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Hydrogen separation and purification processes

Some basic information about the module

Cycle of education: 2022/2023

The name of the faculty organization unit: The faculty Chemistry

The name of the field of study: Hydrogen technologies

The area of study: technical sciences

The profile of studing:

The level of study: second degree study

Type of study: past time

discipline specialities :

The degree after graduating from university: Master of Science (MSc)

The name of the module department : Department of Chemical Engineering and Process Control

The code of the module: 16579

The module status: mandatory for teaching programme

The position in the studies teaching programme: sem: 1 / W18 C9 L18 / 5 ECTS / E

The language of the lecture: Polish

The name of the coordinator: Wojciech Zapała, DSc, PhD, Eng.

The aim of studying and bibliography

The main aim of study: To familiarize students with the basic processes of hydrogen evolution and separation.

The general information about the module: The course will be conducted in Polish during the 2st semester in the following dimensions: 18 hours of lecture, 9 hours of exercises, 18 hours of laboratory. The course ends with an exam.

Bibliography required to complete the module
Bibliography used during lectures
1 R. Koch, A. Kozioł Dyfuzyjno – cieplny rozdział substancji WNT W-wa. 1994
2 R. Petrus, G. Aksielrud, J. Gumnicki, W. Piątkowski Wymiana masy ciało stałe – ciecz OW PRz. 1998
3 R. Rautenbach Procesy membranowe WNT. 1996
4 T. Chmielniak, T. Chmielniak Energetyka wodorowa PWN Warszawa. 2020
Bibliography used during classes/laboratories/others
1 K. Pawłow, P. Romankow, A.Noskow Przykłady i zadania z zakresu aparatury i inżynierii chemicznej WNT. 1981
2 W. Ciesielczyk, K. Kupiec Obliczenia w inżynierii chemicznej cz. IV. Obliczanie procesów przenoszenia masy. Politechnika Krakowska. 2014
3 W. Ciesielczyk, K. Kupiec Obliczenia w inżynierii chemicznej cz. III, Teoria procesów przenoszenia masy. Politechnika Krakowska. 2014

Basic requirements in category knowledge/skills/social competences

Formal requirements: Registration for a given semester.

Basic requirements in category knowledge: The student has ordered knowledge of mathematics, physics, chemistry, covering all issues related to the application of scientific methods in the type of engineering issues.

Basic requirements in category skills: He has ordered, basic knowledge in computer science that allows for efficient handling of basic utility programs such as Matlab, Origin, Excel, etc.

Basic requirements in category social competences: It has a sense of responsibility related to the performance of the engineering profession.

Module outcomes

MEK The student who completed the module Types of classes / teaching methods leading to achieving a given outcome of teaching Methods of verifying every mentioned outcome of teaching Relationships with KEK Relationships with PRK
01 Has knowledge of the theory and design of advanced unit operations in chemical engineering. lecture exam part written K_W04+
K_U02+
K_U05+
K_K02+
K_K03+
P7S_KO
P7S_KR
P7S_UW
P7S_WG
02 Has the knowledge and ability to solve mathematical problems related to the design of basic unit operations of chemical engineering. solving classes Final test K_W07+
K_U01+
K_U02+
K_U07+
P7S_UW
P7S_WG
03 Has the ability to service and identify the chemical apparatus laboratory Evaluation performed exercises and possibly theoretical test K_U04+
K_U11+
P7S_UO
P7S_UU
P7S_UW

Attention: Depending on the epidemic situation, verification of the achieved learning outcomes specified in the study program, in particular credits and examinations at the end of specific classes, can be implemented remotely (real-time meetings).

The syllabus of the module

Sem. TK The content realized in MEK
1 TK01 Advanced unit operations for the separation and / or purification of gaseous mixtures (with particular emphasis on hydrogen). Absorption, adsorption, membrane processes, etc. Thermodynamic description of processes, principles of design, apparatus. The content of exercises and laboratories related to the topic of lectures. W30, C15, L30 MEK01 MEK02 MEK03

The student's effort

The type of classes The work before classes The participation in classes The work after classes
Lecture (sem. 1) The preparation for a test: 5.00 hours/sem.
contact hours: 18.00 hours/sem.
complementing/reading through notes: 25.00 hours/sem.
Studying the recommended bibliography: 15.00 hours/sem.
Class (sem. 1) The preparation for a Class: 5.00 hours/sem.
The preparation for a test: 10.00 hours/sem.
contact hours: 9.00 hours/sem.
Finishing/Studying tasks: 2.00 hours/sem.
Laboratory (sem. 1) The preparation for a Laboratory: 3.00 hours/sem.
The preparation for a test: 2.00 hours/sem.
contact hours: 18.00 hours/sem.
Advice (sem. 1)
Exam (sem. 1) The preparation for an Exam: 15.00 hours/sem.
The written exam: 2.00 hours/sem.

The way of giving the component module grades and the final grade

The type of classes The way of giving the final grade
Lecture Lecture: Completion of the course based on an evaluation of the exam - OW
Class Ćwiczenia: zaliczenie na podstawie oceny z kolokwium - OC
Laboratory Laboratory: on the basis of the performed exercises and reports - OL
The final grade Score: OK = 60%OW+30%OC+10%OL. First term: w=1, second term: w=0,9, third term: w=0,8.

Sample problems

Required during the exam/when receiving the credit
(-)

Realized during classes/laboratories/projects
(-)

Others
(-)

Can a student use any teaching aids during the exam/when receiving the credit : no

The contents of the module are associated with the research profile: yes

1 M. Przywara; R. Przywara; W. Zapała Numerical Investigation on Flowability of Pulverized Biomass Using the Swelling Bed Model 2024
2 A. Bukowska; T. Galek; M. Przywara; R. Przywara; W. Zapała Brief Analysis of Selected Sorption and Physicochemical Properties of Three Different Silica-Based Adsorbents 2023
3 I. Opaliński; M. Przywara; R. Przywara; W. Zapała Mechanical Properties of Solid Biomass as Affected by Moisture Content 2023
4 M. Chutkowski; I. Opaliński; M. Przywara; R. Przywara; W. Zapała Influence of Moisture Content and Composition of Agricultural Waste with Hard Coal Mixtures on Mechanical and Rheological Properties 2023
5 M. Przywara; R. Przywara; W. Zapała Właściwości adsorpcyjne wybranych polarnych faz stacjonarnych 2023
6 Ł. Byczyński; M. Kosińska-Pezda; E. Woźnicka; L. Zapała; W. Zapała Synteza oraz badania składu i właściwości związków: 3-hydroksyflawonu, chryzyny oraz sulfonowych pochodnych chryzyny i kwercetyny z jonami Mn(II) 2023
7 L. Zapała; W. Zapała; P. Ziobrowski Studies on the retention behavior of quercetin, phenol and caffeine as test substances on selected neutral and charged Hydrophilic Interaction Liquid Chromatography stationary phases 2022
8 M. Chutkowski; J. Kamińska; M. Przywara; W. Zapała; P. Ziobrowski Studies on the Effects of Process Conditions on Separation of B1, B2 and B3 Vitamin Mixture Using HILIC and RPLC Chromatography 2022
9 M. Chutkowski; M. Przywara; R. Przywara; W. Zapała Column Testing in Quantitative Determination of Raw Heparin in Porcine Intestinal Mucus Extracts by Liquid Chromatography – Preliminary Investigations 2022
10 M. Kosińska-Pezda; U. Maciołek; E. Woźnicka; L. Zapała; W. Zapała Synteza, badania składu i właściwości spektroskopowych kompleksów wybranych jonów metali przejściowych z kwasem niflumowym 2022
11 W. Zapała; P. Ziobrowski Analiza mechanizmu retencji kofeiny, kwercetyny oraz fenolu w wybranych układach chromatografii oddziaływań hydrofilowych (HILIC) 2022
12 M. Chutkowski; L. Zapała; W. Zapała; P. Ziobrowski Analiza mechanizmu retencji kwercetyny w wybranych układach chromatografii oddziaływań hydrofilowych (HILIC) 2021
13 M. Chutkowski; M. Kosińska-Pezda; M. Przywara; L. Zapała; W. Zapała; P. Ziobrowski Analysis of adsorption energy distribution in selected hydrophilic-interaction chromatography systems with amide, amine, and zwitterionic stationary phases 2021
14 Ł. Byczyński; E. Ciszkowicz; M. Kosińska-Pezda; K. Lecka-Szlachta; U. Maciołek; E. Woźnicka; L. Zapała; W. Zapała Green synthesis of niflumic acid complexes with some transition metal ions (Mn(II), Fe(III), Co(II), Ni(II), Cu(II) and Zn(II)). Spectroscopic, thermoanalytical and antibacterial studies 2021
15 Ł. Byczyński; M. Kosińska-Pezda; U. Maciołek; E. Woźnicka; L. Zapała; W. Zapała Thermal study, temperature diffraction patterns and evolved gas analysis during pyrolysis and oxidative decomposition of novel ternary complexes of light lanthanides with mefenamic acid and 1,10-phenanthroline 2021
16 M. Chutkowski; L. Zapała; W. Zapała; P. Ziobrowski Influence of Mobile Phase Composition and Temperature on the Retention Behavior of Selected Test Substances in Diol-type Column 2020
17 M. Chutkowski; M. Przywara; W. Zapała Modelowanie i analiza płynięcia materiału rozdrobionego podczas ścinania w reometrze pierścieniowym z wykorzystaniem metody elementów dyskretnych 2020
18 M. Kosińska; E. Woźnicka; L. Zapała; W. Zapała Response of the DFT study to the calculations of selected microdissociation constants of anthranilic acid and its derivatives 2019
19 Ł. Byczyński; M. Chutkowski; E. Ciszkowicz; M. Kosińska; K. Lecka-Szlachta; E. Woźnicka; L. Zapała; W. Zapała Comparison of spectral and thermal properties and antibacterial activity of new binary and ternary complexes of Sm(III), Eu(III) and Gd (III) ions with N-phenylanthranilic acid and 1,10-phenanthroline 2019