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Industrial waste and their analysis

Some basic information about the module

Cycle of education: 2022/2023

The name of the faculty organization unit: The faculty Chemistry

The name of the field of study: Chemical Technology

The area of study: technical sciences

The profile of studing:

The level of study: first degree study

Type of study: full time

discipline specialities : Chemical analysis in industry and environment, Chemical and bioprocess engineering, Organic and polymer technology

The degree after graduating from university: Bachelor of Science (BSc)

The name of the module department : Department of Inorganic and Analytical Chemistry

The code of the module: 190

The module status: mandatory for the speciality Chemical analysis in industry and environment

The position in the studies teaching programme: sem: 6 / W15 C15 L40 / 6 ECTS / E

The language of the lecture: Polish

The name of the coordinator 1: Prof. Jan Kalembkiewicz, DSc, PhD, Eng.

office hours of the coordinator: jk.v.prz.edu.pl sem zimowy: pn 12.15-13.45, wt 12.15-13.45, sem. letni: pn 9.45-11.15, wt 12.00-13.30

The name of the coordinator 2: Anna Kuźniar, PhD, Eng.

The aim of studying and bibliography

The main aim of study: The student should obtain most recent knowledge about industrial wastes; ability in calculations and conversion contaminations content. The student is required to perform appropriate analytical method according to chemical analysis of wastes.

The general information about the module: Module in semester 5 as a lecture, accounting exercises and laboratory

Teaching materials: Dostępne na stronie domowej: jk.v.prz.edu.pl; OPA, Kalembkiewicz J., Odpady przemysłowe i ich analiza. Ćwiczenia rachunkowe

Bibliography required to complete the module
Bibliography used during lectures
1 J. Pyssa Odpady przemysłowe i niebezpieczne w gospodarce obiegu zamkniętego Wydawnictwa AGH, Kraków. 2019
2 PZIITS Odpady chemiczne i naftowe. Odpady niebezpieczne Wydawnictwo PZIITS, Poznań . 2001
3 Rosik-Dulewska Cz. Podstawy gospodarki odpadami Wydaw.Nauk.PWN, Warszawa. 2015
4 Namieśnik J., Jamrógiewicz Z. Fizykochemiczne metody kontroli zanieczyszczeń środowiska WNT Warszawa. 1998
5 Brenda Bryant and Betty Hall Municipal and Industrial Waste: Sources, Management Practices and Future Challenges Nova Science Publishers, Inc. New York . 2018
Bibliography used during classes/laboratories/others
1 J. Minczewski, Z. Marczenko Chemia analityczna. T. 2, Chemiczne metody analizy ilościowej PWN, Warszawa. 2012
2 Danzer K., Than E., Molch D., Küchler L. Analityka. Przegląd systematyczny WNT Warszawa. 1993
3 P. Konieczka, J. Namieśnik (red.) Ocena i kontrola jakości wyników pomiarów analitycznych: praca zbiorowa WNT Warszawa. 2009
4 J. Namieśnik, Z. Jamrógiewicz Fizykochemiczne metody kontroli zanieczyszczeń środowiska WNT, Warszawa. 2000
5 Marczenko Z., Balcerzak M. Spektrofotometryczne metody w analizie nieorganicznej PWN Warszawa. 1998

Basic requirements in category knowledge/skills/social competences

Formal requirements: Registration for the semester

Basic requirements in category knowledge: Knowledge of chemistry and analytical chemistry at the basic level

Basic requirements in category skills: The ability to search and interpret the data, perform an experiment and calculations

Basic requirements in category social competences: The ability to cooperate and work in a group

Module outcomes

MEK The student who completed the module Types of classes / teaching methods leading to achieving a given outcome of teaching Methods of verifying every mentioned outcome of teaching Relationships with KEK Relationships with PRK
01 Has basic knowledge of industrial waste, sources of their formation, properties, composition and classification and methods of analysis. lecture written exam K_W08++
K_K02+++
P6S_KO
P6S_KR
P6S_WG
02 Has the ability to perform chemical analyzes of industrial waste. laboratory written test practical test K_U11++
K_U21+++
K_K01+++
P6S_KK
P6S_KO
P6S_KR
P6S_UO
P6S_UW
03 Has the ability to calculate the content of macro and micronutrients in industrial waste. calculations written test K_U21++
P6S_UW

Attention: Depending on the epidemic situation, verification of the achieved learning outcomes specified in the study program, in particular credits and examinations at the end of specific classes, can be implemented remotely (real-time meetings).

The syllabus of the module

Sem. TK The content realized in MEK
6 TK01 Waste classification: nontoxic, hazardous and special wastes. Solid industrial wastes. Sewage and sediments. Air pollution by gases and dusts. Inorganic and organic industrial wastes, others industrial wastes. Composition analysis of wastes. Tests methods of wastes physical chemistry. Contaminants monitoring in wastes and their neutralization products. W15 MEK01
6 TK02 Contaminants in solid wastes. Scheme analysis and calculations. Contaminants in greasy and liquid wastes. Contaminants in greasy and liquid wastes. Sequence extraction in waste physical chemistry examination. Mass balance of analyte in multistage analysis. Mobility evaluation of metals in solid industrial wastes. C15 MEK03
6 TK03 Determination of selected metals and sulfur refuse from furnace. Determination of sulfate and chloride in galvanic sediments. Determination of silica and iron in ceramic wastes. Analysis of selected components in sludge after gum vulcanization. Analysis of inorganic anions in liquid industrial wastes. L40 MEK02

The student's effort

The type of classes The work before classes The participation in classes The work after classes
Lecture (sem. 6) contact hours: 15.00 hours/sem.
Studying the recommended bibliography: 15.00 hours/sem.
Class (sem. 6) The preparation for a test: 15.00 hours/sem.
contact hours: 15.00 hours/sem.
Finishing/Studying tasks: 15.00 hours/sem.
Laboratory (sem. 6) The preparation for a test: 15.00 hours/sem.
contact hours: 40.00 hours/sem.
Finishing/Making the report: 15.00 hours/sem.
Advice (sem. 6) The participation in Advice: 2.00 hours/sem.
Exam (sem. 6) The preparation for an Exam: 15.00 hours/sem.
The written exam: 2.00 hours/sem.

The way of giving the component module grades and the final grade

The type of classes The way of giving the final grade
Lecture Positive mark on written exam (mark E); the student is required to pass the test on calculation exercises (C) before the exam and laboratory exercises. The final mark is rounded according to WKZJK.
Class C: the final mark is averaged mark of two written tests (mark C). The final mark is rounded according to WKZJK.
Laboratory L: the final mark is averaged mark of all experiments performed, current written tests and final test (mark L). The final mark is rounded according to WKZJK.
The final grade Final mark in the module (FM): FM = 0.2 w C + 0.3 w L + 0.5 w E; where: C, L, E denote respectively positive mark in seminar (calculation exercises), laboratory and examination. w- coefficient for examination resits, w=1.0 for a regular examination, w=0.9 for a first resit, w=0.8 for a second resit. The final mark is rounded according to WKZJK.

Sample problems

Required during the exam/when receiving the credit
(-)

Realized during classes/laboratories/projects
(-)

Others
(-)

Can a student use any teaching aids during the exam/when receiving the credit : no

The contents of the module are associated with the research profile: yes

1 B. Guratowska; A. Kuźniar; J. Nizioł; A. Nowak; M. Okrasa; T. Ruman; M. Ryngajłło; J. Szulc Uncontrolled Post-Industrial Landfill—Source of Metals, Potential Toxic Compounds, Dust, and Pathogens in Environment—A Case Study 2024
2 J. Kalembkiewicz; A. Kuźniar; B. Papciak; E. Sočo Zastosowanie materiału krzemionkowego modyfikowanego surfaktantem do immobilizacji moryny 2023
3 J. Kalembkiewicz; M. Kopacz; J. Pusz Współczesne metody badań i zastosowań flawonoidów: praca zbiorowa 2023
4 S. Kuberski; A. Kuźniar; J. Nizioł; A. Nowak; I. Nowak; M. Okrasa; T. Ruman; B. Szponar; J. Szulc Biological and chemical contamination of illegal, uncontrolled refuse storage areas in Poland 2023
5 Ł. Byczyński; M. Huta; A. Kuźniar; E. Sočo Badania produktów sulfonowania kwercetyny 2023
6 D. Galas; J. Kalembkiewicz; E. Sitarz-Palczak Study of the Adsorption of Cu(II), Mn(II), Pb(II), and Zn(II) Ions on Geopolymers Obtained from Ashes from Biomass Combustion 2022
7 J. Kalembkiewicz; E. Pieniążek; J. Pusz; E. Sitarz-Palczak; E. Sočo Badania właściwości kwercetyny i jej sulfonowych pochodnych w układach z fluoroforem 2022
8 J. Kalembkiewicz; M. Kopacz; J. Pusz Flawonoidy i ich pochodne w badaniach naukowych i praktyce 2022
9 M. Dranka; J. Kalembkiewicz; D. Kamiński; A. Kozioł; A. Kuźniar; U. Maciołek; L. Mazur; E. Mendyk Structural and spectroscopic studies of Na+ – Quercetin-5′-sulfonic acid polymeric complexes obtained via solvothermal synthesis 2022
10 A. Hałoń; D. Ksiądzyna; A. Kuźniar; A. Matuszewska; A. Merwid-Ląd; B. Nowak; T. Sozański; M. Szandruk-Bender; A. Szeląg; D. Szkudlarek; M. Trocha Morin-5′-Sulfonic Acid Sodium Salt (NaMSA) Attenuates Cyclophosphamide-Induced Histological Changes in Genitourinary Tract in Rats—Short Report 2021
11 A. Kuźniar; U. Maciołek; E. Pieniążek; J. Pusz; E. Sočo; E. Woźnicka Związek kwasu kwercetyno-5’-sulfonowego z jonami sodu. Synteza, właściwości, zastosowanie 2021
12 E. Ciszkowicz; M. Kosińska-Pezda; A. Kuźniar; K. Lecka-Szlachta; E. Pieniążek; E. Woźnicka; L. Zapała Synteza, charakterystyka i właściwości biologiczne kompleksów jonów antanowców lekkich z 3-hydroksyflawonem 2021
13 J. Kalembkiewicz; B. Papciak; E. Pieniążek; E. Sočo Stałe związki kompleksowe jonów tytanu(IV) z sulfonową pochodną moryny 2021
14 J. Kalembkiewicz; E. Pieniążek; E. Sočo Adsorpcja flawonoidów na uporządkowanych mezoporowych materiałach krzemionkowych 2021
15 J. Kalembkiewicz; E. Sitarz-Palczak Application of halloysite geopolymers to removal of methyl blue from aqueous solution 2021
16 J. Kalembkiewicz; E. Sitarz-Palczak The Influence of Physical Modification on the Sorption Properties of Geopolymers Obtained from Halloysite 2021
17 J. Kalembkiewicz; M. Kopacz; J. Pusz Badania naukowe i aplikacyjne flawonoidów 2021
18 J. Kalembkiewicz; M. Kopacz; J. Pusz Nauka i praktyka w świecie flawonoidów 2021
19 J. Kalembkiewicz; M. Kosińska-Pezda; J. Pusz; E. Woźnicka; L. Zapała Badania równowagi reakcji kompleksowania chryzyny z jonami Er(III) w układach: woda - metanol i woda - metanol - 1,4-dioksan 2021
20 A. Czerwonka; J. Kafałut; A. Kuźniar; U. Maciołek; E. Mendyk; W. Rzeski Anticancer effects of sodium and potassium quercetin-5’-sulfonates through inhibition of proliferation, induction of apoptosis, and cell cycle arrest in the HT-29 human adenocarcinoma cell line 2020
21 J. Kalembkiewicz Surowce i produkty nieorganiczne 2020
22 J. Kalembkiewicz Uzupełnienia 2020
23 J. Kalembkiewicz; A. Kuźniar; B. Papciak; J. Pusz; E. Sitarz-Palczak; E. Sočo; E. Woźnicka Pierwiastki i związki chemiczne 2020
24 J. Kalembkiewicz; A. Kuźniar; E. Pieniążek; E. Sočo; E. Woźnicka Aktywność biochemiczna sulfonowych pochodnych moryny 2020
25 J. Kalembkiewicz; B. Papciak Chemia ogólna i nieorganiczna. Pierwiastki i związki chemiczne. Surowce i produkty nieorganiczne: obliczenia chemiczne i problemy 2020
26 J. Kalembkiewicz; B. Papciak Chemia ogólna i nieorganiczna. Podstawy chemii. Roztwory i procesy w roztworach: obliczenia chemiczne i problemy 2020
27 J. Kalembkiewicz; B. Papciak Uzupełnienia 2020
28 J. Kalembkiewicz; B. Papciak; E. Pieniążek; J. Pusz; P. Skitał; E. Sočo; L. Zapała Podstawy chemii 2020
29 J. Kalembkiewicz; B. Papciak; J. Pusz; E. Sitarz-Palczak; E. Woźnicka Roztwory i procesy w roztworach 2020
30 J. Kalembkiewicz; D. Pająk; E. Sočo Multi-component sorption and utilization of solid waste to simultaneous removing basic dye and heavy metal from aqueous system 2020
31 J. Kalembkiewicz; E. Sočo Characterisation and utilisation of solid waste from coal combustion to modelling of sorption equilibrium in a bi-component system metal-dye 2020
32 J. Kalembkiewicz; E. Sočo Immobilizing and Removal of Cadmium and Rhodamine B from an Aqueous System by Converting Solid Waste from Poland; Studies of Equilibrium and Kinetic Sorption 2020
33 J. Kalembkiewicz; M. Kopacz; J. Pusz Świat flawonoidów w badaniach naukowych 2020
34 J. Kalembkiewicz; R. Rawski; P. Sanecki Units and Methods of Proteolytic Activity Determination 2020
35 M. Kopacz; A. Kuźniar; B. Papciak; J. Pusz; E. Woźnicka Badania reakcji kompleksowania chryzyny z jonami Nd(III), Tb(III) i Dy(III) w roztworach wodno-metanolowych 2020
36 D. Galas; J. Kalembkiewicz; E. Sitarz-Palczak Comparative study on the characteristics of coal fly ash and biomass ash geopolymers 2019
37 D. Galas; J. Kalembkiewicz; E. Sitarz-Palczak Study of potential availability of heavy metals to phytoremediation to use of ash from biomass combustion 2019
38 J. Kalembkiewicz; D. Saletnik; P. Sanecki; P. Skitał Electrodeposition of nickel from alkaline NH4OH/NH4Cl buffer solutions 2019
39 J. Kalembkiewicz; E. Sočo Enhanced sorption capacity of a metal-dye system from water effluents by using activated industrial waste 2019