The aim of studying and bibliography

The main aim of study: To acquaint students with highly effective and pro-ecological techniques of separation and purification of different chemical mixtures.

The general information about the module: Student gains knowledge about the separation and purification of mixtures using the membrane and chromatographic methods.

Bibliography required to complete the module

Bibliography used during lectures

1	R. Rautenbach	Procesy membranowe	WNT.	1996
2	E. Molga	Procesy adsorpcji reaktywnej	WNT.	2008
3	B.K. Głód, P. Piszcz	Podstawy wysokosprawnej chromatografii cieczowej	Wydawnictwo Naukowe Uniwersytetu Przyrodniczo-Humanistycznego w Siedlcach.	2019
4	W. Zapała	Modelowanie procesu retencji w wybranych rodzajach chromatografii cieczowej	Oficyna Wydawnicza Politechniki Rzeszowskiej.	2012
5	A. Selecki, R. Gawroński	Podstawy projektowania wybranych procesów rozdzielania mieszanin.	WNT.	1992

Bibliography used during classes/laboratories/others

1

W. Zapała, K. Kaczmarski, I. Poplewska, W. Piątkowski

Wybrane operacje jednostkowe w inżynierii chemicznej

Oficyna Wydawnicza PRz.

2012

Basic requirements in category knowledge/skills/social competences

Formal requirements: Knowledge of Mathematics, Physics, Physical Chemistry, Thermodynamics, Chemical Technology and Fundamentals of Chemical and Process Engineering

Basic requirements in category knowledge: The student has ordered knowledge of mathematics, physics, chemistry, covering all issues related to the application of scientific methods in the type of engineering issues.

Basic requirements in category skills: He has ordered, basic knowledge in computer science thhandling of basic utility programs such as Matlab, Origin, Excel, etc.at allows for efficient

Basic requirements in category social competences: It has a sense of responsibility related to the performance of the engineering profession.

Module outcomes

MEK	The student who completed the module	Types of classes / teaching methods leading to achieving a given outcome of teaching	Methods of verifying every mentioned outcome of teaching	Relationships with KEK	Relationships with PRK
01	Student gains knowledge about the separation and purification of mixtures with the use of membrane and chromatographic techniques. He knows the principles of physico-chemical separation using permeation methods and different chromatographic methods.	lecure	Exam	K_W05+ K_W07+++ K_W09+++ K_U14++	P7S_UW P7S_WG
02	It can be separated substances by chromatographic and membrane methods.	laboratory	Evaluation performed exercises.	K_W07+++ K_U08+ K_U09++ K_U13+ K_K02+	P7S_KO P7S_UO P7S_UW P7S_WG

Attention: Depending on the epidemic situation, verification of the achieved learning outcomes specified in the study program, in particular credits and examinations at the end of specific classes, can be implemented remotely (real-time meetings).

The syllabus of the module

Sem.	TK	The content	realized in	MEK
2	TK01	Permeation techniques for separating mixtures: ultrafiltration, microfiltration, osmosis, reverse osmosis, dialysis, electrodialysis. Physicochemical background and mathematical models of processes. Theory and applications of ion exclusion chromatography and hydrophilic interaction chromatography. Batch and continuous column chromatography (SMB). Expanded bed technique. Ion exchange chromatography, gel permeation chromatography. Mathematical modeling and optimization of chromatographic separation processes. Theoretical basis and applications of reactive adsorption processes.	-	MEK01 MEK02

The student's effort

The type of classes	The work before classes	The participation in classes	The work after classes
Lecture (sem. 2)	The preparation for a test: 15.00 hours/sem.	contact hours: 30.00 hours/sem.	complementing/reading through notes: 5.00 hours/sem. Studying the recommended bibliography: 5.00 hours/sem.
Laboratory (sem. 2)	The preparation for a Laboratory: 5.00 hours/sem. The preparation for a test: 10.00 hours/sem.	contact hours: 30.00 hours/sem.
Advice (sem. 2)
Exam (sem. 2)	The preparation for an Exam: 15.00 hours/sem.	The written exam: 1.00 hours/sem.

The way of giving the component module grades and the final grade

The type of classes	The way of giving the final grade
Lecture	Written test
Laboratory	the average of the ratings of all exercises
The final grade	w*0.6 * (mark of the lecture)+ w*0.4 * (mark of the laboratory). First term: w=1, second term: w=0,9, third term: w=0,8.

Sample problems

Required during the exam/when receiving the credit
(-)

Realized during classes/laboratories/projects
(-)

Others
(-)

Can a student use any teaching aids during the exam/when receiving the credit : no

The contents of the module are associated with the research profile: yes

1	M. Przywara; R. Przywara; W. Zapała	Numerical Investigation on Flowability of Pulverized Biomass Using the Swelling Bed Model	2024
2	A. Bukowska; T. Galek; M. Przywara; R. Przywara; W. Zapała	Brief Analysis of Selected Sorption and Physicochemical Properties of Three Different Silica-Based Adsorbents	2023
3	D. Antos; R. Muca	Protein association on multimodal chromatography media	2023
4	I. Opaliński; M. Przywara; R. Przywara; W. Zapała	Mechanical Properties of Solid Biomass as Affected by Moisture Content	2023
5	M. Chutkowski; I. Opaliński; M. Przywara; R. Przywara; W. Zapała	Influence of Moisture Content and Composition of Agricultural Waste with Hard Coal Mixtures on Mechanical and Rheological Properties	2023
6	M. Przywara; R. Przywara; W. Zapała	Właściwości adsorpcyjne wybranych polarnych faz stacjonarnych	2023
7	Ł. Byczyński; M. Kosińska-Pezda; E. Woźnicka; L. Zapała; W. Zapała	Synteza oraz badania składu i właściwości związków: 3-hydroksyflawonu, chryzyny oraz sulfonowych pochodnych chryzyny i kwercetyny z jonami Mn(II)	2023
8	L. Zapała; W. Zapała; P. Ziobrowski	Studies on the retention behavior of quercetin, phenol and caffeine as test substances on selected neutral and charged Hydrophilic Interaction Liquid Chromatography stationary phases	2022
9	M. Chutkowski; J. Kamińska; M. Przywara; W. Zapała; P. Ziobrowski	Studies on the Effects of Process Conditions on Separation of B1, B2 and B3 Vitamin Mixture Using HILIC and RPLC Chromatography	2022
10	M. Chutkowski; M. Przywara; R. Przywara; W. Zapała	Column Testing in Quantitative Determination of Raw Heparin in Porcine Intestinal Mucus Extracts by Liquid Chromatography – Preliminary Investigations	2022
11	M. Kosińska-Pezda; U. Maciołek; E. Woźnicka; L. Zapała; W. Zapała	Synteza, badania składu i właściwości spektroskopowych kompleksów wybranych jonów metali przejściowych z kwasem niflumowym	2022
12	W. Zapała; P. Ziobrowski	Analiza mechanizmu retencji kofeiny, kwercetyny oraz fenolu w wybranych układach chromatografii oddziaływań hydrofilowych (HILIC)	2022
13	M. Chutkowski; L. Zapała; W. Zapała; P. Ziobrowski	Analiza mechanizmu retencji kwercetyny w wybranych układach chromatografii oddziaływań hydrofilowych (HILIC)	2021
14	M. Chutkowski; M. Kosińska-Pezda; M. Przywara; L. Zapała; W. Zapała; P. Ziobrowski	Analysis of adsorption energy distribution in selected hydrophilic-interaction chromatography systems with amide, amine, and zwitterionic stationary phases	2021
15	Ł. Byczyński; E. Ciszkowicz; M. Kosińska-Pezda; K. Lecka-Szlachta; U. Maciołek; E. Woźnicka; L. Zapała; W. Zapała	Green synthesis of niflumic acid complexes with some transition metal ions (Mn(II), Fe(III), Co(II), Ni(II), Cu(II) and Zn(II)). Spectroscopic, thermoanalytical and antibacterial studies	2021
16	Ł. Byczyński; M. Kosińska-Pezda; U. Maciołek; E. Woźnicka; L. Zapała; W. Zapała	Thermal study, temperature diffraction patterns and evolved gas analysis during pyrolysis and oxidative decomposition of novel ternary complexes of light lanthanides with mefenamic acid and 1,10-phenanthroline	2021
17	D. Antos; G. Carta; M. Kołodziej; R. Muca; W. Piątkowski	Effects of negative and positive cooperative adsorption of proteins on hydrophobic interaction chromatography media	2020
18	M. Chutkowski; L. Zapała; W. Zapała; P. Ziobrowski	Influence of Mobile Phase Composition and Temperature on the Retention Behavior of Selected Test Substances in Diol-type Column	2020
19	M. Chutkowski; M. Przywara; W. Zapała	Modelowanie i analiza płynięcia materiału rozdrobionego podczas ścinania w reometrze pierścieniowym z wykorzystaniem metody elementów dyskretnych	2020
20	M. Kosińska; E. Woźnicka; L. Zapała; W. Zapała	Response of the DFT study to the calculations of selected microdissociation constants of anthranilic acid and its derivatives	2019
21	Ł. Byczyński; M. Chutkowski; E. Ciszkowicz; M. Kosińska; K. Lecka-Szlachta; E. Woźnicka; L. Zapała; W. Zapała	Comparison of spectral and thermal properties and antibacterial activity of new binary and ternary complexes of Sm(III), Eu(III) and Gd (III) ions with N-phenylanthranilic acid and 1,10-phenanthroline	2019