The aim of studying and bibliography

The main aim of study: A student should obtain theoretical and practical knowledge about classic and some instrumental analytic methods. During the laboratory a student is required to perform accurate analysis according to analytical formula, carry out right calculations and statistical evaluation of results.

The general information about the module: Division of analytical chemistry, scale, accuracy and precision of the methods. Analytical errors, statistical evaluation of the results. General scheme of quantitative analysis. Division and characteristics of chemical analysis methods and selected instrumental methods. Theoretical bases of volumetric analysis. Precipitation analysis, effects accompanying solid product separation. Chemical calculations in the field of volumetric, potentiometric and spectrophotometric analysis and gravimetric methods.

Teaching materials: Instrukcje do ćwiczeń laboratoryjnych

others: Materiały pomocnicze do wykładów udostępniane na stronie internetowej koordynatora.

Bibliography required to complete the module

Bibliography used during lectures

1	Skoog D.A., West D.M., Holler F.J., Crouch S.R.	Podstawy chemii analitycznej	PWN Warszawa .	2007
2	Kopacz M.	Chemia analityczna, podstawy teoretyczne analizy ilościowej	Oficyna Wydawnicza Politechniki Rzeszowskiej, Rzeszów.	1997
3	Minczewski J., Marczenko Z.	Chemia analityczna, t. I i II.	PWN, Warszawa.	1997

Bibliography used during classes/laboratories/others

1	Minczewski J., Marczenko Z.	Chemia analityczna t. II	PWN Warszawa.	1997
2	Praca zbiorowa pod red. Z. Galusa	Ćwiczenia rachunkowe z chemii analitycznej	PWN, Warszawa.	1996
3	Praca zbiorowa pod red. M. Kopacz	Ćwiczenia laboratoryjne i rachunkowe z analizy ilościowej	Oficyna Wydawnicza Politechniki Rzeszowskiej, Rzeszów.	1999

Bibliography to self-study

1

Kealey D. , Haines P.J.

Chemia analityczna, krótkie wykłady

PWN, Warszawa .

2006

Basic requirements in category knowledge/skills/social competences

Formal requirements: Registration for semester 3

Basic requirements in category knowledge: Basic knowledge of general and inorganic chemistry and mathematics.

Basic requirements in category skills: Manual skills necessary to execution of simple chemical analyses. Knowledge of basic laboratory equipment.

Basic requirements in category social competences: Knowledge of basic in health and safety-at-work legislation and fire regulations currently in force in chemical laboratory. Awareness of harmful influence of chemicals on human body and the environmen

Module outcomes

MEK	The student who completed the module	Types of classes / teaching methods leading to achieving a given outcome of teaching	Methods of verifying every mentioned outcome of teaching	Relationships with KEK	Relationships with PRK
01	Has a knowledge in chemical analysis methods: volumetric and precipitation analysis.	lecture, laboratory	written tests, evaluation of accuracy performed determinations	K_W01+++ K_W08++	P6S_WG
02	Has a knowledge in division of analytical chemistry, general scheme of quantitative analysis, division and characteristics of chemical analysis methods and selected instrumental methods.	lecture	written test	K_W02+++	P6S_WG
03	Can characterize accuracy and precision of the analytical methods, estimates analytical errors and makes statistical evaluation of the results.	lecture, laboratory	written test, report	K_U05+++ K_K03+++	P6S_KR P6S_UW
04	Student is knowledgeable about contemporary theories of acids and bases, protolytic solvents, equilibrium constants. solubility and solubility product; effects accompanying solid product separation.	lecture	written test	K_W01+++	P6S_WG
05	Has basic knowledge about selected instrument al methods.	lecture, laboratory	test	K_U05+++	P6S_UW
06	Has ability to work in a small, laboratory team.	laboratory	observation	K_K03+++	P6S_KR
07	Student should to comply with principles of safety in chemical laboratory, especially with toxic, caustic and flammable chemicals.	laboratory	observation	K_U14++ K_K02+++	P6S_KO P6S_KR P6S_UO
08	Can carry out a chemical experiment, perform calculations and is able to describe the results and conclusions.	laboratory	observation, written report, written test	K_U06+ K_U14+++ K_K03+++	P6S_KR P6S_UO P6S_UW

Attention: Depending on the epidemic situation, verification of the achieved learning outcomes specified in the study program, in particular credits and examinations at the end of specific classes, can be implemented remotely (real-time meetings).

The syllabus of the module

Sem.	TK	The content	realized in	MEK
3	TK01	Division of analytical chemistry, scale, accuracy and precision of the methods. General scheme of quantitative analysis. Analytical errors, statistical evaluation of results. Methods of separation and concentration. Division and characteristics of chemical analysis methods. Contemporary theories of acids and bases, protolytic solvents, equilibrium constants. solubility and solubility product. Theoretical bases of volumetric analysis: acid-base, oxidation-reduction and complexation titrations, . Precipitation analysis, effects accompanying solid product separation. Division and characteristics selected instrumental methods. Chemical calculations in the field of volumetric and gravimetric methods.	wykład	MEK01 MEK02 MEK03 MEK04 MEK05
3	TK02	Acid-base titration. Preparation of NaOH solution. Adjustment of NaOH titre.	L01, L02, L03	MEK01 MEK06 MEK07 MEK08
3	TK03	Oxidation-reduction titration. Preparation and adjustment of Na2S2O3 solution titre. Testing analysis: determination of Cu2+ content.	L04, L05	MEK01 MEK06 MEK07 MEK08
3	TK04	Complexation titration. Preparation of EDTA solution. Testing analysis: determination of Ca(II) or Mg(II) content.	L06	MEK01 MEK06 MEK07 MEK08
3	TK05	Determination of: iron(III) by spectrophotometric and NaOH + Na2CO3 by potentiometric methods.	L7, L8	MEK05 MEK06 MEK07 MEK08
3	TK06	Calculations in analytical analysis.	L01-L8	MEK03 MEK08

The student's effort

The type of classes	The work before classes	The participation in classes	The work after classes
Lecture (sem. 3)		contact hours: 15.00 hours/sem.	complementing/reading through notes: 5.00 hours/sem. Studying the recommended bibliography: 8.00 hours/sem.
Laboratory (sem. 3)	The preparation for a Laboratory: 5.00 hours/sem. The preparation for a test: 10.00 hours/sem.	contact hours: 30.00 hours/sem.	Finishing/Making the report: 5.00 hours/sem.
Advice (sem. 3)
Credit (sem. 3)

The way of giving the component module grades and the final grade

The type of classes	The way of giving the final grade
Lecture	written test (OW)
Laboratory	five written tests during semester. Evaluation of accuracy performed determinations - OL. OL depends on test evaluations (50%) and determinations (50%)
The final grade	final grade OK = 0,4 wOW + 0,6wOL Where:OW and OL - positive evaluation of the lecture and lab; w - factor related to the time of credit or examination, w= 1.0 first term, w = 0.9 second term , w = 0.8 third term. The grade is rounded according to WKZJK

Sample problems

Required during the exam/when receiving the credit
(-)

Realized during classes/laboratories/projects
(-)

Others
(-)

Can a student use any teaching aids during the exam/when receiving the credit : no

The contents of the module are associated with the research profile: yes

1	B. Guratowska; A. Kuźniar; J. Nizioł; A. Nowak; M. Okrasa; T. Ruman; M. Ryngajłło; J. Szulc	Uncontrolled Post-Industrial Landfill—Source of Metals, Potential Toxic Compounds, Dust, and Pathogens in Environment—A Case Study	2024
2	J. Kalembkiewicz; A. Kuźniar; B. Papciak; E. Sočo	Zastosowanie materiału krzemionkowego modyfikowanego surfaktantem do immobilizacji moryny	2023
3	S. Kuberski; A. Kuźniar; J. Nizioł; A. Nowak; I. Nowak; M. Okrasa; T. Ruman; B. Szponar; J. Szulc	Biological and chemical contamination of illegal, uncontrolled refuse storage areas in Poland	2023
4	Ł. Byczyński; M. Huta; A. Kuźniar; E. Sočo	Badania produktów sulfonowania kwercetyny	2023
5	M. Dranka; J. Kalembkiewicz; D. Kamiński; A. Kozioł; A. Kuźniar; U. Maciołek; L. Mazur; E. Mendyk	Structural and spectroscopic studies of Na+ – Quercetin-5′-sulfonic acid polymeric complexes obtained via solvothermal synthesis	2022
6	A. Hałoń; D. Ksiądzyna; A. Kuźniar; A. Matuszewska; A. Merwid-Ląd; B. Nowak; T. Sozański; M. Szandruk-Bender; A. Szeląg; D. Szkudlarek; M. Trocha	Morin-5′-Sulfonic Acid Sodium Salt (NaMSA) Attenuates Cyclophosphamide-Induced Histological Changes in Genitourinary Tract in Rats—Short Report	2021
7	A. Kuźniar; U. Maciołek; E. Pieniążek; J. Pusz; E. Sočo; E. Woźnicka	Związek kwasu kwercetyno-5’-sulfonowego z jonami sodu. Synteza, właściwości, zastosowanie	2021
8	E. Ciszkowicz; M. Kosińska-Pezda; A. Kuźniar; K. Lecka-Szlachta; E. Pieniążek; E. Woźnicka; L. Zapała	Synteza, charakterystyka i właściwości biologiczne kompleksów jonów antanowców lekkich z 3-hydroksyflawonem	2021
9	A. Czerwonka; J. Kafałut; A. Kuźniar; U. Maciołek; E. Mendyk; W. Rzeski	Anticancer effects of sodium and potassium quercetin-5’-sulfonates through inhibition of proliferation, induction of apoptosis, and cell cycle arrest in the HT-29 human adenocarcinoma cell line	2020
10	J. Kalembkiewicz; A. Kuźniar; B. Papciak; J. Pusz; E. Sitarz-Palczak; E. Sočo; E. Woźnicka	Pierwiastki i związki chemiczne	2020
11	J. Kalembkiewicz; A. Kuźniar; E. Pieniążek; E. Sočo; E. Woźnicka	Aktywność biochemiczna sulfonowych pochodnych moryny	2020
12	M. Kopacz; A. Kuźniar; B. Papciak; J. Pusz; E. Woźnicka	Badania reakcji kompleksowania chryzyny z jonami Nd(III), Tb(III) i Dy(III) w roztworach wodno-metanolowych	2020