Cycle of education: 2022/2023
The name of the faculty organization unit: The faculty Chemistry
The name of the field of study: Chemical Technology
The area of study: technical sciences
The profile of studing:
The level of study: first degree study
Type of study: past time
discipline specialities : Chemical analysis in industry and environment, Chemical and bioprocess engineering, Organic and polymer technology
The degree after graduating from university: Bachelor of Science (BSc)
The name of the module department : Department of Physical Chemistry
The code of the module: 5273
The module status: mandatory for teaching programme Chemical analysis in industry and environment, Chemical and bioprocess engineering, Organic and polymer technology
The position in the studies teaching programme: sem: 5 / W18 L27 / 6 ECTS / Z
The language of the lecture: Polish
The name of the coordinator 1: Julian Kozioł, PhD, Eng.
The name of the coordinator 2: Prof. Andrzej Sobkowiak, DSc, PhD, Eng.
The main aim of study: Acquisition of a theoretical knowledge and experience on practical applications of modern instrumental analysis techniques used for chemical analysis of organic and inorganic compounds.
The general information about the module: The module is realised in the 5-th semester and include 30 hours of lectures and 45 hours of laboratory practice. Module ends with a graded assignment.
others: Instrukcje do ćwiczeń laboratoryjnych
1 | K. Danzer i inn. | Analityka – przegląd systematyczny | WNT, Warszawa . | 1993 |
2 | A. Cygański | Metody spektroskopowe w chemii analitycznej | WNT, Warszawa. | 1997 |
3 | E. Hoffmann, J. Charette, V. Stroobant | Spektrometria mas | WNT, Warszawa. | 1998 |
4 | A. Cygański | Metody elektroanalityczne | WNT, Warszawa. | 1995 |
5 | Z. Witkiewicz | Podstawy chromatografii | WNT, Warszawa. | 2005 |
1 | W. Szczepaniak | Metody instrumentalne w analizie chemicznej | PWN, Warszawa. | 2004 |
2 | R.M. Silverstein i inn. | Spektroskopowe metody identyfikacji związków organicznych | PWN, Warszawa. | 2007 |
1 | W. Szczepaniak | Metody instrumentalne w analizie chemicznej | PWN, Warszawa. | 2004 |
Formal requirements: Registration for V semester
Basic requirements in category knowledge: Knowledge and understanding of the basic physics, general, analytical, organic and physical chemistry.
Basic requirements in category skills: Skills in calculation of chemical concentration, solutions preparation, operation of basic laboratory equipment for chemical analysis, measurement as well as computer. A basic knowledge of mathematics
Basic requirements in category social competences: Knowledge of principles of safe work in chemical laboratory, responsibility during experiments performed individually or in laboratory group.
MEK | The student who completed the module | Types of classes / teaching methods leading to achieving a given outcome of teaching | Methods of verifying every mentioned outcome of teaching | Relationships with KEK | Relationships with PRK |
---|---|---|---|---|---|
01 | Has a theoretical and practical knowledge of construction and mechanizm of action of modern analytical equipment. | lecture, laboratory | written test, performance observation |
K_W04++ |
P6S_WG |
02 | Has a basic knowledge of the possibilities and application of particular instrumental methods for solving analytical problems. | lecture | written test |
K_W04++ |
P6S_WG |
03 | Knows basic concepts connected with the instrumental methods used for analysis of the materials and organic compounds. | lecture | written test |
K_W04++ |
P6S_WG |
04 | Is able to justify the choice of a particular instrumental method suitable to the analytical and economical conditions. | lecture, laboratory | written test |
K_U11++ K_U21+ |
P6S_UO P6S_UW |
05 | Is able to make use of analytical instruments to perform individual types of analysis. | laboratory | written test, observation of job performance |
K_U21++ |
P6S_UW |
06 | Can select the appropriate calibration method; carry out identification and elimination of measurement errors. | lecture, laboratory | written test |
K_U11+ |
P6S_UO P6S_UW |
07 | Is able to prepare a report on the results of the investigation, perform interpretation and evaluation of the analysis results and draw correct conclusions. | laboratory | written report |
K_U21+ |
P6S_UW |
08 | Is abble to work individually and in a team environment in laboratory of instrumental analysis. | laboratory | observation of job performance |
K_U21+ |
P6S_UW |
09 | Is able to identify a situation threatening to life or health and follow the principles of safe work in chemical laboratory. | laboratory | observation of job performance |
K_U14+ |
P6S_UW |
10 | Understand the need of widening their knowledge in the field of new solutions related to equipment and methods of instrumental analysis. | lecture, laboratory | observation of job performance |
K_K01++ |
P6S_KK P6S_KO P6S_KR |
Attention: Depending on the epidemic situation, verification of the achieved learning outcomes specified in the study program, in particular credits and examinations at the end of specific classes, can be implemented remotely (real-time meetings).
Sem. | TK | The content | realized in | MEK |
---|---|---|---|---|
5 | TK01 | W30 | MEK01 MEK02 MEK03 MEK04 MEK06 MEK10 | |
5 | TK02 | L45 | MEK01 MEK04 MEK05 MEK07 MEK08 MEK09 MEK10 |
The type of classes | The work before classes | The participation in classes | The work after classes |
---|---|---|---|
Lecture (sem. 5) | contact hours:
18.00 hours/sem. |
complementing/reading through notes:
10.00 hours/sem. Studying the recommended bibliography: 20.00 hours/sem. |
|
Laboratory (sem. 5) | The preparation for a Laboratory:
10.00 hours/sem. The preparation for a test: 30.00 hours/sem. |
contact hours:
27.00 hours/sem. |
Finishing/Making the report:
25.00 hours/sem. |
Advice (sem. 5) | |||
Credit (sem. 5) | The preparation for a Credit:
15.00 hours/sem. |
The written credit:
2.00 hours/sem. |
The type of classes | The way of giving the final grade |
---|---|
Lecture | A written test including the content of lectures and laboratories. The test includes theoretical part and calculation problems. The mark (OW) depends on the score gained: 3.0 (50.0%-60.0%) MP ; 3.5 (60.1%-70.0%) MP; 4.0 (70.1%-80.0%) MP; 4,5 (80.1%-90.0%) MP; 5.0 (90.1%-100%) MP. MP denotes the full score. |
Laboratory | The necessary condition for receiving a credit for the laboratory is obtaining at least a passing mark on each exercise included in the schedule. The mark obtained during each laboratory exercise is an arithmetic mean of the marks for a written/oral test, correct performance of an experiment and correct preparation of a report. The total mark in the laboratory work (OL) is calculated as arithmetic mean of the marks obtained for every exercise included in the schedule. A final mark for the laboratory is rounded according to WKZJK. |
The final grade | The final mark in the module (K) is calculated according to the formula: K= w 0,5 OW + w 0,5 OL; where: OW, OL denote positive marks for lecture test and laboratory practice, respectively, w - coefficient for delay, w =1.0 when a passing mark is obtained in due time, w=0.9 for a first resit, w=0.8 for a second resit. The final mark is rounded according to WKZJK. |
Required during the exam/when receiving the credit
(-)
Realized during classes/laboratories/projects
(-)
Others
(-)
Can a student use any teaching aids during the exam/when receiving the credit : no
1 | D. Naróg; A. Sobkowiak | Electrochemistry of Flavonoids | 2023 |
2 | P. Chmielarz; T. Pacześniak; K. Rydel-Ciszek; A. Sobkowiak | Bio-Inspired Iron Pentadentate Complexes as Dioxygen Activators in the Oxidation of Cyclohexene and Limonene | 2023 |
3 | Ł. Florczak; B. Kościelniak; A. Kramek; A. Sobkowiak | The Influence of Potassium Hexafluorophosphate on the Morphology and Anticorrosive Properties of Conversion Coatings Formed on the AM50 Magnesium Alloy by Plasma Electrolytic Oxidation | 2023 |
4 | D. Naróg; A. Sobkowiak | Electrochemical Investigation of some Flavonoids in Aprotic Media | 2022 |
5 | K. Darowicki; Ł. Florczak; G. Nawrat; K. Raga; J. Ryl; J. Sieniawski; A. Sobkowiak; M. Wierzbińska | The Effect of Sodium Tetrafluoroborate on the Properties of Conversion Coatings Formed on the AZ91D Magnesium Alloy by Plasma Electrolytic Oxidation | 2022 |
6 | A. Baran; M. Drajewicz; A. Dryzner; M. Dubiel; Ł. Florczak; M. Kocój-Toporowska; A. Krząkała; K. Kwolek; P. Kwolek; G. Lach; G. Nawrat; Ł. Nieużyła; K. Raga; J. Sieniawski; A. Sobkowiak; T. Wieczorek | Method of Forming Corrosion Resistant Coating and Related Apparatus | 2021 |
7 | P. Chmielarz; A. Miłaczewska; T. Pacześniak; K. Rydel-Ciszek; A. Sobkowiak | ‘Oxygen-Consuming Complexes’–Catalytic Effects of Iron–Salen Complexes with Dioxygen | 2021 |
8 | P. Błoniarz; P. Chmielarz; T. Pacześniak; K. Rydel-Ciszek; A. Sobkowiak; K. Surmacz; I. Zaborniak | Iron-Based Catalytically Active Complexes in Preparation of Functional Materials | 2020 |
9 | P. Chmielarz; A. Gennaro; G. Grześ; A. Isse; A. Sobkowiak; K. Wolski; I. Zaborniak; S. Zapotoczny | Tannic acid-inspired star-like macromolecules via temporally-controlled multi-step potential electrolysis | 2019 |