The aim of studying and bibliography

The main aim of study: Familiarize the students with the theoretical basis of most important instrumental analysis techniques and operational principles of modern apparatus used for chemical analysis in industry and environment protection.

The general information about the module: The module is realised in the 5-th semester and include 30 hours of lectures and 30 hours of laboratory practice. Module ends with a graded assignment.

others: Instrukcje do ćwiczeń laboratoryjnych

Bibliography required to complete the module

Bibliography used during lectures

1	K. Danzer i inn.	Analityka – przegląd systematyczny	WNT, Warszawa .	1993
2	A. Cygański	Metody spektroskopowe w chemii analitycznej	WNT, Warszawa.	1997
3	E. Hoffmann, J. Charette, V. Stroobant	Spektrometria mas	WNT, Warszawa.	1998
4	A. Cygański	Metody elektroanalityczne	WNT, Warszawa.	1995
5	Z. Witkiewicz	Podstawy chromatografii	WNT, Warszawa.	2005

Bibliography used during classes/laboratories/others

1	W. Szczepaniak	Metody instrumentalne w analizie chemicznej	PWN, Warszawa.	2004
2	R.M. Silverstein i inn.	Spektroskopowe metody identyfikacji związków organicznych	PWN, Warszawa.	2007

Bibliography to self-study

1

W. Szczepaniak

Metody instrumentalne w analizie chemicznej

PWN, Warszawa.

2004

Basic requirements in category knowledge/skills/social competences

Formal requirements: Registration for V semester

Basic requirements in category knowledge: Knowledge and understanding of the basic physics, general, analytical, organic and physical chemistry.

Basic requirements in category skills: Skills in calculation of chemical concentration, solutions preparation, operation of basic laboratory equipment for chemical analysis, measurement as well as computer. A basic knowledge of mathematics

Basic requirements in category social competences: Knowledge of principles of safe work in chemical laboratory, responsibility during experiments performed individually or in laboratory group.

Module outcomes

MEK	The student who completed the module	Types of classes / teaching methods leading to achieving a given outcome of teaching	Methods of verifying every mentioned outcome of teaching	Relationships with KEK	Relationships with PRK
01	Has a theoretical and practical knowledge of construction and principles of action of modern analytical equipment.	lecture, laboratory	written test, observation of job performance	K_W06+++	P6S_WG
02	Has a basic knowledge on the mechanism of action of particular components of apparatus for instrumental analysis.	lecture, laboratory	written test	K_W06++ K_U08++	P6S_UW P6S_WG
03	Has a basic knowledge of application of particular instrumental methods for laboratory research and control of industrial processes.	lecture	written test	K_W06+ K_U03+++ K_U08++	P6S_UW P6S_WG
04	Is able to make use of given equipment to perform analysis and obtain the analytical data.	laboratory	written test, observation of job performance	K_U03+++	P6S_UW
05	Can select the appropriate analytical method and calibrate the instrument.	lecture, laboratory	written test	K_U03++	P6S_UW
06	Is able to prepare a report on the results of the investigation, perform interpretation and evaluation of the analysis results and draw correct conclusions.	laboratory	written report	K_U08++	P6S_UW
07	Is able to present schemes and explain the principles of operation of apparatus used for the instrumental analysis.	lecture	written test	K_U03++	P6S_UW
08	Understand the need of widening their knowledge in the field of new solutions related to equipment and methods of instrumental analysis.	lecture, laboratory	performance observation	K_U19+++	P6S_UU

Attention: Depending on the epidemic situation, verification of the achieved learning outcomes specified in the study program, in particular credits and examinations at the end of specific classes, can be implemented remotely (real-time meetings).

The syllabus of the module

Sem.	TK	The content	realized in	MEK
5	TK01	The role and tasks of instrumental analysis in industrial processes. Samples acquisition, storage and preparation for analysis. Classification of instrumental methods. Calibration and calibration plots. Errors of analysis, classification, source and minimization of errors. Optical methods. Polarimetry. Quantitative analysis of elements and compounds using spectroscopic methods. Atomic Emission Spectroscopy - theoretical principles, excitation sources, apparatus, ICP-AES and GDL-AES spectrometers. Atomic Absorption Spectroscopy (AAS) principles and applications. Absorption spectroscopy in UV/VIS. IR absorption spectroscopy - application in quantitative and qualitative analysis of organic compounds. Basic principles of magnetic nuclear resonance. Structural and quantitative analysis on the base of 1H-NMR spectra. Principles of mass spectrometry of organic compounds. Interpretation and analytical application of mass spectra. Chromatographic methods - definition and classification. Chromatography theories and their use in practice. Gas chromatography - influence of chromatographic conditions on separation process and analytical performance. Practical applications. High performance liquid chromatography (HPLC). Apparatus and separation techniques: gradient elution and mobile phase programmed flow speed. Optymalisation of separation processes - theory and practice of stationary and mobile phase selection and separation parameters. HPLC applications. Electroanalytical methods. Potentiometry - principles and instrumentation. Construction, principles of operation and applications of chosen ion-selective electrodes (ISE). Voltammetric methods - the main techniques. Selected applications of voltammetric methods in laboratory and industrial analysis. Conductometry - definition, instrumentation and application. Complementarity of instrumental methods. Hyphenated methods. Criteria of choice of the analytical methods.	W30	MEK01 MEK02 MEK03 MEK05 MEK07 MEK08
5	TK02	Determination of elements by using the atomic absorption spectrometry (AAS). Determination of organic compounds using absorption infrared spectroscopy. Determination of chemical substances using absorption spectriscopy in UV/VIS. Analysis of mixtures of organic compounds with application of 1H-NMR spectroscopy.	L30	MEK01 MEK02 MEK04 MEK06 MEK08

The student's effort

The type of classes	The work before classes	The participation in classes	The work after classes
Lecture (sem. 5)		contact hours: 30.00 hours/sem.	complementing/reading through notes: 3.00 hours/sem. Studying the recommended bibliography: 15.00 hours/sem.
Laboratory (sem. 5)	The preparation for a Laboratory: 2.00 hours/sem. Others: 7.00 hours/sem.	contact hours: 30.00 hours/sem.	Finishing/Making the report: 14.00 hours/sem.
Advice (sem. 5)		The participation in Advice: 3.00 hours/sem.
Credit (sem. 5)	The preparation for a Credit: 15.00 hours/sem.	The written credit: 1.00 hours/sem.

The way of giving the component module grades and the final grade

The type of classes	The way of giving the final grade
Lecture	A written test including the content of lectures and laboratories. The test includes theoretical part and calculation problems. The mark (OW) depends on the score gained: 3.0 (50.0%-60.0%) MP ; 3.5 (60.1%-70.0%) MP; 4.0 (70.1%-80.0%) MP; 4,5 (80.1%-90.0%) MP; 5.0 (90.1%-100%) MP. MP denotes the full score.
Laboratory	Receiving at least the pass mark for each exercise included in the schedule is required. The mark obtained during each laboratory exercise is an arithmetic mean of the marks for a written/oral test, correct performance of an experiment and correct preparation of a report. The total mark in the laboratory work (OL) is calculated as arithmetic mean of the marks obtained for every exercise included in the schedule. A final mark for the laboratory is rounded according to WKZJK.
The final grade	The final mark in the module (K) is calculated according to the formula: K= w 0,5 OW + w 0,5 OL; where: OW, OL denote positive marks for lecture test and laboratory practice, respectively, w - coefficient for delay, w =1.0 when a passing mark is obtained in due course, w=0.9 for a first resit, w=0.8 for a second resit. The final mark is rounded according to WKZJK.

Sample problems

Required during the exam/when receiving the credit
(-)

Realized during classes/laboratories/projects
(-)

Others
(-)

Can a student use any teaching aids during the exam/when receiving the credit : no

The contents of the module are associated with the research profile: yes

1	D. Naróg; A. Sobkowiak	Electrochemistry of Flavonoids	2023
2	D. Naróg; A. Sobkowiak	Electrochemical Investigation of some Flavonoids in Aprotic Media	2022
3	D. Naróg	Electrochemical study of quercetin in the presence of galactopyranose: Potential application to the electrosynthesis of glycoconjugates of quinone/quinone methide of quercetin	2020