The aim of studying and bibliography

The main aim of study: This course focuses on the theory and application of advanced analytical instrumentation. Broadening the knowledge of IR absorption spectroscopy. Introduction to ESR, 13C-NMR spectroscopy. Surface analysis techniques (STM, AFM, SEM, etc.). Electrophoresis.

The general information about the module: Acquisition of a theoretical knowledge and experience on practical applications of advanced instrumental analysis techniques used for chemical analysis of organic and inorganic materials.

others: Instrukcje do ćwiczeń laboratoryjnych.

Bibliography required to complete the module

Bibliography used during lectures

1	Z. Sarbak	Metody instrumentalne w badaniach adsorbentów i katalizatorów	UAM.	2005
2	J. Stankowski, W. Hilczer	Wstęp do spektroskopii rezonansów magnetycznych	PWN, Warszawa.	2005
3	W. Rajca (red)	Metody spektroskopowe i ich zastosowanie do identyfikacji związków organicznych	WNT, Warszawa.	2000
4	Z. Kęcki	Podstawy spektroskopii molekularnej	PWN, Warszawa.	1998
5	M. Symons	Spektroskopia EPR w chemii i biochemii	PWN, Warszawa.	1987
6	M. Berek, M. Dressler, M. Kubin, K. Marcinka	Chromatografia żelowa	PWN, Warszawa.	1989
7	Z. Jóźwiak, G. Bartosz	Biofizyka. Wybrane zagadnienia wraz z ćwiczeniami	PWN Warszawa.	2007

Bibliography to self-study

1	J. A. Weil, J. R. Bolton, J. E. Wertz	Electron Paramagnetic Resonance. Elementary Theory and Practical Applications,	Wiley Intersci. Publ., New York.	1994
2	W. Przygocki,	Metody fizyczne badań polimerów	PWN, Warszawa.	1990
3	P.D. Grossman, J.C. Colburn	Capillary electrophoresis - theory and practice	Academic Press Inc. .	1992

Basic requirements in category knowledge/skills/social competences

Formal requirements: Passed the exam in Physics, Analytical Chemistry, Bases of Instrumental Analysis and also Physical and Organic Chemistry.

Basic requirements in category knowledge: Knowledge of Physics, Chemistry and Instrumental Analysis at the graduate level.

Basic requirements in category skills: Skills in operation of basic laboratory equipment and instruments for basic instrumental analysis techniques as well as computer. A knowledge of mathematics.

Basic requirements in category social competences: Knowledge of principles of safe work in chemical laboratory, responsibility during experiments performed individually or in laboratory group.

Module outcomes

MEK	The student who completed the module	Types of classes / teaching methods leading to achieving a given outcome of teaching	Methods of verifying every mentioned outcome of teaching	Relationships with KEK	Relationships with PRK
01	Student has a widen knowledge of theoretical basis, a construction and operation principles of modern instruments applied in advanced analysis techniques (IR, magnetic resonance, surface analysis, etc.).	lecture, laboratory	written test	K_W01+++	P7S_WG
02	Student has a knowledge about the possibilities of application the particular instrumental methods of analysis for problem solving in materials analysis, adequately to chosen specialization.	lecture	written test	K_W01++	P7S_WG
03	Is able to assess significance of data obtained with particular methods as well as to choose a technique adequate for testing given phenomenon or material.	lecture, laboratory	written test	K_U14++	P7S_UW
04	Is able to interpret qualitatively and quantitatively results of spectroscopic measurements and to assess values of experimental errors.	lecture, laboratory	written test, written report	K_U08+ K_U14++	P7S_UW
05	He can perform an experiment in laboratory team and recount the results as well as participate in discussion around data interpretation.	laboratory	practical performance evaluation	K_K02+	P7S_KO
06	He knows and follows the principles of safe work with lasers, microwaves, using high strength magnetic fields.	lecture, laboratory	written test, practical performance evaluation	K_W11+	P7S_WG
07	Understands the need of widening his knowledge in connection with spreading of new analytical techniques in laboratory investigations and industrial control practice.	lecture, laboratory	practical performance evaluation	K_K01+	P7S_KK

Attention: Depending on the epidemic situation, verification of the achieved learning outcomes specified in the study program, in particular credits and examinations at the end of specific classes, can be implemented remotely (real-time meetings).

The syllabus of the module

Sem.	TK	The content	realized in	MEK
1	TK01	Applications of optical methods and molecular spectroscopies in analysis of chemical and biological materials as well as polymers, copolymers and polymeric composites. Advanced spectroscopic and microspectroscopic techniques in IR. Magnetic properties of the matter, electronic paramagnetic resonance, relaxation processes in EPR. Free radicals. Applications of NMR spectrometry for structural and quantitative analysis of polymers and copolymers. Scanning microscopy. Inductively coupled plasma mass spectrometry (ICP-MS), multielement analysis of materials and environmental samples. Electrophoresis as an analytical separation method. Chromatographic methods in application for polymers and macromolecular materials analysis.	W15	MEK01 MEK02 MEK03 MEK04 MEK06 MEK07
1	TK02	The laboratory experience focuses on practical utilization of analytical techniques for materals testing. Experiments designed to illustrate the principles and practices of modern instrumental techniques for the identification and characterization of organic compounds and materials. Topics include use of: electrphoresis, absorption spectroscopy and surface microscopy techniques.	L15	MEK01 MEK03 MEK04 MEK05 MEK06 MEK07

The student's effort

The type of classes	The work before classes	The participation in classes	The work after classes
Lecture (sem. 1)		contact hours: 15.00 hours/sem.	complementing/reading through notes: 3.00 hours/sem. Studying the recommended bibliography: 4.00 hours/sem.
Laboratory (sem. 1)	The preparation for a Laboratory: 2.00 hours/sem. Others: 5.00 hours/sem.	contact hours: 15.00 hours/sem.	Finishing/Making the report: 8.00 hours/sem.
Advice (sem. 1)		The participation in Advice: 2.00 hours/sem.
Credit (sem. 1)	The preparation for a Credit: 5.00 hours/sem.	The written credit: 1.00 hours/sem.

The way of giving the component module grades and the final grade

The type of classes	The way of giving the final grade
Lecture	A written test including the content of the course. The test includes theoretical part and calculation problems. The mark (OW) depends on the score gained: 3.0 (50.0%-60.0%) MP ; 3.5 (60.1%-70.0%) MP; 4.0 (70.1%-80.0%) MP; 4,5 (80.1%-90.0%) MP; 5.0 (90.1%-100%) MP. MP denotes the full score.
Laboratory	To pass the course, the student must successfully complete the laboratory experiments with positive grade. The mark obtained during each laboratory exercise is an arithmetic mean of the marks for a written/oral test, correct performance of an experiment and correct preparation of a report. The total mark in the laboratory work (OL) is calculated as arithmetic mean of the marks obtained for every exercise included in the schedule. A final mark for the laboratory is rounded according to WKZJK.
The final grade	The final mark in the module (K) is calculated according to the formula: K= w 0,5 OW + w 0,5 OL; where: OW, OL denote positive marks for lecture test and laboratory practice, respectively, w- coefficient for delay, w =1.0 when a passing mark is obtained in due course, w=0.9 for a first resit, w=0.8 for a second resit. The final mark is rounded according to WKZJK.

Sample problems

Required during the exam/when receiving the credit
(-)

Realized during classes/laboratories/projects
(-)

Others
(-)

Can a student use any teaching aids during the exam/when receiving the credit : no

The contents of the module are associated with the research profile: yes

1	Ł. Florczak; B. Pilch-Pitera; K. Pojnar; N. Roś	Low-temperature powder paint modified with graphene oxide	2024
2	Ł. Florczak; B. Kościelniak; A. Kramek; A. Sobkowiak	The Influence of Potassium Hexafluorophosphate on the Morphology and Anticorrosive Properties of Conversion Coatings Formed on the AM50 Magnesium Alloy by Plasma Electrolytic Oxidation	2023
3	D. Czachor-Jadacka; Ł. Florczak; B. Pilch-Pitera; K. Pojnar	Właściwości ochronne niskotemperaturowych poliuretanowych lakierów proszkowych na bazie żywic akrylowych	2022
4	K. Darowicki; Ł. Florczak; G. Nawrat; K. Raga; J. Ryl; J. Sieniawski; A. Sobkowiak; M. Wierzbińska	The Effect of Sodium Tetrafluoroborate on the Properties of Conversion Coatings Formed on the AZ91D Magnesium Alloy by Plasma Electrolytic Oxidation	2022
5	Ł. Florczak; S. Kozdra; P. Michałowski; M. Możdżonek; I. Opaliński; A. Wójcik	Poly (vinylidene fluoride) solid polymer electrolyte structure revealed by secondary ion mass spectrometry	2022
6	A. Baran; M. Drajewicz; A. Dryzner; M. Dubiel; Ł. Florczak; M. Kocój-Toporowska; A. Krząkała; K. Kwolek; P. Kwolek; G. Lach; G. Nawrat; Ł. Nieużyła; K. Raga; J. Sieniawski; A. Sobkowiak; T. Wieczorek	Method of Forming Corrosion Resistant Coating and Related Apparatus	2021
7	D. Czachor-Jadacka; Ł. Florczak; B. Pilch-Pitera	Właściwości ochronne niskotemperaturowych poliuretanowych lakierów proszkowych o zwiększonej hydrofobowości	2021
8	Ł. Florczak	Ocena właściwości antykorozyjnych powłok konwersyjnych wytworzonych na magnezie i jego stopach w procesie elektrolitycznego utleniania plazmowego– przegląd	2021
9	Ł. Byczyński; D. Czachor; Ł. Florczak; K. Kowalczyk; E. Pavlova; B. Pilch-Pitera; J. Wojturski	Conductive polyurethane-based powder clear coatings modified with carbon nanotubes	2019