The aim of studying and bibliography

The main aim of study: The main goal is to teach students theoretical knowledge for the analysis of raw materials and industrial products as well as selected aspects of process control, and quality assurance procedures in industrial analysis. Furthermore, the acquisition by the student of the practical execution of exemplary analytical determinations of raw materials and products.

The general information about the module: The module is implemented in the second semester and includes 30 hours of lecture and 30 hours laboratory. The module ends with an exam. Main topics: Aim and scope of technical analysis. Analysis of raw materials and industrial inorganic and organic products, including analysis of water, gas and dust, solid and liquid fuels, lubricants, fertilizers, construction binders, glass products. Analysis of raw materials and related industries: pharmaceutical, food, and others, including the analysis of sugars, fats, protein material, methods of surface analysis of electronic materials. Selected aspects of the analysis of wastewater. Quality assurance procedures in industrial analysis. Lectures are conducted in the form of Power Point presentations (after POWER-Kadra training).

Teaching materials: Instrukcje do ćwiczeń laboratoryjnych.

others: Mat. pom.: http://bogdanpapciak.v.prz.edu.pl/. Poz. lit. nr 2(W) i 1(L) dost. u koordynatora

Bibliography required to complete the module

Bibliography used during lectures

1	J. Berćik	Fizyczne i fizykochemiczne metody analizy	W N T, Warszawa .	1981
2	B. Klepaczko‑Filipiak, J. Łoin	Pracownia chemiczna, Analiza techniczna	wyd.2, W S i P, Warszawa .	1998
3	Z. Łada, C. Różycki	Pracownia chemii analitycznej, Analiza techniczna i instrumentalna	wyd. 6, W S i P, Warszawa .	1990
4	J. Namieśnik	Fizykochemiczne metody kontroli zanieczyszczeń środowiska	W N T, Warszawa.	1998
5	A. Hulanicki	Współczesna chemia analityczna. Wybrane zagadnienia	PWN, Warszawa.	2001
6	A. Cygański	Chemiczne metody analizy ilościowej	wyd. 5 rozsz., W N T, Warszawa.	1999
7	Normy Polskie i Europejskie		.
8	M. Trojanowicz, .	Automatyzacja w analizie chemicznej	W N T, Warszawa.	1992

Bibliography used during classes/laboratories/others

1

I.B. Czerwiński, A. Iwasiewicz, Z. Paszek, A. Sikorski

Metody statystyczne dla chemików

PWN, Warszawa.

1996

Basic requirements in category knowledge/skills/social competences

Formal requirements: Registration a student by the dean's office and a referral to classes

Basic requirements in category knowledge: Basic theoretical knowledge in the field of analytical chemistry and instrumental analysis.

Basic requirements in category skills: Basic theoretical and manual skills required to perform simple analyzes. Knowledge of basic laboratory equipment used in the analytical laboratory.

Basic requirements in category social competences: Ability and understanding of the need to work in the laboratory in accordance with the principles of occupational safety and health and awareness of the harmful effects on the environment.

Module outcomes

MEK	The student who completed the module	Types of classes / teaching methods leading to achieving a given outcome of teaching	Methods of verifying every mentioned outcome of teaching	Relationships with KEK	Relationships with PRK
01	Theoretical knowledge regarding the purpose, scope, methods and techniques used in the chemical and physico-chemical industrial analysis is obtained.	lecture	written exam	K_W08++ K_W10++ K_U14+++	P7S_UW P7S_WG
02	Ability to perform practical examples of analytical determinations of raw materials and products is achieved.	laboratory classes	written test, written report, observation of execution	K_U14++	P7S_UW
03	Able to work in a team performing analytical determination.	laboratory exercises	observation of execution	K_K01++ K_K02++	P7S_KK P7S_KO
04	Knows the basic analytical methods used for the determination of raw materials, intermediate products and products of selected industries inorganic, organic, food, electronics, etc.	lecture, laboratory	written test	K_W08++	P7S_WG

Attention: Depending on the epidemic situation, verification of the achieved learning outcomes specified in the study program, in particular credits and examinations at the end of specific classes, can be implemented remotely (real-time meetings).

The syllabus of the module

Sem.	TK	The content	realized in	MEK
2	TK01	Aim and scope technical analysis. Analysis of raw materials and industrial products of inorganic and organic, including analysis of water, gas and dust, solid and liquid fuels, lubricants, fertilizers, construction binders, glass products. Analysis of raw materials and related industries: pharmaceutical, food, and others, including the analysis of sugars, fats, protein material, methods of surface analysis of electronic materials. Selected aspects of the analysis of wastewater. Quality assurance procedures in industrial analysis.	W01-W30	MEK01 MEK04
2	TK02	Analysis of paper products: determination of matter insoluble in HCl, determination of selected heavy metals. Analysis of metallic alloys: determination of zinc in alloys. Determination of the composition and physico-chemical properties of water: determination of chemical oxygen demand. Evaluation of the properties and composition of the mineral industry: determination of macro-and micro- components in technical hydrochloric acid. Analysis of inorganic commercial fertilizers: determination of potassium content by flame photometry.	L01-L30	MEK02 MEK03

The student's effort

The type of classes	The work before classes	The participation in classes	The work after classes
Lecture (sem. 2)		contact hours: 30.00 hours/sem.	complementing/reading through notes: 5.00 hours/sem. Studying the recommended bibliography: 5.00 hours/sem.
Laboratory (sem. 2)	The preparation for a Laboratory: 2.00 hours/sem. The preparation for a test: 10.00 hours/sem.	contact hours: 30.00 hours/sem.	Finishing/Making the report: 6.00 hours/sem.
Advice (sem. 2)	The preparation for Advice: 2.00 hours/sem.	The participation in Advice: 2.00 hours/sem.
Exam (sem. 2)	The preparation for an Exam: 25.00 hours/sem.	The written exam: 2.00 hours/sem.

The way of giving the component module grades and the final grade

The type of classes	The way of giving the final grade
Lecture	A positive result (OW) of the written exam. The unfavorable result: 2.0 (ndst) refers to obtain from 0.0 to 49.9% of the total points. Satisfactory results: 3,0 (dst) refers to obtain from 50,0 to 66,1% of the points, 3,5 (+dst) refers to obtain from 66,2 to 75,1% of the points, 4,0 (db) refers to obtain from 75,2 to 85,1% of the points, 4,5 (+db) refers to obtain from od 85,2 to 94,1% of the points, 5,0 (bdb) refers to obtain from od 94,2 to 100% of the points.
Laboratory	The pass is to get good ratings in the written tests from material referred to in the field and perform all the exercises included in the program. Rating of Laboratory (OL) is the arithmetic mean of written tests and report grade during the classes.
The final grade	Final grade (Ok) is calculated according to the formula: Ok = 0,6·w·OW + 0,4·w·OL , where w is a factor related to the term examination: 1.0 - a first time; 0.9 - a second time, 0.8 - third time, and then rounded according to the rules given in the Quality Education Faculty (Part 6 of Chapter V, Section 2).

Sample problems

Required during the exam/when receiving the credit
(-)

Realized during classes/laboratories/projects
(-)

Others
(-)

Can a student use any teaching aids during the exam/when receiving the credit : no

The contents of the module are associated with the research profile: yes

1	J. Kalembkiewicz; A. Kuźniar; B. Papciak; E. Sočo	Zastosowanie materiału krzemionkowego modyfikowanego surfaktantem do immobilizacji moryny	2023
2	J. Kalembkiewicz; B. Papciak; E. Pieniążek; E. Sočo	Stałe związki kompleksowe jonów tytanu(IV) z sulfonową pochodną moryny	2021
3	J. Kalembkiewicz; A. Kuźniar; B. Papciak; J. Pusz; E. Sitarz-Palczak; E. Sočo; E. Woźnicka	Pierwiastki i związki chemiczne	2020
4	J. Kalembkiewicz; B. Papciak	Chemia ogólna i nieorganiczna. Pierwiastki i związki chemiczne. Surowce i produkty nieorganiczne: obliczenia chemiczne i problemy	2020
5	J. Kalembkiewicz; B. Papciak	Chemia ogólna i nieorganiczna. Podstawy chemii. Roztwory i procesy w roztworach: obliczenia chemiczne i problemy	2020
6	J. Kalembkiewicz; B. Papciak	Uzupełnienia	2020
7	J. Kalembkiewicz; B. Papciak; E. Pieniążek; J. Pusz; P. Skitał; E. Sočo; L. Zapała	Podstawy chemii	2020
8	J. Kalembkiewicz; B. Papciak; J. Pusz; E. Sitarz-Palczak; E. Woźnicka	Roztwory i procesy w roztworach	2020
9	M. Kopacz; A. Kuźniar; B. Papciak; J. Pusz; E. Woźnicka	Badania reakcji kompleksowania chryzyny z jonami Nd(III), Tb(III) i Dy(III) w roztworach wodno-metanolowych	2020