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Environmental analysis

Some basic information about the module

Cycle of education: 2022/2023

The name of the faculty organization unit: The faculty Chemistry

The name of the field of study: Chemical Technology

The area of study: technical sciences

The profile of studing:

The level of study: first degree study

Type of study: full time

discipline specialities : Chemical analysis in industry and environment, Chemical and bioprocess engineering, Organic and polymer technology

The degree after graduating from university: Bachelor of Science (BSc)

The name of the module department : Department of Inorganic and Analytical Chemistry

The code of the module: 168

The module status: mandatory for the speciality Chemical analysis in industry and environment

The position in the studies teaching programme: sem: 6 / W15 L30 / 4 ECTS / Z

The language of the lecture: Polish

The name of the coordinator 1: Janusz Pusz, PhD

office hours of the coordinator: Wtorek: 14.00-15.30 Czwartek: 13.00-14.30

The name of the coordinator 2: Elżbieta Woźnicka, PhD

The name of the coordinator 3: Lidia Zapała, PhD, Eng.

semester 6: Bogdan Papciak, PhD, Eng. , office hours Tuesdays, at. 8:15-9:00 a. m. Wednesdays, at. 3:00-3:45 p. m. Thursdays, at. 12:30-14:00

The aim of studying and bibliography

The main aim of study: Introduction of the students with harmful, burdensome and dangerous factors occuring in the working environment.

The general information about the module: Introduction to problems with safety and the protection man health in the working environment. The profile of dangerous chemical substances. Opinion of the danger of the work with toxic substances. The acustic noises. Lighting. Pollunation and the toxicology of the air. Personal protective equipment. Application of the statistics methods for the evaluation measurements results for the diffrent concentrations of the toxic substances.

Teaching materials: Instrukcje do ćwiczeń laboratoryjnych.

others: Materiały pomocnicze do wykładu i laboratoriów udostępniane na stronie internetowej koordynatora.

Bibliography required to complete the module
Bibliography used during lectures
1 Hansen A. Kompleksowa ocena poziomu bezpieczeństwa i higieny pracy Inst. Wyd.Zw Zawodowych Warszawa. 1983
2 Zakrzewski Sigmund F. Podstawy toksykologii środowiska PWN, Warszawa . 1997
3 Augustyńska D., Zawieski W. Ochrona przed hałasem i drganiami w środowisku pracy CIOP, Warszawa . 1999
4 Wolska A., Pawlak A. Oświetlenie pomieszczeń i stanowisk pracy CIOP, Warszawa . 1998
5 Puzyna Cz. Fizjologia i higiena pracy: „Hałas w przemyśle” Inst.Wyd.CRZZ,Warszawa. 1997
Bibliography used during classes/laboratories/others
1 Norma PN-84,Z-4008/02 (Ochrona czystości powietrza. Pobieranie próbek), Wytyczne ogólne .
2 Norma PN-89,Z-04008/07. Zasady pobierania próbek powietrza w śr.pracy i interpretacja wyników .
3 Norma PN-Z-04008-7. Zasady pobierania próbek powietrza w środowisku pracy i interpretacja wyników .
4 PN-ISO6879:2000: Jakość powietrza .
5 PN-EN 689 Powietrze na stanowiskach pracy. Wytyczne oceny narażenia inhalacyjnego na czynniki chem .

Basic requirements in category knowledge/skills/social competences

Formal requirements: Registration for the given semester.

Basic requirements in category knowledge: Basic knowledge from analytic chemistry, physics and physical chemistry.

Basic requirements in category skills: Practical and manual skills necessary for executing laboratory experiments. Theu use of basic laboratory equipment with the valid principles of BHP and PPOŻ

Basic requirements in category social competences: The abbility to work in the group.

Module outcomes

MEK The student who completed the module Types of classes / teaching methods leading to achieving a given outcome of teaching Methods of verifying every mentioned outcome of teaching Relationships with KEK Relationships with PRK
01 After learning of materials, students should know the basic definations regarding of the lighting technique and to characterize the basic abbility and the kinds of lighting. lecture the written test K_U02++
K_K01++
P6S_KK
P6S_KO
P6S_KR
P6S_UK
02 The student should have a basic knowledge about the dangerous of the acustic noise, influence on the organism and his results, the methods of measurement and their abbility to evaluation and ways of prevention. lecture the written test K_W06++
P6S_WG
03 Student should know recognize the sources of the emission of dusts, show kinds and properties of the most harmful dusts occuring in the environment of the work, to know the basic parameters of dusts, essential due to of their harmful influance on the human organism. lecture the written test K_W06++
K_U02++
K_U13++
P6S_UK
P6S_UW
P6S_WG
04 Student should know the conceptions of the highest admissible concentrations and the intensities of harmful factors and the principle their using to the estimation of the conditions of the work. lecture the written test K_W06++
K_K02++
P6S_KO
P6S_KR
P6S_WG
05 Student should know general principles and the methods of prepartion the samples of the air to the estimation of the concentrations of toxic substances in the environment of the work. lecture the written test K_W06++
K_U13++
P6S_UW
P6S_WG
06 The student obtaine the practical skill to perform the some examples of the experimental estimation for chemical and physical harmful and burdensome factors for the health in the environment of the work. laboratory the written test, the written reaport

Attention: Depending on the epidemic situation, verification of the achieved learning outcomes specified in the study program, in particular credits and examinations at the end of specific classes, can be implemented remotely (real-time meetings).

The syllabus of the module

Sem. TK The content realized in MEK
6 TK01 The acustic noise – measurement and the interpretation of results. The measurement of intensity and the equableness of the lighting of the position of the work – opinion, the interpretation of results. Estimating the concentration of dusts hung in the air of the place of the work - measurement, the interpretation of results. Determination of the concentration of toxic gas components in the air (O3, NH3, HCl, NO2) Laboratorium MEK06
6 TK02 Introduction to problems with safety and the protection man health in the working environment. The profile of dangerous chemical substances. Opinion of the danger of the work with toxic substances. The acustic noises. Lighting. Pollunation and the toxicology of the air. Personal protective equipment. Application of the statistics methods for the evaluation measurements results for the diffrent concentrations of the toxic substances. Wykład MEK01 MEK02 MEK03 MEK04 MEK05

The student's effort

The type of classes The work before classes The participation in classes The work after classes
Lecture (sem. 6) contact hours: 15.00 hours/sem.
complementing/reading through notes: 5.00 hours/sem.
Studying the recommended bibliography: 5.00 hours/sem.
Laboratory (sem. 6) The preparation for a Laboratory: 2.00 hours/sem.
The preparation for a test: 10.00 hours/sem.
contact hours: 30.00 hours/sem.
Finishing/Making the report: 5.00 hours/sem.
Advice (sem. 6) The participation in Advice: 7.00 hours/sem.
Credit (sem. 6) The preparation for a Credit: 10.00 hours/sem.
The written credit: 1.00 hours/sem.

The way of giving the component module grades and the final grade

The type of classes The way of giving the final grade
Lecture Obtainment of the positive score from the test (OW). The grade of test depends on the amount of points : 3,0 (60,0 %-68,0%); 3,5 (68,1%-76,0%); 4,0 (76,1%-84,0%); 4,5 (84,1%-92,0%); 5,0 (92,1%-100%).
Laboratory The subject is passed based on all performed experiments, reports and two written tests. The final score from the laboratory (OL) is average arithmetical scores from tests.
The final grade The final score from the object (OK) is counted according to the example OK = 0,5wOW + 0,5wOL; where w-factor related w=1,0 (first term), w=0,9 (second term), w=0,8 (third term). The grade is rounded according to WKZJK.

Sample problems

Required during the exam/when receiving the credit
Pytania kontrolne.PDF

Realized during classes/laboratories/projects
Pomiary hałasu-lab.pdf
Pomiary oświetlenia-lab.pdf
OZNACZANIE ZAWARTOŚCI AMONIAKU.pdf
Oznaczanie tlenków azotu w powietrzu.pdf

Others
(-)

Can a student use any teaching aids during the exam/when receiving the credit : no

The contents of the module are associated with the research profile: yes

1 J. Kalembkiewicz; M. Kopacz; J. Pusz Współczesne metody badań i zastosowań flawonoidów: praca zbiorowa 2023
2 M. Kosińska-Pezda; U. Maciołek; L. Zapała Synthesis, Spectral Characterization and Potential Fluorescent Properties of Three Lanthanide(III) Ions Complexes with Nalidixic Acid 2023
3 Ł. Byczyński; M. Kosińska-Pezda; E. Woźnicka; L. Zapała; W. Zapała Synteza oraz badania składu i właściwości związków: 3-hydroksyflawonu, chryzyny oraz sulfonowych pochodnych chryzyny i kwercetyny z jonami Mn(II) 2023
4 Ł. Byczyński; M. Kosińska-Pezda; U. Maciołek; L. Zapała Study of the thermal behavior, evolved gas analysis and temperature diffraction patterns of new light lanthanide complexes with niflumic acid 2023
5 E. Ciszkowicz; M. Kosińska-Pezda; K. Lecka-Szlachta; A. Miłoś; E. Woźnicka; L. Zapała Analiza właściwości antybakteryjnych oraz cytotoksyczności kompleksów jonów Co(II), Mn(II) oraz Zn(II) z chryzyną oraz 3-hydroksyflawonem 2022
6 J. Kalembkiewicz; E. Pieniążek; J. Pusz; E. Sitarz-Palczak; E. Sočo Badania właściwości kwercetyny i jej sulfonowych pochodnych w układach z fluoroforem 2022
7 J. Kalembkiewicz; M. Kopacz; J. Pusz Flawonoidy i ich pochodne w badaniach naukowych i praktyce 2022
8 L. Zapała; W. Zapała; P. Ziobrowski Studies on the retention behavior of quercetin, phenol and caffeine as test substances on selected neutral and charged Hydrophilic Interaction Liquid Chromatography stationary phases 2022
9 M. Drewniak; M. Kosińska-Pezda; U. Maciołek; A. Nowicka; L. Zapała Synteza i charakterystyka spektroskopowa kompleksu kwasu nalidyksowego z jonami samaru(III) 2022
10 M. Kosińska-Pezda; E. Woźnicka; L. Zapała Synteza i charakterystyka spektroskopowa kompleksów jonów lantanowców ciężkich z 3-hydroksyflawonem 2022
11 M. Kosińska-Pezda; U. Maciołek; E. Woźnicka; L. Zapała Kompleksy 3-hydroksyflawonu z jonami Zn(II) - synteza i właściwości związków 2022
12 M. Kosińska-Pezda; U. Maciołek; E. Woźnicka; L. Zapała; W. Zapała Synteza, badania składu i właściwości spektroskopowych kompleksów wybranych jonów metali przejściowych z kwasem niflumowym 2022
13 A. Kuźniar; U. Maciołek; E. Pieniążek; J. Pusz; E. Sočo; E. Woźnicka Związek kwasu kwercetyno-5’-sulfonowego z jonami sodu. Synteza, właściwości, zastosowanie 2021
14 E. Ciszkowicz; K. Lecka-Szlachta; J. Pusz; E. Woźnicka Antybakteryjna aktywność sulfonowych pochodnych chryzyny 2021
15 E. Ciszkowicz; M. Kosińska-Pezda; A. Kuźniar; K. Lecka-Szlachta; E. Pieniążek; E. Woźnicka; L. Zapała Synteza, charakterystyka i właściwości biologiczne kompleksów jonów antanowców lekkich z 3-hydroksyflawonem 2021
16 J. Kalembkiewicz; M. Kopacz; J. Pusz Badania naukowe i aplikacyjne flawonoidów 2021
17 J. Kalembkiewicz; M. Kopacz; J. Pusz Nauka i praktyka w świecie flawonoidów 2021
18 J. Kalembkiewicz; M. Kosińska-Pezda; J. Pusz; E. Woźnicka; L. Zapała Badania równowagi reakcji kompleksowania chryzyny z jonami Er(III) w układach: woda - metanol i woda - metanol - 1,4-dioksan 2021
19 M. Chutkowski; L. Zapała; W. Zapała; P. Ziobrowski Analiza mechanizmu retencji kwercetyny w wybranych układach chromatografii oddziaływań hydrofilowych (HILIC) 2021
20 M. Chutkowski; M. Kosińska-Pezda; M. Przywara; L. Zapała; W. Zapała; P. Ziobrowski Analysis of adsorption energy distribution in selected hydrophilic-interaction chromatography systems with amide, amine, and zwitterionic stationary phases 2021
21 Ł. Byczyński; E. Ciszkowicz; M. Kosińska-Pezda; K. Lecka-Szlachta; U. Maciołek; E. Woźnicka; L. Zapała; W. Zapała Green synthesis of niflumic acid complexes with some transition metal ions (Mn(II), Fe(III), Co(II), Ni(II), Cu(II) and Zn(II)). Spectroscopic, thermoanalytical and antibacterial studies 2021
22 Ł. Byczyński; M. Kosińska-Pezda; U. Maciołek; E. Woźnicka; L. Zapała; W. Zapała Thermal study, temperature diffraction patterns and evolved gas analysis during pyrolysis and oxidative decomposition of novel ternary complexes of light lanthanides with mefenamic acid and 1,10-phenanthroline 2021
23 J. Kalembkiewicz; A. Kuźniar; B. Papciak; J. Pusz; E. Sitarz-Palczak; E. Sočo; E. Woźnicka Pierwiastki i związki chemiczne 2020
24 J. Kalembkiewicz; A. Kuźniar; E. Pieniążek; E. Sočo; E. Woźnicka Aktywność biochemiczna sulfonowych pochodnych moryny 2020
25 J. Kalembkiewicz; B. Papciak; E. Pieniążek; J. Pusz; P. Skitał; E. Sočo; L. Zapała Podstawy chemii 2020
26 J. Kalembkiewicz; B. Papciak; J. Pusz; E. Sitarz-Palczak; E. Woźnicka Roztwory i procesy w roztworach 2020
27 J. Kalembkiewicz; M. Kopacz; J. Pusz Świat flawonoidów w badaniach naukowych 2020
28 M. Chutkowski; L. Zapała; W. Zapała; P. Ziobrowski Influence of Mobile Phase Composition and Temperature on the Retention Behavior of Selected Test Substances in Diol-type Column 2020
29 M. Kopacz; A. Kuźniar; B. Papciak; J. Pusz; E. Woźnicka Badania reakcji kompleksowania chryzyny z jonami Nd(III), Tb(III) i Dy(III) w roztworach wodno-metanolowych 2020
30 M. Kosińska-Pezda; E. Pieniążek; E. Woźnicka; L. Zapała Badania stałych produktów reakcji jonów Ag(I) i Cu(II) z 3-hydroksyflawonem i moryną 2020
31 M. Kosińska; E. Woźnicka; L. Zapała; W. Zapała Response of the DFT study to the calculations of selected microdissociation constants of anthranilic acid and its derivatives 2019
32 Ł. Byczyński; M. Chutkowski; E. Ciszkowicz; M. Kosińska; K. Lecka-Szlachta; E. Woźnicka; L. Zapała; W. Zapała Comparison of spectral and thermal properties and antibacterial activity of new binary and ternary complexes of Sm(III), Eu(III) and Gd (III) ions with N-phenylanthranilic acid and 1,10-phenanthroline 2019