Cycle of education: 2022/2023
The name of the faculty organization unit: The faculty Chemistry
The name of the field of study: Chemical Technology
The area of study: technical sciences
The profile of studing:
The level of study: first degree study
Type of study: past time
discipline specialities : Chemical analysis in industry and environment, Chemical and bioprocess engineering, Organic and polymer technology
The degree after graduating from university: Bachelor of Science (BSc)
The name of the module department : Department of Technology and Materials Chemistry
The code of the module: 5317
The module status: mandatory for the speciality Chemical analysis in industry and environment
The position in the studies teaching programme: sem: 7 / W9 L18 / 4 ECTS / Z
The language of the lecture: Polish
The name of the coordinator: Dorota Naróg, PhD, Eng.
The main aim of study: Provide knowledge on the modern chromatographic methods, hyphenated techniques, including sample preparation methods used in environmental, pharmaceutical laboratories and food analysis.
The general information about the module: The module is implemented in 7 semester and includes 15 hours of lectures and 30 hours of lab. The module ends with a pass.
Teaching materials: instrukcje do ćwiczeń laboratoryjnych
1 | Z. Witkiewicz | Podstawy chromatografii, wyd.2-gie | WNT, Warszawa. | 1995 |
2 | J. Namieśnik, J. Łukasiak, Z. Jamrógiewicz | Pobieranie próbek środowiskowych do analizy | PWN, Warszawa. | 1995 |
3 | K. Robards, P. Jackson, P. Haddad | Principles and Practice of Modern Chromatographic Methods, 1st Edition | Academic Press, London. | 1994 |
4 | W. Rödel, G. Wölm | Chromatografia gazowa | WN PWN, Warszawa . | 1992 |
5 | R. Rosset, H. Kołodziejczyk | Współczesna chromatografia cieczowa | PWN, Warszawa. | 2000 |
1 | Z. Witkiewicz | Nowe kierunki w chromatografii | WNT, Warszawa . | 1988 |
2 | L. R. Snyder, J. J Kirkland, J. L. Gleic | Practical HPLC method development, sec. ed. | J. Wiley, New York. | 1997 |
3 | R.J. Hamilton, P.A. Sewell | Wysokosprawna chromatografia cieczowa | PWN, Warszawa . | 1982 |
Formal requirements: required course credits: instrumental analysis, analytical chemistry, physical chemistry, mathematics, pyisics
Basic requirements in category knowledge: Required basic knowledge of instrumental methods of analysis, physics and mathematics
Basic requirements in category skills: required basic laboratory skills and practical experience in the use of basic equipment and instrumentation
Basic requirements in category social competences: organizational skills, manipulative and observational skills, being able to work in teams
MEK | The student who completed the module | Types of classes / teaching methods leading to achieving a given outcome of teaching | Methods of verifying every mentioned outcome of teaching | Relationships with KEK | Relationships with PRK |
---|---|---|---|---|---|
01 | Has knowledge of the chromatographic techniques applied in environmental, food and material analysis. Mastered the separation mechanisms, column chemistry and can apply optimization procedures. Learned the modern techniques for the preparation of samples for chromatographic analysis. | lecture, laboratory exercise | written test and report for every laboratory exercise, observation of performance, pass a final written test |
K_W04+++ |
P6S_WG |
02 | Acquired knowledge of the modern chromatographic techniques such as two-dimensional chromatography, multicapilary gas chromatography, ultra-fast performance liquid chromatography and chromatographic hyphenated methods. | lecture, laboratory exercise | written test and report for every laboratory exercise, observation of performance, pass a final written test |
K_W13+++ |
P6S_WG |
03 | He can design and use approprate chromatographic analysis method for the specific analyte or group of analytes and a sample type. | laboratory exercise | written test and report for every laboratory exercise, observation of performance, |
K_U11+ |
P6S_UO P6S_UW |
04 | He uses quantitative methods of analysis, including callibration techniques. Acquired the practical knowledge and skills to interpret and evaluate the quality and reliability of the results of analysis. | laboratory exercises | pass a written test, observation of performance |
K_U21+ K_K01+ |
P6S_KK P6S_KO P6S_KR P6S_UW |
05 | He has the ability to work independly and in the team during the planning of the analytical procedure and analytical problem solving. | laboratory exercises | observation of performance |
K_K03+ |
P6S_KR |
Attention: Depending on the epidemic situation, verification of the achieved learning outcomes specified in the study program, in particular credits and examinations at the end of specific classes, can be implemented remotely (real-time meetings).
Sem. | TK | The content | realized in | MEK |
---|---|---|---|---|
7 | TK01 | W01-W7 | MEK01 MEK05 | |
7 | TK02 | W08-W12 | MEK02 MEK03 | |
7 | TK03 | W13-W15 | MEK03 MEK04 | |
7 | TK04 | L01-L30 | MEK03 MEK05 |
The type of classes | The work before classes | The participation in classes | The work after classes |
---|---|---|---|
Lecture (sem. 7) | contact hours:
9.00 hours/sem. |
Studying the recommended bibliography:
15.00 hours/sem. |
|
Laboratory (sem. 7) | The preparation for a Laboratory:
5.00 hours/sem. The preparation for a test: 15.00 hours/sem. |
contact hours:
18.00 hours/sem. |
Finishing/Making the report:
10.00 hours/sem. |
Advice (sem. 7) | The participation in Advice:
2.00 hours/sem. |
||
Credit (sem. 7) | The preparation for a Credit:
25.00 hours/sem. |
The written credit:
2.00 hours/sem. |
The type of classes | The way of giving the final grade |
---|---|
Lecture | |
Laboratory | |
The final grade |
Required during the exam/when receiving the credit
(-)
Realized during classes/laboratories/projects
(-)
Others
(-)
Can a student use any teaching aids during the exam/when receiving the credit : no
1 | D. Naróg; A. Sobkowiak | Electrochemistry of Flavonoids | 2023 |
2 | D. Naróg; A. Sobkowiak | Electrochemical Investigation of some Flavonoids in Aprotic Media | 2022 |
3 | D. Naróg | Electrochemical study of quercetin in the presence of galactopyranose: Potential application to the electrosynthesis of glycoconjugates of quinone/quinone methide of quercetin | 2020 |