Item card
Instrumental analysis
Some basic information about the module
Cycle of education:
2022/2023
The name of the faculty organization unit:
The faculty Chemistry
The name of the field of study:
Pharmaceutical engineering
The area of study:
technical/biological sciences
The profile of studing:
The level of study:
first degree study
Type of study:
full time
discipline specialities :
The degree after graduating from university:
Bachelor of Science (BSc)
The name of the module department :
Department of Physical Chemistry
The code of the module:
12700
The module status:
mandatory for teaching programme
The position in the studies teaching programme:
sem: 5 / W30 L45 / 7 ECTS / E
The language of the lecture:
Polish
The name of the coordinator:
Dorota Naróg, PhD, Eng.
office hours of the coordinator:
poniedziałek 12.00 - 13.30
czwartek 12.00 - 13.30
semester 5:
Paweł Błoniarz, PhD, Eng. , office hours Monday 10.30 - 12.00
Tuesday 12.30-14.00
The aim of studying and bibliography
The main aim of study:
To provide students with the basic methods of instrumental analysis, construction and operation of the equipment and its use for the determination of the composition, purity of biotechnology products and materials.
The general information about the module:
The module is implemented in the 5th semester and includes 30 hours of lecture and 45 hours of laboratory. The module ends with an exam
others:
instrukcje do ćwiczeń laboratoryjnych
Bibliography required to complete the module
| 1 | A.Cygański | Metody spektroskopowe w chemii analitycznej | WNT Warszawa. | 1997 |
| 2 | E. Hoffmann, J. Charette, V. Stroobant | Spektrometria mas | WNT Warszawa. | 1998 |
| 3 | A. Cygański | Metody elektroanalityczne | WNT Warszawa. | 1995 |
| 4 | J. krysiak | Chemiczna analiza instrumentalna | PZWL. | 1999 |
| 5 | Z. Witkiewicz | Podstawy chromatografii | WNT Warszawa. | 2005 |
| 1 | W. Szczepaniak | Metody instrumentalne w analizie chemicznej | PWN Warszawa. | 2004 |
| 2 | R.M. Silverstein i inn. | Spekroskopowe metody identyfikacji związkow organicznych | PWN Warszawa. | 2007 |
| 1 | W. Szczepaniak | Metody instrumentalne w analizie chemicznej | PWN Warszawa. | 2004 |
Basic requirements in category knowledge/skills/social competences
Formal requirements:
completed course of general chemistry, analytical chemistry,and physical chemistry
Basic requirements in category knowledge:
Knowledge of physics, analytical, organic and physical chemistry.
Basic requirements in category skills:
Basic skills relating to the calculation of analyte concentration, preparing solutions
and the use of the chemical laboratory equipment.
Basic requirements in category social competences:
Knowledge of safety rules in the chemical laboratory, the responsibility required during chemical experiments performed individually and in a group.
Module outcomes
| MEK | The student who completed the module | Types of classes / teaching methods leading to achieving a given outcome of teaching | Methods of verifying every mentioned outcome of teaching | Relationships with KEK | Relationships with PRK |
|---|---|---|---|---|---|
| MEK01 | Has knowledge about theoretical foundations of the common intrumental methods of analysis, principles of operation and construction of modern analytical instrumentation. | lecture, laboratory | written test and report for every laboratory exercise, observation of performance, |
K-W02+ K-W08++ K-U06+ K-U15+ |
P6S-UU P6S-UW P6S-WG |
| MEK02 | Acquired knowlewdge on the application of the various instrumental techniques to the solution of analytical problems in experimental research, biotechnology and chemical production. | lecture | pass a final written exam |
K-W07+ K-W08++ K-U06++ |
P6S-UW P6S-WG |
| MEK03 | Able to select and justify the use of instrumental methods of analysis in terms of analytical and economic requirements. | lecture, | written test and report for every laboratory exercise, observation of performance, |
K-U01+ K-U06++ K-K03+ |
P6S-KR P6S-UK P6S-UW |
| MEK04 | Mastered the practical usage of the instrumental methods to perform chemical analyses | laboratory | written test , observation of performance, |
K-U05+ K-U06++ K-K02+ |
P6S-KO P6S-KR P6S-UW |
| MEK05 | Knows and can practically use the qualitative and quantitative methods of analysis, and calibration techniques. | lecture, laboratory | written test , observation of performance, |
K-U06+++ |
P6S-UW |
| MEK06 | Knows how to prepare a report on laboratory exercises, is able to evaluate the results and draw valid conclusions. | laboratory | written raport |
K-U01+ |
P6S-UK P6S-UW |
| MEK07 | Has ability to work independently and to interact in a team. | laboratory | observation of performance, |
K-U14++ K-K02++ K-K03++ |
P6S-KO P6S-KR P6S-UO |
| MEK08 | Knows the principles of good laboratory practice, including the principles of safety, waste collection. | laboratory | observation of performance, |
K-K02++ |
P6S-KO P6S-KR |
| MEK09 | Understands the need for continuous complement of knowledge about the new solutions and methods of instrumental analysis. | lecture, laboratory | observation of performance, |
K-K01++ |
P6S-KK |
The syllabus of the module
| Sem. | TK | The content | realized in | MEK |
|---|---|---|---|---|
| 5 | TK01 | W30 | MEK01 MEK03 MEK05 MEK09 | |
| 5 | TK02 | L45 | MEK01 MEK02 MEK03 MEK04 MEK05 MEK06 MEK07 MEK08 |
The student's effort
| The type of classes | The work before classes | The participation in classes | The work after classes |
|---|---|---|---|
| Lecture (sem. 5) | The preparation for a test:
3.00 hours/sem. |
contact hours:
30.00 hours/sem. |
complementing/reading through notes:
15.00 hours/sem. Studying the recommended bibliography: 15.00 hours/sem. |
| Laboratory (sem. 5) | The preparation for a Laboratory:
5.00 hours/sem. The preparation for a test: 20.00 hours/sem. |
contact hours:
45.00 hours/sem. |
Finishing/Making the report:
20.00 hours/sem. |
| Advice (sem. 5) | The participation in Advice:
2.00 hours/sem. |
||
| Exam (sem. 5) | The preparation for an Exam:
20.00 hours/sem. |
The written exam:
2.00 hours/sem. |
The way of giving the component module grades and the final grade
| The type of classes | The way of giving the final grade |
|---|---|
| Lecture | Written examination in the form of a test (51% of the maximum number of points is required to pass) -OE. The test includes theoretical part and calculation problems. The mark (OE) depends on the score gained: 3.0 (50.0%-60.0%) MP ; 3.5 (60.1%-70.0%) MP; 4.0 (70.1%-80.0%) MP; 4,5 (80.1%-90.0%) MP; 5.0 (90.1%-100%) MP. MP denotes the full score. |
| Laboratory | The necessary condition for receiving a credit for the laboratory is obtaining at least a passing mark on each exercise included in the schedule. The mark obtained during each laboratory exercise is an arithmetic mean of the marks for a written/oral test, correct performance of an experiment and correct preparation of a report. The total mark in the laboratory work (OL) is calculated as arithmetic mean of the marks obtained for every exercise included in the schedule. |
| The final grade | The final mark in the module (K) is calculated according to the formula: K= w 0,5 OE + w 0,5 OL; where: OE, OL denote positive marks for lecture test and laboratory practice, respectively, w - coefficient for delay, w =1.0 when a passing mark is obtained in due time, w=0.9 for a first resit, w=0.8 for a second resit. The final mark is rounded according to WKZJK. |
Sample problems
Required during the exam/when receiving the credit
(-)
Realized during classes/laboratories/projects
(-)
Others
(-)
Can a student use any teaching aids during the exam/when receiving the credit : no
The contents of the module are associated with the research profile yes
| 1 | D. Naróg; A. Sobkowiak | Electrochemistry of Flavonoids | 2023 |
| 2 | D. Naróg; A. Sobkowiak | Electrochemical Investigation of some Flavonoids in Aprotic Media | 2022 |
| 3 | D. Naróg | Electrochemical study of quercetin in the presence of galactopyranose: Potential application to the electrosynthesis of glycoconjugates of quinone/quinone methide of quercetin | 2020 |