioxygen	2021
4	W. Frącz; T. Pacześniak; I. Zarzyka	Rigid polyurethane foams modified with borate and oxamide groups-Preparation and properties	2021
5	P. Błoniarz; J. Muzart; T. Pacześniak; A. Pokutsa; S. Tkach; A. Zaborovskyi	Sustainable oxidation of cyclohexane and toluene in the presence of affordable catalysts: Impact of the tandem of promoter/oxidant on process efficiency	2020
6	P. Błoniarz; O. Fliunt; Y. Kubaj; T. Pacześniak; A. Pokutsa; A. Zaborovskyi	Sustainable oxidation of cyclohexane catayzed by a VO(acac)2 - oxalic acid tandem: the electrochemical motive of the process efficiency	2020
7	P. Błoniarz; P. Chmielarz; T. Pacześniak; K. Rydel-Ciszek; A. Sobkowiak; K. Surmacz; I. Zaborniak	Iron-Based Catalytically Active Complexes in Preparation of Functional Materials	2020
8	P. Błoniarz; Y. Kubaj; D. Maksym; J. Muzart; T. Pacześniak; A. Pokutsa; A. Zaborovskyi	Versatile and Affordable Approach for Tracking the Oxidative Stress Caused by the Free Radicals: the Chemical Perception	2020