The aim of studying and bibliography

The main aim of study: Acquiring knowledge on the physicochemical methods used for the characterization of materials properties.

The general information about the module: The module provides information about the methods of determination of the physicochemical properties of materials. The module is introduced in the 2nd semester of the second degree studies. It is accomplished with 30 hours and ends with an examination-based assessment.

Bibliography required to complete the module

Bibliography used during lectures

1	Oliver H. Wyatt, David Dew-Hughes	Wprowadzenie do inżynierii materiałowej; metale, ceramika i tworzywa sztuczne	WNT Warszawa .	1978
2	Marek Blicharski	Wstęp do inżynierii materiałowej	WNT Warszawa.	1998
3	Włodzimierz Przygocki	Metody fizyczne badań polimerów	WNT Warszawa.	1990
4	Jan F. Rabek	Współczesna wiedza o polimerach	PWN Warszawa.	2008
5	Teresa Kasprzycka-Gutman	Elementy kalorymetrii statycznej i dynamicznej,	WNT Warszawa.	1993
6	Kevin P. Menard	Dynamic mechanical analysis. A practical introduction	CRC Press, Taylor & Francis Group.	2008
7	Grzegorz Golański, Agata Dudek, Zbigniew Bałaga	Metody badania właściwości materiałów	Wydawnictwo Politechniki Częstochowskiej, Częstochowa.	2011
8	Henryk Leda	Materiały inżynierskie w zastosowaniach biomedycznych	Wydawnictwo Politechniki Poznańskiej, Poznań.	2011
9	Jan Sieniawski, Aleksander Cyunczyk	Właściwości ciał stałych	Oficyna Wydawnicza Politechniki Rzeszowskiej, Rzeszów.	2009
10	Jan Sieniawski, Aleksander Cyunczyk	Struktura ciał stałych	Oficyna Wydawnicza Politechniki Rzeszowskiej, Rzeszów.	2008
11	Elton N. Kaufmann	Characterization of materials, vol.2	Hoboken, N.J., Wiley-Interscience, Great Britain.	2003
12	Aneta Liber-Kneć, Sylwia Łagan	Ćwiczenia laboratoryjne z biomateriałów : pomoc dydaktyczna	Wydawnictwo Politechniki Krakowskiej, Kraków.	2011
13	Mieczysław Jurczyk, Jarosław Jakubowicz	Bionanomateriały	Wydawnictwo Politechniki Poznańskiej, Poznań.	2008

Basic requirements in category knowledge/skills/social competences

Formal requirements: Completed modulus on instrumental and chemical analysis and physical chemistry

Basic requirements in category knowledge: Has knowledge on instrumental and chemical analysis and physical chemistry.

Basic requirements in category skills: Has a skill in analysis of measurement data, performing calculations and interpretation of results.

Basic requirements in category social competences: Knows safety and fire protection regulation in chemical laboratory. Capable of working in team and individually.

Module outcomes

MEK	The student who completed the module	Types of classes / teaching methods leading to achieving a given outcome of teaching	Methods of verifying every mentioned outcome of teaching	Relationships with KEK	Relationships with PRK
01	Has the basic knowledge on the types of materials and their basic properties, with particular emphasis on organic materials and biomaterials.	lecture	written test, oral test	K_W05+ K_W08+	P7S_WG
02	Knows the methods used for assessing of the properties of organic materials and biomaterilas, in particular the physical and chemical properties.	lecture	written test, oral test	K_W05+ K_W08++	P7S_WG
03	Knows advanced testing methods of structure and properties of organic materials both in a condensed state and in solution.	lecture	written test, oral test	K_W05++	P7S_WG
04	Can propose, evaluate the usefulness and apply appropriate methods to the determination of selected properties of materials.	lecture	written test, oral test	K_W08+	P7S_WG

Attention: Depending on the epidemic situation, verification of the achieved learning outcomes specified in the study program, in particular credits and examinations at the end of specific classes, can be implemented remotely (real-time meetings).

The syllabus of the module

Sem.	TK	The content	realized in	MEK
2	TK01	Organic materials, metals, ceramic and composites - characteristic of basic properties.	W01	MEK01
2	TK02	Methods of samples preparation for analytical process.	W02	MEK01
2	TK03	Characteristic of the basic physical properties of materials: density, porosity, solubility, moisture content, absorbability, etc. Measurements of viscosity.	W03, W04	MEK02 MEK03 MEK04
2	TK04	Macromolecular compounds - types of average molecular weight of polymers and biopolymers.	W05	MEK02 MEK03 MEK04
2	TK05	The study of polymer solutions: determination of the molecular weight: viscometry, osmometry, ebullioscopy and cryoscopy, sedimentation methods, gel permeation chromatography GPC and i MALDI-TOF, etc.	W06, W07	MEK02 MEK03 MEK04
2	TK06	Methods for determination of particle size. Zeta potential.	W08, W09	MEK02 MEK03 MEK04
2	TK07	Testing methods using electromagnetic radiation: static (Rayleigh) light scattering, dynamic (quasi-elastic) light scattering, small angle light scattering, X-ray methods (SAXS, WAXS), neutron scattering.	W09, W10, W11	MEK02 MEK03 MEK04
2	TK08	Testing methods of materials in condensed state: optical and electron microscopy, atomic force microscopy.	W12	MEK02 MEK03 MEK04
2	TK09	Methods of thermal analysis (DSC, TGA, TMA, DMA, etc.).	W13, W14	MEK02 MEK03 MEK04
2	TK10	Determination of electric, magnetic, acustic, optical properties of organic materials and biomaterials.	W14, W15

The student's effort

The type of classes	The work before classes	The participation in classes	The work after classes
Lecture (sem. 2)		contact hours: 30.00 hours/sem.	complementing/reading through notes: 2.00 hours/sem. Studying the recommended bibliography: 3.00 hours/sem.
Laboratory (sem. 2)		contact hours: 15.00 hours/sem.
Advice (sem. 2)		The participation in Advice: 2.00 hours/sem.
Credit (sem. 2)	The preparation for a Credit: 2.00 hours/sem.	The written credit: 1.00 hours/sem. The oral credit: 1.00 hours/sem.

The way of giving the component module grades and the final grade

The type of classes	The way of giving the final grade
Lecture	Mark of the written test and oral test (W1).
Laboratory
The final grade	Mark of the written test and oral test (W1).

Sample problems

Required during the exam/when receiving the credit
(-)

Realized during classes/laboratories/projects
(-)

Others
(-)

Can a student use any teaching aids during the exam/when receiving the credit : no

The contents of the module are associated with the research profile: yes

1	J. Bieniaś; Ł. Byczyński; D. Czachor-Jadacka; M. Droździel-Jurkiewic; M. Kisiel; B. Mossety-Leszczak; G. Pietruszewska; M. Włodarska; W. Zając	Nonterminal liquid crystalline epoxy resins as structurally ordered low Tg thermosets with potential as smart polymers	2024
2	K. Awsiuk; N. Janiszewska; B. Mossety-Leszczak; J. Raczkowska; A. Strachota; B. Strachota; M. Walczak; A. Zioło	Synthesis and Morphology Characteristics of New Highly Branched Polycaprolactone PCL	2024
3	M. Kisiel; B. Mossety-Leszczak	The Effect of Nonterminal Liquid Crystalline Epoxy Resin Structure and Curing Agents on the Glass Transition of Polymer Networks	2024
4	M. Kisiel; B. Mossety-Leszczak; L. Okrasa; M. Włodarska	Modification of the Dielectric and Thermal Properties of Organic Frameworks Based on Nonterminal Epoxy Liquid Crystal with Silicon Dioxide and Titanium Dioxide	2024
5	M. Kisiel; B. Mossety-Leszczak; W. Zając	Advancements in The Cross-Linking and Morphology of Liquid Crystals	2024
6	Ł. Byczyński; D. Czachor-Jadacka; M. Kisiel; B. Mossety-Leszczak; B. Pilch-Pitera; K. Pojnar; M. Walczak; J. Wojturska	Poliuretanowy lakier proszkowy oraz sposób wytwarzania poliuretanowego lakieru proszkowego	2024
7	Ł. Byczyński; E. Ciszkowicz; D. Czachor-Jadacka; M. Kisiel; B. Mossety-Leszczak; B. Pilch-Pitera; M. Walczak; J. Wojturska	Wodna dyspersja kationomerów uretanowo-akrylowych, sposób wytwarzania wodnej dyspersji kationomerów uretanowo-akrylowych oraz sposób wytwarzania fotoutwardzalnej powłoki z wykorzystaniem tej wodnej dyspersji	2024
8	M. Kisiel; B. Mossety-Leszczak; L. Okrasa; M. Włodarska; W. Zając	Changes in molecular relaxations and network properties of a triaromatic liquid crystal epoxy resin with nonterminal functional groups	2023
9	Ż. Szymaszek; M. Twardowska; Ł. Uram; M. Walczak; S. Wołowiec; K. Wróbel	Exploring the Potential of Lapatinib, Fulvestrant, and Paclitaxel Conjugated with Glycidylated PAMAM G4 Dendrimers for Cancer and Parasite Treatment	2023
10	J. Karaś; M. Kisiel; B. Mossety-Leszczak; B. Pilch-Pitera; M. Włodarska; W. Zając	The application of liquid crystalline epoxy resin for forming hybrid powder coatings	2022
11	J. Lubczak; M. Walczak	e-caprolactone and pentaerythritol derived oligomer for rigid polyurethane foams preparation	2022
12	K. Byś; J. Hodan; B. Mossety-Leszczak; E. Pavlova; A. Strachota; B. Strachota	Self-Healing and Super-Elastomeric PolyMEA-co-SMA Nanocomposites Crosslinked by Clay Platelets	2022
13	M. Kisiel; B. Mossety-Leszczak	Liquid Crystalline Polymers	2022
14	Ł. Byczyński; A. Kramek; B. Pilch-Pitera; K. Pojnar; M. Walczak; W. Zając	Polyacrylate resins containing fluoroalkyl groups for powder clear coatings	2022
15	B. Mossety-Leszczak; M. Włodarska	DFT Studies of Selected Epoxies with Mesogenic Units–Impact of Molecular Structure on Electro-Optical Response	2021
16	J. Lubczak; R. Lubczak; M. Szpiłyk; M. Walczak	Polyol and polyurethane foam from cellulose hydrolysate	2021
17	K. Byś; B. Mossety-Leszczak; E. Pavlova; M. Steinhart; A. Strachota; B. Strachota; W. Zając	Novel Tough and Transparent Ultra-Extensible Nanocomposite Elastomers Based on Poly(2-methoxyethylacrylate) and Their Switching between Plasto-Elasticity and Viscoelasticity	2021
18	M. Bakar; A. Białkowska; A. Czerniecka-Kubicka; L. Dobrowolski; K. Hęclik; K. Leś; M. Pyda; M. Walczak; I. Zarzyka	Thermally stable biopolymer composites based on poly(3-hydroxybutyrate) modified with linear aliphatic polyurethanes – preparation and properties	2021
19	M. Kisiel; B. Mossety-Leszczak; A. Strachota; B. Strachota	Achieving structural anisotropy of liquid crystalline epoxy by manipulation with crosslinking parameters	2021
20	M. Kowal; B. Król; P. Król; K. Nowicka; K. Pielichowska; M. Walczak	Polyurethane cationomers containing fluorinated soft segments with hydrophobic properties	2021
21	B. Król; P. Król; K. Pielichowska; M. Sochacka-Piętal; Ł. Uram; M. Walczak	Synthesis and property of polyurethane elastomer for biomedical applications based on nonaromatic isocyanates, polyesters, and ethylene glycol	2020
22	E. Chmiel; A. Czerniecka-Kubicka; M. Misiorek; M. Pyda; P. Tutka; Ł. Uram; M. Walczak; S. Wołowiec	Stepwise glucoheptoamidation of poly(amidoamine) dendrimer G3 to tune physicochemical properties of the potential drug carrier: in vitro tests for cytisine conjugates	2020
23	M. Kisiel; B. Mossety-Leszczak	Development in liquid crystalline epoxy resins and composites – A review	2020
24	M. Marchel; B. Mossety-Leszczak; M. Walczak	Maize (Zea mays) reaction in response to rubber rag additive into the soil	2020
25	S. Horodecka; D. Kaňková; B. Mossety-Leszczak; M. Netopilík; M. Šlouf; A. Strachota; B. Strachota; M. Vyroubalová; Z. Walterová; A. Zhigunov	Low-Temperature Meltable Elastomers Based on Linear Polydimethylsiloxane Chains Alpha, Omega-Terminated with Mesogenic Groups as Physical Crosslinkers: A Passive Smart Material with Potential as Viscoelastic Coupling. Part I: Synthesis and Phase Behavior	2020
26	S. Horodecka; D. Kaňková; B. Mossety-Leszczak; M. Netopilík; M. Šlouf; A. Strachota; M. Vyroubalová; A. Zhigunov	Meltable copolymeric elastomers based on polydimethylsiloxane with multiplets of pendant liquid-crystalline groups as physical crosslinker: A self-healing structural material with a potential for smart applications.	2020
27	S. Horodecka; M. Kisiel; B. Mossety-Leszczak; M. Šlouf; A. Strachota; B. Strachota	Low-Temperature-Meltable Elastomers Based on Linear Polydimethylsiloxane Chains Alpha, Omega-Terminated with Mesogenic Groups as Physical Crosslinker: A Passive Smart Material with Potential as Viscoelastic Coupling. Part II—Viscoelastic and Rheological Properties	2020
28	A. Frańczak; M. Kisiel; B. Mossety-Leszczak; D. Szczęch	Quantitative analysis of the polymeric blends	2019
29	D. Aebisher; A. Białońska; M. Kopaczyńska; P. Sareło; Ł. Uram; M. Walczak; S. Wołowiec; M. Zaręba	Mixed-Generation PAMAM G3-G0 Megamer as a Drug Delivery System for Nimesulide: Antitumor Activity of the Conjugate Against Human Squamous Carcinoma and Glioblastoma Cells	2019
30	N. Buszta; M. Kisiel; J. Lechowicz; B. Mossety-Leszczak; R. Ostatek; M. Włodarska	Analysis of curing reaction of liquid-crystalline epoxy compositions by using temperature-modulated DSC TOPEM (R)	2019