The aim of studying and bibliography

The main aim of study: Students become conversant with solid-fluid mass transfer processes

The general information about the module: The module is implemented in the sixth semester. It includes 30 hours of lectures, 30 hours of classes and 15 hours laboratory. It ends with an exam.

Bibliography required to complete the module

Bibliography used during lectures

1	R. Petrus, G. Aksielrud, J. Gumnicki, W. Piątkowski	Wymiana masy ciało stałe – ciecz	OW PRz.	1998
2	R. Koch, A. Kozioł	Dyfuzyjno-cieplny rozdział substancji	WNT.	1994

Bibliography used during classes/laboratories/others

1	K. Pawłow, P. Romankow, A.Noskow	Przykłady i zadania z zakresu aparatury i inżynierii chemicznej	WNT.	1981
2	Praca zbiorowa pod red. R. Zarzycki	Zadania rachunkowe z inżynierii chemicznej	PWN.	1980

Basic requirements in category knowledge/skills/social competences

Formal requirements: Registration for the corresponding semester

Basic requirements in category knowledge: student has basic knowledge in mathematics (calculus) and understands the principles of balancing processes

Basic requirements in category skills: Student can derive simple mass or heat balance

Basic requirements in category social competences: no requirements

Module outcomes

MEK	The student who completed the module	Types of classes / teaching methods leading to achieving a given outcome of teaching	Methods of verifying every mentioned outcome of teaching	Relationships with KEK	Relationships with PRK
01	knows mechanisms of mass transfer in the liquid-solid systems	lecture	written exam
02	has knowledge on drying, crystallization and dissolution proceses	lecture	written exam
03	has knowledge of the apparatus used for drying, crystallization and dissolution of solids	lecture	written exam	K_W13++	P6S_WG
04	can propose the balance of a typical process and calculate some parameters	lecture, classes, laboratory	written test, written report	K_U09+ K_U12+++	P6S_UW
05	is able to supervise the simple experiment in the laboratory scale for mass exchange process, to prepare a report	laboratory	observation of performance, written report	K_U09+ K_K01+	P6S_KK P6S_KO P6S_KR P6S_UW
06	is able to work in a team	laboratory	observation of performance	K_K03++	P6S_KR

Attention: Depending on the epidemic situation, verification of the achieved learning outcomes specified in the study program, in particular credits and examinations at the end of specific classes, can be implemented remotely (real-time meetings).

The syllabus of the module

Sem.	TK	The content	realized in	MEK
6	TK01	Mechanisms of mass transfer. Diffusion equation and its application. The mass balance in the system liquid-solid	W01-W06,C01-C07	MEK01
6	TK02	Special cases of mass transfer - simplification of balance equations	W07-W09,C08-C09	MEK01 MEK02
6	TK03	Objectives and methods of drying. Basic concepts. The first and second drying period. Non-continuous and continuous drying. Mass and energy balance . Dryers	W10-W21,C10-C21,L01-L06	MEK02 MEK03 MEK04 MEK05 MEK06
6	TK04	Objectives and methods of the dissolution process. Basic concepts. The kinetics of dissolution. Different methods of dissolution.	W22-W25,C22-C25	MEK02 MEK03 MEK04
6	TK05	Objectives and methods of crystallization. Basic concepts. Growth of crystals. Phase equilibrium . Mass and heat balance. Special methods of crystallization.	W26-W30,C26-C30,L07-10	MEK02 MEK03 MEK04 MEK05 MEK06
6	TK06	Industrial apparatus and techniques of mass-exchange processes for solid-liquid systems	L11-L15	MEK05 MEK06

The student's effort

The type of classes	The work before classes	The participation in classes	The work after classes
Lecture (sem. 6)		contact hours: 18.00 hours/sem.	Studying the recommended bibliography: 20.00 hours/sem.
Class (sem. 6)	The preparation for a Class: 20.00 hours/sem. The preparation for a test: 20.00 hours/sem.	contact hours: 18.00 hours/sem.	Finishing/Studying tasks: 20.00 hours/sem.
Laboratory (sem. 6)	The preparation for a test: 20.00 hours/sem.	contact hours: 9.00 hours/sem.	Finishing/Making the report: 20.00 hours/sem.
Advice (sem. 6)	The preparation for Advice: 2.00 hours/sem.	The participation in Advice: 2.00 hours/sem.
Exam (sem. 6)	The preparation for an Exam: 30.00 hours/sem.	The written exam: 2.00 hours/sem.

The way of giving the component module grades and the final grade

The type of classes	The way of giving the final grade
Lecture	written exam 47,0-60,0% =3,0 60,1-70,0% = 3,5 70,1-80,0% = 4,0 81,1-90,0% = 4,5 90,1-100% = 5,0
Class	two written tests 47,0-60,0% =3,0 60,1-70,0% = 3,5 70,1-80,0% = 4,0 81,1-90,0% = 4,5 90,1-100% = 5,0
Laboratory	passing all labs reports, written test 47,0-60,0% =3,0 60,1-70,0% = 3,5 70,1-80,0% = 4,0 81,1-90,0% = 4,5 90,1-100% = 5,0
The final grade	final mark (K): K=0,5 w C + 0,1 w L + 0,4 w W; W - mark for lecture L - mark for lab C - mark for classes w - weighting factor: w = 1,0 first term, w = 0,9 second term, w = 0,8 third term.

Sample problems

Required during the exam/when receiving the credit
(-)

Realized during classes/laboratories/projects
(-)

Others
(-)

Can a student use any teaching aids during the exam/when receiving the credit : no

The contents of the module are associated with the research profile: yes

1	E. Chmiel-Szukiewicz; A. Szałek; M. Szukiewicz	Graph Theory in Chemical Kinetics Practice Problems	2024
2	E. Chmiel-Szukiewicz; M. Szukiewicz	Generalized Linear Driving Force Formulas for Diffusion and Reaction in Porous Catalysts	2024
3	E. Chmiel-Szukiewicz; M. Szukiewicz; L. Zaręba	Application of the kinetic polynomial idea to describecatalytic hydrogenation of propene	2024
4	K. Kaczmarski; M. Szukiewicz	Analytical and numerical solutions of linear and nonlinear chromatography column models	2024
5	A. Szałek; M. Szukiewicz	Application of transfer function for quick estimation of gas flow parameters—A useful model‐based approach to enhancing measurements	2021
6	E. Chmiel-Szukiewicz; A. Szałek; M. Szukiewicz	Kinetic investigations of heterogeneous reactor processes – Optimization of experiments	2021
7	K. Kaczmarski; M. Szukiewicz	An efficient and robust method for numerical analysis of a dead zone in catalyst particle and packed bed reactor	2021
8	K. Kaczmarski; M. Szukiewicz	Modeling of a Real-Life Industrial Reactor for Hydrogenation of Benzene Process	2021
9	M. Szukiewicz	Differential quadrature method for some diffusion-reaction problems	2020
10	M. Szukiewicz	Study of reaction - diffusion problem: modeling, exact analytical solution, and experimental verification	2020
11	E. Chmiel-Szukiewicz; K. Kaczmarski; A. Szałek; M. Szukiewicz	Dead zone for hydrogenation of propylene reaction carried out on commercial catalyst pellets	2019
12	M. Chutkowski; G. Król; M. Szukiewicz	Formation of dead zone in catalytic particles in catalysis and biocatalysis - New alternative method of determination	2019
13	M. Szukiewicz; M. Wójcik	A simple method of determination of the degree of gas mixing by numerical Laplace inversion and Maple	2019