The aim of studying and bibliography

The main aim of study: Obtaining by the student's the knowledge about the theory and design of the most important diffusive and heat - diffusive operations applied to separation processes. Obtaining by the student's the knowledge about the theory and design of the most important diffusive and heat - diffusive operations applied to separation processes.

The general information about the module: The syllabus contained in this sheet concern the "HYDROGEN TECHNOLOGIES" specialty. The course is conducted in Polish in semesters 5 and 6. Semester 5: 30h lectures, 15h classes. Semester 6: 15h lectures, 15h classes, 15h projects 15h laboratories. In both semesters module ends with an exam.

Bibliography required to complete the module

Bibliography used during lectures

1	R. Koch, A. Kozioł	Dyfuzyjno – cieplny rozdział substancji WNT W-wa 1994	WNT W-wa.	1994
2	A. Selecki, L. Gradoń	Podstawowe procesy przemysłu chemicznego	WNT W-wa .	1985
3	T. Hobler	Dyfuzyjny ruch masy i absorbery	WNT W-wa.	1976
4	R. Zarzycki i inni	Absorpcja i absorbery	WNT W-wa.	1987
5	J. Bandrowski, L. Troniewski	Destylacja i rektyfikacja	PWN W-wa.	1980
6	Z. Ziołkowski	Ekstrakcja cieczy w przemyśle chemicznym	WNT W-wa.	1980
7	M. Serwiński	Zasady Inżynierii chemicznej i procesowej	WNT W-wa.	1982
8	G.K. Fiłonienko, P.D. Lebiediew	Urządzenia suszarnicze	PWT W-wa.	1956
9	R. Petrus, G. Aksielrud, J. Gumnicki, W. Piątkowski	Wymiana masy ciało stałe – ciecz	OW PRz.	1998
10	R. Rautenbach	Procesy membranowe	WNT.	1996

Bibliography used during classes/laboratories/others

1	R. Zarzycki i inni	Zadania rachunkowe z inżynierii chemicznej	PWN W-wa.	1980
2	T. Kudra i inni	Zbiór zadań z podstaw teoretycznych inżynierii chemicznej i procesowej	WNT W-wa.	1985
3	J. Bandrowski i inni	Materiały pomocnicze do ćwiczeń i projektów z inżynierii chemicznej	Skrypt Politechniki Śląskiej, Gliwice.	1993
4	R. Petrus i inni	Inżynieria chemiczna - laboratorium	Politechnika Rzeszowska.	1990
5	K. Pawłow, P. Romankow, A.Noskow	Przykłady i zadania z zakresu aparatury i inżynierii chemicznej	WNT.	1981
6	W. Ciesielczyk, K. Kupiec	Obliczenia w inżynierii chemicznej cz. IV. Obliczanie procesów przenoszenia masy.	Politechnika Krakowska.	2014
7	W. Ciesielczyk, K. Kupiec	Obliczenia w inżynierii chemicznej cz. III, Teoria procesów przenoszenia masy.	Politechnika Krakowska.	2014

Basic requirements in category knowledge/skills/social competences

Formal requirements: Registration for a given semester.

Basic requirements in category knowledge: The student has ordered knowledge of mathematics, physics, chemistry, covering all issues related to the application of scientific methods in the type of engineering issues.

Basic requirements in category skills: He has ordered, basic knowledge in computer science that allows for efficient handling of basic utility programs such as Matlab, Origin, Excel, etc.

Basic requirements in category social competences: It has a sense of responsibility related to the performance of the engineering profession.

Module outcomes

MEK	The student who completed the module	Types of classes / teaching methods leading to achieving a given outcome of teaching	Methods of verifying every mentioned outcome of teaching	Relationships with KEK	Relationships with PRK
01	Has the knowledge about the theory and design of unit operations in chemical engineering.	lecture	written and oral exam	K_W03+++ K_W05++ K_U01+++ K_U09+	P6S_UW P6S_WG
02	Has the knowledge and ability to solve mathematical problems related to the design of basic unit operations of chemical engineering.	solving classes	Final test	K_W05+++ K_U05+++ K_K01+	P6S_KK P6S_UW P6S_WG
03	Has the ability to design basic unit processes of chemical engineering.	project	Evaluation projects carried out individually	K_U06+++ K_U08+++ K_U19++	P6S_UU P6S_UW
04	Has the ability to service and identify the basic chemical apparatus	laboratory	Evaluation performed exercises and possibly theoretical test	K_W03+++ K_U06+++ K_U08+	P6S_UW P6S_WG

Attention: Depending on the epidemic situation, verification of the achieved learning outcomes specified in the study program, in particular credits and examinations at the end of specific classes, can be implemented remotely (real-time meetings).

The syllabus of the module

Sem.	TK	The content	realized in	MEK
5	TK01	Distillation and rectification. Liquid-vapor equilibrium for two-component and multi-component systems. Simple equilibrium distillation. Simple differential distillation. Steam and molecular distillation. Periodic and continuous two-component rectification: balances, operating lines, minimum and maximum return, determination of the number of theoretical plates by graphical and analytical methods. Rectification of multi-component mixtures. Design issues: selection of the type of apparatus, characteristics of the shelves and their efficiency, kinetic mass transfer coefficients, packed columns. Absorption. Characteristics of the process. Gas-liquid balance. Mass balance of the process and operating line. Methods for calculating the height of absorbers. Hydrodynamic problems and the diameter of the apparatus. Apparatus. Drying processes. Drying thermodynamics. Movement of mass and heat during drying. Ways of conducting the process. Drying apparatus. Crystallization. Material and energy balances, applications, apparatus and design. The topics of the exercises are closely related to the topics presented in the lecture.	W30C15	MEK01 MEK02 MEK03 MEK04
6	TK01	Liquid-liquid extraction. Physicochemical basics of extraction: solubility, equilibrium, partition coefficient, solvent selectivity, drip system mechanism. Calculation of mass transfer coefficients in the extraction process. One-step extraction. Co-current and counter-current multistage extraction. Determination of the minimum, maximum and optimal amount of solvent. Calculation of the number of steps and their efficiency. Column extraction in ternary systems: calculating the height and diameter of a column. Apparatus. Membrane processes. Types of membranes, applications, process modeling and design issues, apparatus. The topics of the exercises are closely related to the topics presented in the lecture. Laboratory: Five laboratory exercises related to the subject matter. Projects: Students design a mass exchanger working in a fluid-fluid system: rectification column and / or absorber.	W15C15P15L15	MEK01 MEK02 MEK03 MEK04

The student's effort

The type of classes	The work before classes	The participation in classes	The work after classes
Lecture (sem. 5)	The preparation for a test: 6.00 hours/sem.	contact hours: 30.00 hours/sem.	complementing/reading through notes: 2.00 hours/sem. Studying the recommended bibliography: 30.00 hours/sem.
Class (sem. 5)	The preparation for a Class: 7.00 hours/sem. The preparation for a test: 20.00 hours/sem.	contact hours: 15.00 hours/sem.
Advice (sem. 5)
Exam (sem. 5)	The preparation for an Exam: 10.00 hours/sem.
Lecture (sem. 6)	The preparation for a test: 5.00 hours/sem.	contact hours: 15.00 hours/sem.	complementing/reading through notes: 5.00 hours/sem. Studying the recommended bibliography: 5.00 hours/sem.
Class (sem. 6)	The preparation for a Class: 10.00 hours/sem. The preparation for a test: 20.00 hours/sem.	contact hours: 15.00 hours/sem.
Laboratory (sem. 6)	The preparation for a Laboratory: 1.00 hours/sem. The preparation for a test: 20.00 hours/sem.	contact hours: 15.00 hours/sem.
Project/Seminar (sem. 6)	The preparation for projects/seminars: 1.00 hours/sem.	contact hours: 15.00 hours/sem..	Doing the project/report/ Keeping records: 3.00 hours/sem. The preparation for the presentation: 1.00 hours/sem.
Advice (sem. 6)
Exam (sem. 6)	The preparation for an Exam: 10.00 hours/sem.

The way of giving the component module grades and the final grade

The type of classes	The way of giving the final grade
Lecture	Lecture: Completion of the course based on an evaluation of the exam - OW
Class	Classes: completion on the basis of the evaluation of the test - OC
The final grade
Lecture	Lecture: Completion of the course based on an evaluation of the exam - OW
Class	Classes: completion on the basis of the evaluation of the test - OC
Laboratory	Laboratory: on the basis of the performed exercises and reports - OL
Project/Seminar	Project: completion on the basis of completed projects - OP
The final grade	Score: OK = 60%OW+30%OC+10%OP. First term: w=1, second term: w=0,9, third term: w=0,8.

Sample problems

Required during the exam/when receiving the credit
(-)

Realized during classes/laboratories/projects
(-)

Others
(-)

Can a student use any teaching aids during the exam/when receiving the credit : no

The contents of the module are associated with the research profile: yes

1	M. Przywara; R. Przywara; W. Zapała	Numerical Investigation on Flowability of Pulverized Biomass Using the Swelling Bed Model	2024
2	A. Bukowska; T. Galek; M. Przywara; R. Przywara; W. Zapała	Brief Analysis of Selected Sorption and Physicochemical Properties of Three Different Silica-Based Adsorbents	2023
3	I. Opaliński; M. Przywara; R. Przywara; W. Zapała	Mechanical Properties of Solid Biomass as Affected by Moisture Content	2023
4	M. Chutkowski; I. Opaliński; M. Przywara; R. Przywara; W. Zapała	Influence of Moisture Content and Composition of Agricultural Waste with Hard Coal Mixtures on Mechanical and Rheological Properties	2023
5	M. Przywara; R. Przywara; W. Zapała	Właściwości adsorpcyjne wybranych polarnych faz stacjonarnych	2023
6	Ł. Byczyński; M. Kosińska-Pezda; E. Woźnicka; L. Zapała; W. Zapała	Synteza oraz badania składu i właściwości związków: 3-hydroksyflawonu, chryzyny oraz sulfonowych pochodnych chryzyny i kwercetyny z jonami Mn(II)	2023
7	L. Zapała; W. Zapała; P. Ziobrowski	Studies on the retention behavior of quercetin, phenol and caffeine as test substances on selected neutral and charged Hydrophilic Interaction Liquid Chromatography stationary phases	2022
8	M. Chutkowski; J. Kamińska; M. Przywara; W. Zapała; P. Ziobrowski	Studies on the Effects of Process Conditions on Separation of B1, B2 and B3 Vitamin Mixture Using HILIC and RPLC Chromatography	2022
9	M. Chutkowski; M. Przywara; R. Przywara; W. Zapała	Column Testing in Quantitative Determination of Raw Heparin in Porcine Intestinal Mucus Extracts by Liquid Chromatography – Preliminary Investigations	2022
10	M. Kosińska-Pezda; U. Maciołek; E. Woźnicka; L. Zapała; W. Zapała	Synteza, badania składu i właściwości spektroskopowych kompleksów wybranych jonów metali przejściowych z kwasem niflumowym	2022
11	W. Zapała; P. Ziobrowski	Analiza mechanizmu retencji kofeiny, kwercetyny oraz fenolu w wybranych układach chromatografii oddziaływań hydrofilowych (HILIC)	2022
12	M. Chutkowski; L. Zapała; W. Zapała; P. Ziobrowski	Analiza mechanizmu retencji kwercetyny w wybranych układach chromatografii oddziaływań hydrofilowych (HILIC)	2021
13	M. Chutkowski; M. Kosińska-Pezda; M. Przywara; L. Zapała; W. Zapała; P. Ziobrowski	Analysis of adsorption energy distribution in selected hydrophilic-interaction chromatography systems with amide, amine, and zwitterionic stationary phases	2021
14	Ł. Byczyński; E. Ciszkowicz; M. Kosińska-Pezda; K. Lecka-Szlachta; U. Maciołek; E. Woźnicka; L. Zapała; W. Zapała	Green synthesis of niflumic acid complexes with some transition metal ions (Mn(II), Fe(III), Co(II), Ni(II), Cu(II) and Zn(II)). Spectroscopic, thermoanalytical and antibacterial studies	2021
15	Ł. Byczyński; M. Kosińska-Pezda; U. Maciołek; E. Woźnicka; L. Zapała; W. Zapała	Thermal study, temperature diffraction patterns and evolved gas analysis during pyrolysis and oxidative decomposition of novel ternary complexes of light lanthanides with mefenamic acid and 1,10-phenanthroline	2021
16	M. Chutkowski; L. Zapała; W. Zapała; P. Ziobrowski	Influence of Mobile Phase Composition and Temperature on the Retention Behavior of Selected Test Substances in Diol-type Column	2020
17	M. Chutkowski; M. Przywara; W. Zapała	Modelowanie i analiza płynięcia materiału rozdrobionego podczas ścinania w reometrze pierścieniowym z wykorzystaniem metody elementów dyskretnych	2020
18	M. Kosińska; E. Woźnicka; L. Zapała; W. Zapała	Response of the DFT study to the calculations of selected microdissociation constants of anthranilic acid and its derivatives	2019
19	Ł. Byczyński; M. Chutkowski; E. Ciszkowicz; M. Kosińska; K. Lecka-Szlachta; E. Woźnicka; L. Zapała; W. Zapała	Comparison of spectral and thermal properties and antibacterial activity of new binary and ternary complexes of Sm(III), Eu(III) and Gd (III) ions with N-phenylanthranilic acid and 1,10-phenanthroline	2019