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Experimental methodology

Some basic information about the module

Cycle of education: 2022/2023

The name of the faculty organization unit: The faculty Chemistry

The name of the field of study: Biotechnology

The area of study: technical sciences

The profile of studing:

The level of study: second degree study

Type of study: full time

discipline specialities : Laboratory diagnostics in biotechnology, Pharmaceutical biotechnology, Process and bioprocess engineering, Purification and analysis of biotechnological products

The degree after graduating from university: Master of Science (MSc)

The name of the module department : Department of Biochemistry and Bioinformatics

The code of the module: 1399

The module status: mandatory for teaching programme Process and bioprocess engineering, Purification and analysis of biotechnological products

The position in the studies teaching programme: sem: 1 / W5 L30 / 2 ECTS / Z

The language of the lecture: Polish

The name of the coordinator 1: Lucjan Dobrowolski, PhD, Eng.

The name of the coordinator 2: Karol Hęclik, PhD, Eng.

The aim of studying and bibliography

The main aim of study: Preparing students to independently planning and conducting experimental work and the elaboration of experimental results in a form suitable for publication.

The general information about the module: The student gains the skills and competence to independently plan and carry out the experimental work and the elaboration of experimental results in a form suitable for publication.

Teaching materials: Materiały dydaktyczne opublikowane na stronach portalu www.e-chemia.pl

Bibliography required to complete the module
Bibliography used during lectures
1 B. Dębska Konspekty do wykładów opublikowane na stronie Zakładu Informatyki Chemicznej http://www.prz.rzeszow.pl/chemia/zich/index.php/do-pobrania. 2011
Bibliography used during classes/laboratories/others
1 B. Dębska, B. Guzowska-Świder Instrukcje laboratoryjne opublikowane na stronie Zakładu Informatyki Chemicznej http://www.prz.rzeszow.pl/chemia/zich/index.php/do-pobrania. 2011
Bibliography to self-study
1 W. Pytkowski Organizacja badań i prac naukowych PWN, Warszawa . 1985
2 Z. Hippe Zastosowanie metod sztucznej inteligencji w chemii PWN, Warszawa. 1993
3 C. Radhakrishna Rao Statystka i prawda PWN, Warszawa . 1994
4 J. Jakubowski, J. Wątroba Zastosowanie metod statystycznych w badaniach naukowych StatSoft, Kraków . 2000
5 A. Pyrża Poradnik wynalazcy Urząd Patentowy RP, Warszawa. 2008

Basic requirements in category knowledge/skills/social competences

Formal requirements: Credit required courses: scientific and technologiical information, computer science, statistics and results elaboration.

Basic requirements in category knowledge: Knowledge about the literature databases and statistical processing of the experimental results.

Basic requirements in category skills: Ability: searching literature databases, posing and verifying statistical hypotheses, the use of STATISTICA program.

Basic requirements in category social competences: The ability to work individually and in a team.

Module outcomes

MEK The student who completed the module Types of classes / teaching methods leading to achieving a given outcome of teaching Methods of verifying every mentioned outcome of teaching Relationships with KEK Relationships with PRK
01 has advanced knowledge of information technology allowing him to use computer techniques and software packages in biotechnology practice lecture, laboratory, e-learning test K_W02+++
P7S_WG
02 has the practical knowledge in modeling, planning, design, optimization, and characterization of biotechnological processes lecture, laboratory, e-learning practice exam K_W04+++
P7S_WG
03 has the ability to independent preparation of scientific study, taking into account the literature review, the definition of the subject, the research methodology and discussion of the obtained results laboratory at which the student solves the problems project report K_U03+++
K_U08++
P7S_UO
P7S_UW
04 can use basic information and communication technologies and computer programs supporting experimental research methodology in the field of biotechnology laboratory observation of the task performance K_U07+++
P7S_UW
05 is able to plan, carry out and evaluate the experiment, interpret results and draw conclusions laboratory at which the student solves the problems project report K_U03++
K_U08+++
P7S_UO
P7S_UW

Attention: Depending on the epidemic situation, verification of the achieved learning outcomes specified in the study program, in particular credits and examinations at the end of specific classes, can be implemented remotely (real-time meetings).

The syllabus of the module

Sem. TK The content realized in MEK
1 TK01 Subject of study, research problems and their formulation. Stages of the research process. Review of the subject literature. Arrangement of gathered information. Defining the problems insufficiently known.Research hypotheses. Design of experiments. W01 MEK01
1 TK02 Optimization of experimental techniques. Development and validation of experimental data. Preparing the data for publication. W02 MEK02
1 TK03 Review of the literature. Analytical databases, library resources, patent databases. Finding connected problems and their dependence, defining the problems insufficiently known. L01-L02 MEK01
1 TK04 - L03-L04 MEK04
1 TK05 Registration and verification of the measurement results. Graphical presentation and interpretation of the experiment results. L05 MEK05
1 TK06 Designing and carrying out the processes aimed at obtaining products with the desired characteristics (properties) – classification and forecasting systems, artificial neural networks. L06-L08 MEK01
1 TK07 Optimization of experimental techniques. Development and validation of experimental data. L09 MEK02
1 TK08 Elaboration of experimental results in the form suitable for publication. L10 MEK03 MEK05

The student's effort

The type of classes The work before classes The participation in classes The work after classes
Lecture (sem. 1) The preparation for a test: 5.00 hours/sem.
contact hours: 5.00 hours/sem.
Laboratory (sem. 1) The preparation for a Laboratory: 2.00 hours/sem.
The preparation for a test: 2.00 hours/sem.
Others: 10.00 hours/sem.
contact hours: 30.00 hours/sem.
Advice (sem. 1) The participation in Advice: 2.00 hours/sem.
Credit (sem. 1) The preparation for a Credit: 3.00 hours/sem.
The written credit: 1.00 hours/sem.

The way of giving the component module grades and the final grade

The type of classes The way of giving the final grade
Lecture Lecture: credit course based on the evaluation of the test – OW
Laboratory Computer lab: credit based on the evaluation of completed tasks
The final grade Final evaluation of the module is calculated by the following formula: OK = 50% OW + 50% OL

Sample problems

Required during the exam/when receiving the credit
(-)

Realized during classes/laboratories/projects
(-)

Others
(-)

Can a student use any teaching aids during the exam/when receiving the credit : no

The contents of the module are associated with the research profile: yes

1 A. Czerniecka-Kubicka; L. Dobrowolski; K. Hęclik; I. Zarzyka Kompozyt polimerowy oraz sposób wytwarzania kompozytu polimerowego 2024
2 L. Dobrowolski; K. Hęclik; M. Jaromin; I. Zarzyka A Practical Test of Distance Learning During the COVID-19 Lockdown 2023
3 M. Bakar; A. Białkowska; A. Czerniecka-Kubicka; L. Dobrowolski; K. Hęclik; B. Krzykowska; M. Longosz; I. Zarzyka Polymer Biocompositions and Nanobiocomposites Based on P3HB with Polyurethane and Montmorillonite 2023
4 M. Chmiela; A. Czerniecka-Kubicka; L. Dobrowolski; W. Gonciarz; K. Hęclik; M. Longosz; A. Szyszkowska; D. Trzybiński; K. Woźniak; A. Wróbel; I. Zarzyka Molecular Modeling of 3-chloro-3-phenylquinoline-2,4-dione, Crystal Structure and Cytotoxic Activity for developments in a potential new drug 2023
5 K. Hęclik; M. Jacquet; J. Kargul; S. Kozdra; P. Michałowski; A. Wójcik Insight into structure-property relationship of organometallic terpyridine wires: Combined theoretical and experimental study 2022
6 M. Bakar; A. Białkowska; A. Czerniecka-Kubicka; L. Dobrowolski; K. Hęclik; B. Krzykowska; I. Zarzyka Biobased poly(3-hydroxybutyrate acid) composites with addition of aliphatic polyurethane based on polypropylene glycols 2022
7 K. Hęclik; K. Hęclik; I. Zarzyka Metal-Humus Acid Nanoparticles - Synthesis, Characterization and Molecular Modeling 2021
8 M. Bakar; A. Białkowska; A. Czerniecka-Kubicka; L. Dobrowolski; K. Hęclik; K. Leś; M. Pyda; M. Walczak; I. Zarzyka Thermally stable biopolymer composites based on poly(3-hydroxybutyrate) modified with linear aliphatic polyurethanes – preparation and properties 2021
9 A. Białkowska; L. Dobrowolski; L. Wianowski; I. Zarzyka Physical blowing agents for polyurethanes 2020
10 A. Czerniecka-Kubicka; L. Dobrowolski; K. Hęclik; I. Zarzyka Biodegradowalne kompozyty polimerowe na osnowie P3HB 2020
11 R. Bartosik; L. Dobrowolski; K. Hęclik; A. Klasek; A. Lycka; I. Zarzyka New mono- and diesters with imidazoquinolinone ring- synthesis, structure characterization and molecular modeling 2020
12 B. Dębska; J. Duliban; K. Hęclik; J. Lubczak Analysis of the Possibility and Conditions of Application of Methylene Blue to Determine the Activity of Radicals in Model System with Preaccelerated Cross-Linking of Polyester Resins 2019
13 B. Dębska; L. Dobrowolski; M. Inger; M. Jaromin; M. Wilk Komputerowo-wspomagane obliczanie bilansu masowego i cieplnego instalacji chemicznej 2019
14 K. Hęclik; A. Klasek; S. Pawlędzio; A. Szyszkowska; D. Trzybiński; K. Woźniak; I. Zarzyka Unprecedented reaction course of 1-phenyl-2H,6H-imidazo[1,5-c]quinazoline-3,5-dione with an excess of ethylene oxide 2019
15 K. Hęclik; A. Szyszkowska; I. Zarzyka Spatial packing of diols and esters with imidazoquinazoline ring - quantum-mechanical modelling 2019