The aim of studying and bibliography

The main aim of study: Familiarizing students with the basic processes of heavy organic synthesis.

The general information about the module: The module is carried out in the six semester. It includes 30 hours of lecture and 60 hours laboratory. The module ends with an exam.

Teaching materials: Instrukcje do ćwiczeń laboratoryjnych

Bibliography required to complete the module

Bibliography used during lectures

1	Grzywa E., Molenda J.	Technologia podstawowych syntez organicznych (t. 1 i 2)	WNT.	2009
2	Arpe H.J.	Industrial organic Chemistry	Wiley-VCH.	2010
3	Bukowska A., Bukowski W.	Przemysłowa chemia organiczna. Monomery nasycone	Oficyna Wydawnicza Politechniki Rzeszowskiej.	2012
4	Bukowska A., Bukowski B.	Przemysłowa chemia organiczna. Monomery nienasycone	Oficyna Wydawnicza Politechniki Rzeszowskiej.	2013

Basic requirements in category knowledge/skills/social competences

Formal requirements: Registration for the sixth semester.

Basic requirements in category knowledge: Knowledge of the basic organic chemistry as well as basic technological operations.

Basic requirements in category skills: Ability to perform simple chemical calculations (e.g. stoichiometric calculations, mass balance), as well as basic laboratory operations.

Basic requirements in category social competences: Awareness of the need to work individually and in teams of 2-3 people.

Module outcomes

MEK	The student who completed the module	Types of classes / teaching methods leading to achieving a given outcome of teaching	Methods of verifying every mentioned outcome of teaching	Relationships with KEK	Relationships with PRK
01	Student has basic knowledge of the methods production of the most important organic chemicals.	lecture	written exam	K_W08+++	P6S_WG
02	Student has general knowledge of the prospective methods of production of the most important organic chemicals.	lecture	written exam	K_W11+	P6S_WG
03	Student knows the basic intermidies for production of the most important organic chemicals.	lecture	written exam	K_W08++	P6S_WG
04	Student is able to make a simple analysis of technological solutions for manufacturing the basic organic chemicals.	lecture	written exam	K_U17+++	P6S_UW
05	Student is able to put together a simple glassware set for synthesis of organic compounds and apply basic laboratory techniques.	laboratory	observation of performance	K_U10++	P6S_UW
06	Student is able to control syntheses of the selected organic chemicals, perform balance calculations, draw correct conclusions and prepare the final reports.	laboratory	written report
07	Student obeys rules of the fire protection and safety, in particular, the use of protective clothing and conducting with toxic, corrosive and inflammable chemicals.	laboratory	observation of performance	K_U14+	P6S_UW
08	Student knows and applies principles of the proper management of waste. He segregate chemical waste (solid and liquid) from synthesis of organic chemicals.	laboratory	observation of performance	K_U15+	P6S_UW
09	Student is able to perform basic analysis of the organic products provided in performed syntheses.	laboratory	written report	K_U17+	P6S_UW
10	Student is able to work in a team performing syntheses of the selected organic chemicals in a laboratory scale.	laboratory	observation of performance	K_K03++	P6S_KR
11	Student is able to point the main directions of application of the basic organic chemicals.	lecture, laboratory	written exam	K_U19+	P6S_UW

Attention: Depending on the epidemic situation, verification of the achieved learning outcomes specified in the study program, in particular credits and examinations at the end of specific classes, can be implemented remotely (real-time meetings).

The syllabus of the module

Sem.	TK	The content	realized in	MEK
6	TK01	Synthesis involving carbon monoxide. Preparation of methanol, acetic acid, oxo aldehydes. Fischer-Tropsch synthesis	W01-W02	MEK01 MEK02 MEK03
6	TK02	Halogenation processes. Production of chloromethanes, vinyl chloride and chlorobenzene as well as propylene oxide and epichlorohydrin by chlorine methods.	W03-W04	MEK01 MEK02 MEK03 MEK04
6	TK03	Alkylation processes. Production of ethylbenzene and cumene, and N, O, S and Al alkylation products.	W05	MEK01 MEK02 MEK03
6	TK04	Hydrogenation and dehydrogenation. Production of formaldehyde, styrene, cyclohexane, aniline, diaminebenzene and toluenediamine.	W06-W07	MEK01 MEK02 MEK03
6	TK05	Oxidation. Production of ethylene and propylene oxides, adipic and terephthalic acids, phthalic and maleic anhydrides, phenol and acetone as well as hydrogen peroxide.	W08-W11	MEK01 MEK02 MEK03
6	TK06	Addition and condensation processes. Preparation of Bisphenol A.	W12	MEK01 MEK02 MEK03
6	TK07	Hydration and esterification. Production of ethanol and ethylene oxide, esters of acetic and phthalic acids.	W13	MEK01 MEK02 MEK03
6	TK08	Nitration processes. Preparation nitrobenzene, dinitrobenzene and dinitrotoluene toluene.	W14	MEK01 MEK02 MEK03
6	TK09	Sulfonation processes	W15	MEK01 MEK02 MEK03
6	TK10	Syntheses of the selected organic chemicals, e.g. cyclohexanone oxime and caprolactam, adipic acid, dibutyl phthalate, methacrylate.	L01-L10	MEK05 MEK06 MEK07 MEK08 MEK09 MEK10 MEK11

The student's effort

The type of classes	The work before classes	The participation in classes	The work after classes
Lecture (sem. 6)		contact hours: 30.00 hours/sem.	Studying the recommended bibliography: 4.50 hours/sem.
Laboratory (sem. 6)	The preparation for a Laboratory: 3.00 hours/sem. The preparation for a test: 8.00 hours/sem.	contact hours: 60.00 hours/sem.	Finishing/Making the report: 8.00 hours/sem.
Advice (sem. 6)
Exam (sem. 6)	The preparation for an Exam: 35.00 hours/sem.	The written exam: 1.00 hours/sem.

The way of giving the component module grades and the final grade

The type of classes	The way of giving the final grade
Lecture	Positive mark of the written exam. The grading scale is given during an exam. The 2nd exam with 0.9 coeficient.
Laboratory	Passed all practical tasks, final reports and theoretical tests.
The final grade	The final grade (K): K = 0.6wE + 0.4L: where E, L - positive grade of the exam and laboratory, respectively w – a coefficient, w = 1.0 for the first exam, 0.9 for the second exam

Sample problems

Required during the exam/when receiving the credit
(-)

Realized during classes/laboratories/projects
(-)

Others
(-)

Can a student use any teaching aids during the exam/when receiving the credit : no

The contents of the module are associated with the research profile: no