The aim of studying and bibliography

The main aim of study: Students become conversant with solid-fluid mass transfer processes

The general information about the module: The module is implemented in the sixth semester. It includes 30 hours of lectures, 30 hours of classes, 15 hours of designing and 15 hours laboratory. It ends with an exam.

Bibliography required to complete the module

Bibliography used during lectures

1	R. Petrus, G. Aksielrud, J. Gumnicki, W. Piątkowski	Wymiana masy ciało stałe – ciecz	OW PRz.	1998
2	R. Rautenbach	Procesy membranowe	WNT.	1996
3	R. Koch, A. Kozioł	Dyfuzyjno-cieplny rozdział substancji	WNT.	1994
4	S. Wroński, R. Pohorecki, J. Siwiński	Przykłady obliczeń z termodynamiki i kinetyki procesów inżynierii chemicznej	WNT.	1979

Bibliography used during classes/laboratories/others

1	K. Pawłow, P. Romankow, A.Noskow	Przykłady i zadania z zakresu aparatury i inżynierii chemicznej	WNT.	1981
2	Praca zbiorowa pod red. R. Zarzycki	Zadania rachunkowe z inżynierii chemicznej	PWN.	1980

Basic requirements in category knowledge/skills/social competences

Formal requirements: Registration for the corresponding semester

Basic requirements in category knowledge: student has basic knowledge in mathematics (calculus) and understands the principles of balancing processes

Basic requirements in category skills: Student can derive simple mass or heat balance

Basic requirements in category social competences: no requirements

Module outcomes

MEK	The student who completed the module	Types of classes / teaching methods leading to achieving a given outcome of teaching	Methods of verifying every mentioned outcome of teaching	Relationships with KEK	Relationships with PRK
01	knows mechanisms of mass transfer in the liquid-solid systems	lecture	written exam	K_W03+	P6S_WG
02	has knowledge on membrane processes, crystallization and dissolution proceses	lecture	written exam	K_W05+	P6S_WG
03	has knowledge of the apparatus used for membrane processes, crystallization and dissolution of solids	lecture	written exam	K_W05+	P6S_WG
04	can propose the balance of a typical process and calculate some parameters	classes, laboratory, designing	written tests, written report, presentation of the prepared design	K_U05+ K_U08+ K_U19+ K_K01+	P6S_KK P6S_UU P6S_UW
05	is able to supervise the simple experiment in the laboratory scale for mass exchange process, to prepare a report	laboratory	observation of performance, written report	K_U06+	P6S_UW
06	is able to work in a team	laboratory	observation of performance	K_U18+	P6S_UO

Attention: Depending on the epidemic situation, verification of the achieved learning outcomes specified in the study program, in particular credits and examinations at the end of specific classes, can be implemented remotely (real-time meetings).

The syllabus of the module

Sem.	TK	The content	realized in	MEK
6	TK01	Mechanisms of mass transfer. Diffusion equation and its application. The mass balance in the system liquid-solid	W01-W06,C01-C08	MEK01
6	TK02	Mass transfer for fluid flow around solid particle for small and large values ​​of Reynolds number. Mass transfer and natural convection.	W07-W09,C09-C12	MEK01 MEK02
6	TK03	Objectives and methods of the dissolution process. Basic concepts. The kinetics of dissolution. Different methods of dissolution.	W10-W15,C13-C16,L01-L04	MEK02 MEK03 MEK04
6	TK04	Objectives and methods of crystallization. Basic concepts. Growth of crystals. Phase equilibrium . Mass and heat balance. Special methods of crystallization.	W16-W21,C17-C24,L05-08	MEK02 MEK03 MEK04 MEK05 MEK06
6	TK05	Objectives and methods of membrane processes. The structure and preparation of membranes. Classification of membranes. The driving force and transport resistance. Models of mass transport in the membrane. Applications of membrane processes.	W22-W30,C25-C30	MEK01 MEK03 MEK04
6	TK06	Presentation of commercial apparatus and techniques for mass transfer processes.	L09-L15	MEK05 MEK06
6	TK07	Computing procedures and methods for the typical process of mass transfer	P01-P15	MEK04 MEK05

The student's effort

The type of classes	The work before classes	The participation in classes	The work after classes
Lecture (sem. 6)		contact hours: 30.00 hours/sem.	complementing/reading through notes: 10.00 hours/sem. Studying the recommended bibliography: 15.00 hours/sem.
Class (sem. 6)	The preparation for a Class: 15.00 hours/sem. The preparation for a test: 6.00 hours/sem.	contact hours: 15.00 hours/sem.	Finishing/Studying tasks: 10.00 hours/sem.
Laboratory (sem. 6)	The preparation for a Laboratory: 6.00 hours/sem.	contact hours: 15.00 hours/sem.	Finishing/Making the report: 10.00 hours/sem.
Project/Seminar (sem. 6)	The preparation for projects/seminars: 2.00 hours/sem.	contact hours: 15.00 hours/sem..	Doing the project/report/ Keeping records: 15.00 hours/sem. Others: 2.00 hours/sem.
Advice (sem. 6)	The preparation for Advice: 2.00 hours/sem.	The participation in Advice: 8.00 hours/sem.
Exam (sem. 6)	The preparation for an Exam: 15.00 hours/sem.	The written exam: 3.00 hours/sem.

The way of giving the component module grades and the final grade

The type of classes	The way of giving the final grade
Lecture	written exam 47,0-60,0% =3,0 60,1-70,0% = 3,5 70,1-80,0% = 4,0 81,1-90,0% = 4,5 90,1-100% = 5,0
Class	two written tests 47,0-60,0% =3,0 60,1-70,0% = 3,5 70,1-80,0% = 4,0 81,1-90,0% = 4,5 90,1-100% = 5,0
Laboratory	passing all labs reports, written test 47,0-60,0% =3,0 60,1-70,0% = 3,5 70,1-80,0% = 4,0 81,1-90,0% = 4,5 90,1-100% = 5,0
Project/Seminar	passing of the project
The final grade	final mark (K): K=0,4 w C + 0,1 w L +0,2 w P + 0,3 w E; E - mark for lecture L - mark for lab C - mark for classes P - mark for design w - weigthing factor: w = 1,0 first term, w = 0,9 second term, w = 0,8 third term.

Sample problems

Required during the exam/when receiving the credit
(-)

Realized during classes/laboratories/projects
(-)

Others
(-)

Can a student use any teaching aids during the exam/when receiving the credit : no

The contents of the module are associated with the research profile: yes

1	M. Przywara; R. Przywara; W. Zapała	Numerical Investigation on Flowability of Pulverized Biomass Using the Swelling Bed Model	2024
2	A. Bukowska; T. Galek; M. Przywara; R. Przywara; W. Zapała	Brief Analysis of Selected Sorption and Physicochemical Properties of Three Different Silica-Based Adsorbents	2023
3	I. Opaliński; M. Przywara; R. Przywara; W. Zapała	Mechanical Properties of Solid Biomass as Affected by Moisture Content	2023
4	M. Chutkowski; I. Opaliński; M. Przywara; R. Przywara; W. Zapała	Influence of Moisture Content and Composition of Agricultural Waste with Hard Coal Mixtures on Mechanical and Rheological Properties	2023
5	M. Przywara; R. Przywara; W. Zapała	Właściwości adsorpcyjne wybranych polarnych faz stacjonarnych	2023
6	Ł. Byczyński; M. Kosińska-Pezda; E. Woźnicka; L. Zapała; W. Zapała	Synteza oraz badania składu i właściwości związków: 3-hydroksyflawonu, chryzyny oraz sulfonowych pochodnych chryzyny i kwercetyny z jonami Mn(II)	2023
7	L. Zapała; W. Zapała; P. Ziobrowski	Studies on the retention behavior of quercetin, phenol and caffeine as test substances on selected neutral and charged Hydrophilic Interaction Liquid Chromatography stationary phases	2022
8	M. Chutkowski; J. Kamińska; M. Przywara; W. Zapała; P. Ziobrowski	Studies on the Effects of Process Conditions on Separation of B1, B2 and B3 Vitamin Mixture Using HILIC and RPLC Chromatography	2022
9	M. Chutkowski; M. Przywara; R. Przywara; W. Zapała	Column Testing in Quantitative Determination of Raw Heparin in Porcine Intestinal Mucus Extracts by Liquid Chromatography – Preliminary Investigations	2022
10	M. Kosińska-Pezda; U. Maciołek; E. Woźnicka; L. Zapała; W. Zapała	Synteza, badania składu i właściwości spektroskopowych kompleksów wybranych jonów metali przejściowych z kwasem niflumowym	2022
11	W. Zapała; P. Ziobrowski	Analiza mechanizmu retencji kofeiny, kwercetyny oraz fenolu w wybranych układach chromatografii oddziaływań hydrofilowych (HILIC)	2022
12	M. Chutkowski; L. Zapała; W. Zapała; P. Ziobrowski	Analiza mechanizmu retencji kwercetyny w wybranych układach chromatografii oddziaływań hydrofilowych (HILIC)	2021
13	M. Chutkowski; M. Kosińska-Pezda; M. Przywara; L. Zapała; W. Zapała; P. Ziobrowski	Analysis of adsorption energy distribution in selected hydrophilic-interaction chromatography systems with amide, amine, and zwitterionic stationary phases	2021
14	Ł. Byczyński; E. Ciszkowicz; M. Kosińska-Pezda; K. Lecka-Szlachta; U. Maciołek; E. Woźnicka; L. Zapała; W. Zapała	Green synthesis of niflumic acid complexes with some transition metal ions (Mn(II), Fe(III), Co(II), Ni(II), Cu(II) and Zn(II)). Spectroscopic, thermoanalytical and antibacterial studies	2021
15	Ł. Byczyński; M. Kosińska-Pezda; U. Maciołek; E. Woźnicka; L. Zapała; W. Zapała	Thermal study, temperature diffraction patterns and evolved gas analysis during pyrolysis and oxidative decomposition of novel ternary complexes of light lanthanides with mefenamic acid and 1,10-phenanthroline	2021
16	M. Chutkowski; L. Zapała; W. Zapała; P. Ziobrowski	Influence of Mobile Phase Composition and Temperature on the Retention Behavior of Selected Test Substances in Diol-type Column	2020
17	M. Chutkowski; M. Przywara; W. Zapała	Modelowanie i analiza płynięcia materiału rozdrobionego podczas ścinania w reometrze pierścieniowym z wykorzystaniem metody elementów dyskretnych	2020
18	M. Kosińska; E. Woźnicka; L. Zapała; W. Zapała	Response of the DFT study to the calculations of selected microdissociation constants of anthranilic acid and its derivatives	2019
19	Ł. Byczyński; M. Chutkowski; E. Ciszkowicz; M. Kosińska; K. Lecka-Szlachta; E. Woźnicka; L. Zapała; W. Zapała	Comparison of spectral and thermal properties and antibacterial activity of new binary and ternary complexes of Sm(III), Eu(III) and Gd (III) ions with N-phenylanthranilic acid and 1,10-phenanthroline	2019