Item card
Instrumential analysis
Some basic information about the module
Cycle of education:
2022/2023
The name of the faculty organization unit:
The faculty Chemistry
The name of the field of study:
Chemical Technology
The area of study:
technical sciences
The profile of studing:
The level of study:
first degree study
Type of study:
past time
discipline specialities :
Chemical analysis in industry and environment, Chemical and bioprocess engineering, Organic and polymer technology
The degree after graduating from university:
Bachelor of Science (BSc)
The name of the module department :
Department of Physical Chemistry
The code of the module:
5273
The module status:
mandatory for teaching programme Chemical analysis in industry and environment, Chemical and bioprocess engineering, Organic and polymer technology
The position in the studies teaching programme:
sem: 5 / W18 L27 / 6 ECTS / Z
The language of the lecture:
Polish
The name of the coordinator 1:
Julian Kozioł, PhD, Eng.
The name of the coordinator 2:
Prof. Andrzej Sobkowiak, DSc, PhD, Eng.
The aim of studying and bibliography
The main aim of study:
Acquisition of a theoretical knowledge and experience on practical applications of modern instrumental analysis techniques used for chemical analysis of organic and inorganic compounds.
The general information about the module:
The module is realised in the 5-th semester and include 30 hours of lectures and 45 hours of laboratory practice. Module ends with a graded assignment.
others:
Instrukcje do ćwiczeń laboratoryjnych
Bibliography required to complete the module
| 1 | K. Danzer i inn. | Analityka – przegląd systematyczny | WNT, Warszawa . | 1993 |
| 2 | A. Cygański | Metody spektroskopowe w chemii analitycznej | WNT, Warszawa. | 1997 |
| 3 | E. Hoffmann, J. Charette, V. Stroobant | Spektrometria mas | WNT, Warszawa. | 1998 |
| 4 | A. Cygański | Metody elektroanalityczne | WNT, Warszawa. | 1995 |
| 5 | Z. Witkiewicz | Podstawy chromatografii | WNT, Warszawa. | 2005 |
| 1 | W. Szczepaniak | Metody instrumentalne w analizie chemicznej | PWN, Warszawa. | 2004 |
| 2 | R.M. Silverstein i inn. | Spektroskopowe metody identyfikacji związków organicznych | PWN, Warszawa. | 2007 |
| 1 | W. Szczepaniak | Metody instrumentalne w analizie chemicznej | PWN, Warszawa. | 2004 |
Basic requirements in category knowledge/skills/social competences
Formal requirements:
Registration for V semester
Basic requirements in category knowledge:
Knowledge and understanding of the basic physics, general, analytical, organic and physical chemistry.
Basic requirements in category skills:
Skills in calculation of chemical concentration, solutions preparation, operation of basic laboratory equipment for chemical analysis, measurement as well as computer. A basic knowledge of mathematics
Basic requirements in category social competences:
Knowledge of principles of safe work in chemical laboratory, responsibility during experiments performed individually or in laboratory group.
Module outcomes
| MEK | The student who completed the module | Types of classes / teaching methods leading to achieving a given outcome of teaching | Methods of verifying every mentioned outcome of teaching | Relationships with KEK | Relationships with PRK |
|---|---|---|---|---|---|
| MEK01 | Has a theoretical and practical knowledge of construction and mechanizm of action of modern analytical equipment. | lecture, laboratory | written test, performance observation |
K-W04++ |
P6S-WG |
| MEK02 | Has a basic knowledge of the possibilities and application of particular instrumental methods for solving analytical problems. | lecture | written test |
K-W04++ |
P6S-WG |
| MEK03 | Knows basic concepts connected with the instrumental methods used for analysis of the materials and organic compounds. | lecture | written test |
K-W04++ |
P6S-WG |
| MEK04 | Is able to justify the choice of a particular instrumental method suitable to the analytical and economical conditions. | lecture, laboratory | written test |
K-U11++ K-U21+ |
P6S-UO P6S-UW |
| MEK05 | Is able to make use of analytical instruments to perform individual types of analysis. | laboratory | written test, observation of job performance |
K-U21++ |
P6S-UW |
| MEK06 | Can select the appropriate calibration method; carry out identification and elimination of measurement errors. | lecture, laboratory | written test |
K-U11+ |
P6S-UO P6S-UW |
| MEK07 | Is able to prepare a report on the results of the investigation, perform interpretation and evaluation of the analysis results and draw correct conclusions. | laboratory | written report |
K-U21+ |
P6S-UW |
| MEK08 | Is abble to work individually and in a team environment in laboratory of instrumental analysis. | laboratory | observation of job performance |
K-U21+ |
P6S-UW |
| MEK09 | Is able to identify a situation threatening to life or health and follow the principles of safe work in chemical laboratory. | laboratory | observation of job performance |
K-U14+ |
P6S-UW |
| MEK10 | Understand the need of widening their knowledge in the field of new solutions related to equipment and methods of instrumental analysis. | lecture, laboratory | observation of job performance |
K-K01++ |
P6S-KK P6S-KO P6S-KR |
The syllabus of the module
| Sem. | TK | The content | realized in | MEK |
|---|---|---|---|---|
| 5 | TK01 | W30 | MEK01 MEK02 MEK03 MEK04 MEK06 MEK10 | |
| 5 | TK02 | L45 | MEK01 MEK04 MEK05 MEK07 MEK08 MEK09 MEK10 |
The student's effort
| The type of classes | The work before classes | The participation in classes | The work after classes |
|---|---|---|---|
| Lecture (sem. 5) | contact hours:
18.00 hours/sem. |
complementing/reading through notes:
10.00 hours/sem. Studying the recommended bibliography: 20.00 hours/sem. |
|
| Laboratory (sem. 5) | The preparation for a Laboratory:
10.00 hours/sem. The preparation for a test: 30.00 hours/sem. |
contact hours:
27.00 hours/sem. |
Finishing/Making the report:
25.00 hours/sem. |
| Advice (sem. 5) | |||
| Credit (sem. 5) | The preparation for a Credit:
15.00 hours/sem. |
The written credit:
2.00 hours/sem. |
The way of giving the component module grades and the final grade
| The type of classes | The way of giving the final grade |
|---|---|
| Lecture | A written test including the content of lectures and laboratories. The test includes theoretical part and calculation problems. The mark (OW) depends on the score gained: 3.0 (50.0%-60.0%) MP ; 3.5 (60.1%-70.0%) MP; 4.0 (70.1%-80.0%) MP; 4,5 (80.1%-90.0%) MP; 5.0 (90.1%-100%) MP. MP denotes the full score. |
| Laboratory | The necessary condition for receiving a credit for the laboratory is obtaining at least a passing mark on each exercise included in the schedule. The mark obtained during each laboratory exercise is an arithmetic mean of the marks for a written/oral test, correct performance of an experiment and correct preparation of a report. The total mark in the laboratory work (OL) is calculated as arithmetic mean of the marks obtained for every exercise included in the schedule. A final mark for the laboratory is rounded according to WKZJK. |
| The final grade | The final mark in the module (K) is calculated according to the formula: K= w 0,5 OW + w 0,5 OL; where: OW, OL denote positive marks for lecture test and laboratory practice, respectively, w - coefficient for delay, w =1.0 when a passing mark is obtained in due time, w=0.9 for a first resit, w=0.8 for a second resit. The final mark is rounded according to WKZJK. |
Sample problems
Required during the exam/when receiving the credit
(-)
Realized during classes/laboratories/projects
(-)
Others
(-)
Can a student use any teaching aids during the exam/when receiving the credit : no
The contents of the module are associated with the research profile yes
| 1 | K. Rydel-Ciszek; A. Sobkowiak | The [(Bn-tpen)FeII]2+ Complex as a Catalyst for the Oxidation of Cyclohexene and Limonene with Dioxygen | 2024 |
| 2 | D. Naróg; A. Sobkowiak | Electrochemistry of Flavonoids | 2023 |
| 3 | P. Chmielarz; T. Pacześniak; K. Rydel-Ciszek; A. Sobkowiak | Bio-Inspired Iron Pentadentate Complexes as Dioxygen Activators in the Oxidation of Cyclohexene and Limonene | 2023 |
| 4 | Ł. Florczak; B. Kościelniak; A. Kramek; A. Sobkowiak | The Influence of Potassium Hexafluorophosphate on the Morphology and Anticorrosive Properties of Conversion Coatings Formed on the AM50 Magnesium Alloy by Plasma Electrolytic Oxidation | 2023 |
| 5 | D. Naróg; A. Sobkowiak | Electrochemical Investigation of some Flavonoids in Aprotic Media | 2022 |
| 6 | K. Darowicki; Ł. Florczak; G. Nawrat; K. Raga; J. Ryl; J. Sieniawski; A. Sobkowiak; M. Wierzbińska | The Effect of Sodium Tetrafluoroborate on the Properties of Conversion Coatings Formed on the AZ91D Magnesium Alloy by Plasma Electrolytic Oxidation | 2022 |
| 7 | A. Baran; M. Drajewicz; A. Dryzner; M. Dubiel; Ł. Florczak; M. Kocój-Toporowska; A. Krząkała; K. Kwolek; P. Kwolek; G. Lach; G. Nawrat; Ł. Nieużyła; K. Raga; J. Sieniawski; A. Sobkowiak; T. Wieczorek | Method of Forming Corrosion Resistant Coating and Related Apparatus | 2021 |
| 8 | P. Chmielarz; A. Miłaczewska; T. Pacześniak; K. Rydel-Ciszek; A. Sobkowiak | ‘Oxygen-Consuming Complexes’–Catalytic Effects of Iron–Salen Complexes with Dioxygen | 2021 |
| 9 | P. Błoniarz; P. Chmielarz; T. Pacześniak; K. Rydel-Ciszek; A. Sobkowiak; K. Surmacz; I. Zaborniak | Iron-Based Catalytically Active Complexes in Preparation of Functional Materials | 2020 |