The aim of studying and bibliography

The main aim of study: Acquiring knowledge on the modern physicochemical methods used in the analysis of medicinal products.

The general information about the module: The module takes place in the seventh semester, includes 10 hours of lecture and 20 hours laboratory. The module ends with a final test.

Bibliography required to complete the module

Bibliography used during lectures

1	Rabek J.F.	Współczesna wiedza o polimerach	PWN Warszawa.	2008
2	Schultze D.	Termiczna analiza różnicowa	PWN Warszawa.	1974
3	Kasprzycka-Gutman T.	Elementy kalorymetrii statycznej i dynamicznej	WNT Warszawa .	1993
4	Menard K.P.	Dynamic Mechanical analysis, a practical introduction	CRC Press, Boca Raton.	2008
5	Rui Y.	Analytical methods for polymer characterization	Apple Academic Press Inc. .	2018
6	Przedmojski J.	Rentgenowskie metody badawcze w inżynierii materiałowej	WNT Warszawa.	1990
7	Cullity B.D.	Elements of X-Ray Diffraction. 2nd Edition	Addison-Wesley Publishing Company Inc., Phillippines.	1978
8	Howland R., Benatar L.; tłumaczenie polskie: Woźniak M., Kozubowski J.M.	STM / AFM mikroskopy ze skanującą sondą: elementy teorii i praktyki	WIM PW, Warszawa.	2002

Bibliography used during classes/laboratories/others

1

Aktualne artykuły w czasopismach naukowych, dostępnych w PRz

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Bibliography to self-study

1

Instrukcje do ćwiczeń laboratoryjnych

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Basic requirements in category knowledge/skills/social competences

Formal requirements: Registration for the seventh semester.

Basic requirements in category knowledge: Has basic knowledge in the field of physicochemical properties of materials and instrumental analysis.

Basic requirements in category skills: Has the ability to work in an instrument laboratory and to perform calculations and interpretation of results.

Basic requirements in category social competences: Knows safety and fire protection regulation in chemical laboratory. Capable of working in team and individually.

Module outcomes

MEK	The student who completed the module	Types of classes / teaching methods leading to achieving a given outcome of teaching	Methods of verifying every mentioned outcome of teaching	Relationships with KEK	Relationships with PRK
01	Knows advanced testing methods of structure and properties of organic and inorganic materials both in a condensed state and in solution.	lecture, laboratory exercises	written test, written report, skill assessment	K_W01+ K_W08++	P6S_WG
02	Has skill ito present the results of the analysis of the properties of materials used in the pharmaceutical industry and can prepare a report.	lecture, laboratory exercises	written test, written report, skill assessment	K_U01+ K_U06++	P6S_UK P6S_UW
03	Can propose, evaluate the usefulness and apply appropriate instrumental methods to study the structure and properties of materials used in the pharmaceutical industry.	lecture, laboratory exercises	written test, written report, skill assessment	K_U01++ K_U06+++ K_U15+	P6S_UK P6S_UU P6S_UW
04	Understands the need for complement the knowledge of the new and updated methods of analysis of materials used in the production of medicinal products.	lecture, laboratory exercises	written test, written report, skill assessment	K_U15+ K_K01+++	P6S_KK P6S_UU

Attention: Depending on the epidemic situation, verification of the achieved learning outcomes specified in the study program, in particular credits and examinations at the end of specific classes, can be implemented remotely (real-time meetings).

The syllabus of the module

Sem.	TK	The content	realized in	MEK
7	TK01	Methods of thermal analysis (DSC, TM-DSC, TGA, TMA, DMA, etc.) and their application in the pharmaceutical industry.	W01, W02	MEK01 MEK03
7	TK02	Research methods using electromagnetic radiation: light scattering, X-ray methods (SAXS, WAXS), and neutron scattering. Application of synchrotron radiation.	W03, W04	MEK01 MEK03
7	TK03	Microscopic methods: optical and electron microscopy. Scanning probe microscopy.	W05	MEK01 MEK03
7	TK04	Application of the DSC method in studies of the active pharmaceutical ingredients and excipients - determination of the temperture of phase transition (including polymorphism) and purity. Compatibility testing of components used in the manufacture of medicinal products. Characterization of thermomechanical properties of materials used in the pharmaceutical industry using the DMA method. X-ray analysis of the active pharmaceutical ingredients and excipients (degree of crystallinity, polymorphism) used in the pharmaceutical industry.	L01, L02, L03, L04	MEK01 MEK02 MEK03 MEK04

The student's effort

The type of classes	The work before classes	The participation in classes	The work after classes
Lecture (sem. 7)	The preparation for a test: 5.00 hours/sem.	contact hours: 10.00 hours/sem.	complementing/reading through notes: 1.00 hours/sem. Studying the recommended bibliography: 4.00 hours/sem.
Laboratory (sem. 7)	The preparation for a Laboratory: 2.00 hours/sem. The preparation for a test: 4.00 hours/sem.	contact hours: 20.00 hours/sem.	Finishing/Making the report: 4.00 hours/sem.
Advice (sem. 7)		The participation in Advice: 2.00 hours/sem.
Credit (sem. 7)	The preparation for a Credit: 3.00 hours/sem.	The written credit: 2.00 hours/sem.

The way of giving the component module grades and the final grade

The type of classes	The way of giving the final grade
Lecture	Mark of the written test from the lectures – W1. The test mark depends on the score gained: 50,1-60%: 3.0 60,1-70%: 3.5 70,1-80%: 4.0 80,1-90%: 4.5 90,1-100%: 5.0
Laboratory	Student must perform all of the planed experiments, prepare and pass written reports, pass tests from theoretical information connected with laboratory lessons.Average mark from test, written report from each exercise, taking into account the observations of performance of each exercise – W2.
The final grade	Final mark: W = w 0,5 W1 + w 0,5 W2; w - weighting factor: w = 1,0 first term, w = 0,9 second term, w = 0,8 third term.

Sample problems

Required during the exam/when receiving the credit
(-)

Realized during classes/laboratories/projects
(-)

Others
(-)

Can a student use any teaching aids during the exam/when receiving the credit : no

The contents of the module are associated with the research profile: yes

1	J. Bieniaś; Ł. Byczyński; D. Czachor-Jadacka; M. Droździel-Jurkiewic; M. Kisiel; B. Mossety-Leszczak; G. Pietruszewska; M. Włodarska; W. Zając	Nonterminal liquid crystalline epoxy resins as structurally ordered low Tg thermosets with potential as smart polymers	2024
2	K. Awsiuk; N. Janiszewska; B. Mossety-Leszczak; J. Raczkowska; A. Strachota; B. Strachota; M. Walczak; A. Zioło	Synthesis and Morphology Characteristics of New Highly Branched Polycaprolactone PCL	2024
3	M. Kisiel; B. Mossety-Leszczak	The Effect of Nonterminal Liquid Crystalline Epoxy Resin Structure and Curing Agents on the Glass Transition of Polymer Networks	2024
4	M. Kisiel; B. Mossety-Leszczak; L. Okrasa; M. Włodarska	Modification of the Dielectric and Thermal Properties of Organic Frameworks Based on Nonterminal Epoxy Liquid Crystal with Silicon Dioxide and Titanium Dioxide	2024
5	M. Kisiel; B. Mossety-Leszczak; W. Zając	Advancements in The Cross-Linking and Morphology of Liquid Crystals	2024
6	Ł. Byczyński; D. Czachor-Jadacka; M. Kisiel; B. Mossety-Leszczak; B. Pilch-Pitera; K. Pojnar; M. Walczak; J. Wojturska	Poliuretanowy lakier proszkowy oraz sposób wytwarzania poliuretanowego lakieru proszkowego	2024
7	Ł. Byczyński; E. Ciszkowicz; D. Czachor-Jadacka; M. Kisiel; B. Mossety-Leszczak; B. Pilch-Pitera; M. Walczak; J. Wojturska	Wodna dyspersja kationomerów uretanowo-akrylowych, sposób wytwarzania wodnej dyspersji kationomerów uretanowo-akrylowych oraz sposób wytwarzania fotoutwardzalnej powłoki z wykorzystaniem tej wodnej dyspersji	2024
8	M. Kisiel; B. Mossety-Leszczak; L. Okrasa; M. Włodarska; W. Zając	Changes in molecular relaxations and network properties of a triaromatic liquid crystal epoxy resin with nonterminal functional groups	2023
9	J. Karaś; M. Kisiel; B. Mossety-Leszczak; B. Pilch-Pitera; M. Włodarska; W. Zając	The application of liquid crystalline epoxy resin for forming hybrid powder coatings	2022
10	K. Byś; J. Hodan; B. Mossety-Leszczak; E. Pavlova; A. Strachota; B. Strachota	Self-Healing and Super-Elastomeric PolyMEA-co-SMA Nanocomposites Crosslinked by Clay Platelets	2022
11	M. Kisiel; B. Mossety-Leszczak	Liquid Crystalline Polymers	2022
12	B. Mossety-Leszczak; M. Włodarska	DFT Studies of Selected Epoxies with Mesogenic Units–Impact of Molecular Structure on Electro-Optical Response	2021
13	K. Byś; B. Mossety-Leszczak; E. Pavlova; M. Steinhart; A. Strachota; B. Strachota; W. Zając	Novel Tough and Transparent Ultra-Extensible Nanocomposite Elastomers Based on Poly(2-methoxyethylacrylate) and Their Switching between Plasto-Elasticity and Viscoelasticity	2021
14	M. Kisiel; B. Mossety-Leszczak; A. Strachota; B. Strachota	Achieving structural anisotropy of liquid crystalline epoxy by manipulation with crosslinking parameters	2021
15	M. Kisiel; B. Mossety-Leszczak	Development in liquid crystalline epoxy resins and composites – A review	2020
16	M. Marchel; B. Mossety-Leszczak; M. Walczak	Maize (Zea mays) reaction in response to rubber rag additive into the soil	2020
17	S. Horodecka; D. Kaňková; B. Mossety-Leszczak; M. Netopilík; M. Šlouf; A. Strachota; B. Strachota; M. Vyroubalová; Z. Walterová; A. Zhigunov	Low-Temperature Meltable Elastomers Based on Linear Polydimethylsiloxane Chains Alpha, Omega-Terminated with Mesogenic Groups as Physical Crosslinkers: A Passive Smart Material with Potential as Viscoelastic Coupling. Part I: Synthesis and Phase Behavior	2020
18	S. Horodecka; D. Kaňková; B. Mossety-Leszczak; M. Netopilík; M. Šlouf; A. Strachota; M. Vyroubalová; A. Zhigunov	Meltable copolymeric elastomers based on polydimethylsiloxane with multiplets of pendant liquid-crystalline groups as physical crosslinker: A self-healing structural material with a potential for smart applications.	2020
19	S. Horodecka; M. Kisiel; B. Mossety-Leszczak; M. Šlouf; A. Strachota; B. Strachota	Low-Temperature-Meltable Elastomers Based on Linear Polydimethylsiloxane Chains Alpha, Omega-Terminated with Mesogenic Groups as Physical Crosslinker: A Passive Smart Material with Potential as Viscoelastic Coupling. Part II—Viscoelastic and Rheological Properties	2020
20	A. Frańczak; M. Kisiel; B. Mossety-Leszczak; D. Szczęch	Quantitative analysis of the polymeric blends	2019
21	N. Buszta; M. Kisiel; J. Lechowicz; B. Mossety-Leszczak; R. Ostatek; M. Włodarska	Analysis of curing reaction of liquid-crystalline epoxy compositions by using temperature-modulated DSC TOPEM (R)	2019