The aim of studying and bibliography

The main aim of study: Introduction with principles and methods applied during sampling and sample storage.

The general information about the module: Classification of analytical methods. Stages of the analysis process. Sampling procedure. Sampling errors. Sample types. Influence of physicochemical properties of materials on their sampling. Sampling solid, liquid and gas materials. Characterization of sampling equipment. Essential stage of sample preparation: preservation, transport, storage and handling conditions. Method of isolations and enrichment of analytes.

Teaching materials: Materiały można pobrać ze strony domowej koordynatora modułu

Bibliography required to complete the module

Bibliography used during lectures

1	J. Namieśnik, J. Łukasiak, Z. Jamrogiewicz,	Pobieranie próbek środowiskowych do analizy	PWN, Warszawa .	1995
2	J. Namieśnik, Z. Jamrogiewicz, M. Pilarczyk, L. Torres	Przygotowanie próbek środowiskowych do analizy	WNT, Warszawa.	2000
3	J. Siepak	Metody pobierania i przygotowania próbek wód, ścieków i osadów do analiz fizykochemicznych	Zakład Graficzny UAM, Poznań.	1997

Bibliography used during classes/laboratories/others

1	PN-ISO 10381-1	Jakość gleby. Pobieranie próbek. Część 1: Zasady dotyczące opracowania programów pobierania próbek	.
2	PN-ISO 10381-2	Jakość gleby. Pobieranie próbek. Część 2: Zasady dotyczące techniki pobierania	.
3	PN-ISO 10381-3	Jakość gleby. Pobieranie próbek. Część 3: Zasady dotyczące bezpieczeństwa	.
4	PN-EN 5667-1:2008 część 1	Jakość wody. Pobieranie próbek. Część 1 – Wytyczne dotyczące opracowania programów pobierania próbek	.
5	PN-EN 5667-3:2005	Jakość wody. Pobieranie próbek. Wytyczne dotyczące utrwalania i postępowania z próbkami	.
6	PN-EN ISO 5667-5:2003	Jakość wody. Pobieranie próbek. Wytyczne dotyczące pobierania próbek wody do picia i wody używanej d	.
7	PN-EN 5667-18:2004	Wytyczne dotyczące pobierania wód podziemnych w miejscach zanieczyszczonych	.
8	Praca zbiorowa	Ćwiczenia Laboratoryjne z Analizy Zanieczyszczeń Powietrza	UAM, Poznań.	2008

Basic requirements in category knowledge/skills/social competences

Formal requirements: Passed module : analytical chemistry.

Basic requirements in category knowledge: Student should possess basic knowledge of analytical chemistry and instrumental analysis.

Basic requirements in category skills: Manual skills necessary to execution of chemical analyses.

Basic requirements in category social competences: Knowledge of basic in health and safety-at-work legislation and fire regulations currently in force in chemical laboratory. Awareness of harmful influence of chemicals on human body and the environmen

Module outcomes

MEK	The student who completed the module	Types of classes / teaching methods leading to achieving a given outcome of teaching	Methods of verifying every mentioned outcome of teaching	Relationships with KEK	Relationships with PRK
01	He has knowledge of the classification of analytical methods, stages of the analysis process.	lecture	oral presentation	K_W03++	P6S_WG
02	He knows how sampling and sample preparation influences on the analysis.	lecture	oral presentation	K_W04+++	P6S_WG
03	He knows the general principles of sampling of solid, liquid and gas. and the influence of changeable properties on the sampling process.	lecture	oral presentation	K_W04+++	P6S_WG
04	He knows the basic characteristics of samplers.	lecture, laboratory	written test, observation of performance, a written report	K_W04++	P6S_WG
05	He knows the basic characteristics of samplers.	lecture, laboratory	written test, observation of performance	K_K03++	P6S_KR
06	Student can analyze a simple analytical problems and find their solutions based on known methods and literature data.	lecture, laboratory	written test and report	K_U01++	P6S_UW

Attention: Depending on the epidemic situation, verification of the achieved learning outcomes specified in the study program, in particular credits and examinations at the end of specific classes, can be implemented remotely (real-time meetings).

The syllabus of the module

Sem.	TK	The content	realized in	MEK
5	TK01	Classification of analytical methods. Stages of the analysis process. Sampling procedure. Sampling errors. Sample types. Influence of physicochemical properties of materials on their sampling. Sampling solid, liquid and gas materials. Characterization of sampling equipment. Essential stage of sample preparation: preservation, transport, storage and handling conditions. Method of isolations and enrichment of analytes.	wykład	MEK01 MEK02 MEK03 MEK04 MEK05
5	TK02	Sampling and preservation of water. Preparation of analytical sample.	L01	MEK02 MEK06
5	TK03	Sampling air . Preparation of analytical sample.	L02	MEK02 MEK04
5	TK04	Sampling soil. Preparation of analytical sample.	L03	MEK02 MEK03

The student's effort

The type of classes	The work before classes	The participation in classes	The work after classes
Lecture (sem. 5)		contact hours: 15.00 hours/sem.	Studying the recommended bibliography: 5.00 hours/sem.
Laboratory (sem. 5)		contact hours: 15.00 hours/sem.
Advice (sem. 5)
Credit (sem. 5)	The preparation for a Credit: 15.00 hours/sem.	The written credit: 2.00 hours/sem.

The way of giving the component module grades and the final grade

The type of classes	The way of giving the final grade
Lecture
Laboratory
The final grade	Final grade OK = 0,5 wOW + 0,5wOL Where:OW and OL - positive evaluation of the lecture and lab; w - factor related to the time of credit or examination, w= 1.0 first term, w = 0.9 second term , w = 0.8 third term. The grade is rounded according to WKZJK

Sample problems

Required during the exam/when receiving the credit
(-)

Realized during classes/laboratories/projects
(-)

Others
(-)

Can a student use any teaching aids during the exam/when receiving the credit : no

The contents of the module are associated with the research profile: yes

1	B. Guratowska; A. Kuźniar; J. Nizioł; A. Nowak; M. Okrasa; T. Ruman; M. Ryngajłło; J. Szulc	Uncontrolled Post-Industrial Landfill—Source of Metals, Potential Toxic Compounds, Dust, and Pathogens in Environment—A Case Study	2024
2	J. Kalembkiewicz; A. Kuźniar; B. Papciak; E. Sočo	Zastosowanie materiału krzemionkowego modyfikowanego surfaktantem do immobilizacji moryny	2023
3	S. Kuberski; A. Kuźniar; J. Nizioł; A. Nowak; I. Nowak; M. Okrasa; T. Ruman; B. Szponar; J. Szulc	Biological and chemical contamination of illegal, uncontrolled refuse storage areas in Poland	2023
4	Ł. Byczyński; M. Huta; A. Kuźniar; E. Sočo	Badania produktów sulfonowania kwercetyny	2023
5	M. Dranka; J. Kalembkiewicz; D. Kamiński; A. Kozioł; A. Kuźniar; U. Maciołek; L. Mazur; E. Mendyk	Structural and spectroscopic studies of Na+ – Quercetin-5′-sulfonic acid polymeric complexes obtained via solvothermal synthesis	2022
6	A. Hałoń; D. Ksiądzyna; A. Kuźniar; A. Matuszewska; A. Merwid-Ląd; B. Nowak; T. Sozański; M. Szandruk-Bender; A. Szeląg; D. Szkudlarek; M. Trocha	Morin-5′-Sulfonic Acid Sodium Salt (NaMSA) Attenuates Cyclophosphamide-Induced Histological Changes in Genitourinary Tract in Rats—Short Report	2021
7	A. Kuźniar; U. Maciołek; E. Pieniążek; J. Pusz; E. Sočo; E. Woźnicka	Związek kwasu kwercetyno-5’-sulfonowego z jonami sodu. Synteza, właściwości, zastosowanie	2021
8	E. Ciszkowicz; M. Kosińska-Pezda; A. Kuźniar; K. Lecka-Szlachta; E. Pieniążek; E. Woźnicka; L. Zapała	Synteza, charakterystyka i właściwości biologiczne kompleksów jonów antanowców lekkich z 3-hydroksyflawonem	2021
9	A. Czerwonka; J. Kafałut; A. Kuźniar; U. Maciołek; E. Mendyk; W. Rzeski	Anticancer effects of sodium and potassium quercetin-5’-sulfonates through inhibition of proliferation, induction of apoptosis, and cell cycle arrest in the HT-29 human adenocarcinoma cell line	2020
10	J. Kalembkiewicz; A. Kuźniar; B. Papciak; J. Pusz; E. Sitarz-Palczak; E. Sočo; E. Woźnicka	Pierwiastki i związki chemiczne	2020
11	J. Kalembkiewicz; A. Kuźniar; E. Pieniążek; E. Sočo; E. Woźnicka	Aktywność biochemiczna sulfonowych pochodnych moryny	2020
12	M. Kopacz; A. Kuźniar; B. Papciak; J. Pusz; E. Woźnicka	Badania reakcji kompleksowania chryzyny z jonami Nd(III), Tb(III) i Dy(III) w roztworach wodno-metanolowych	2020