Item card
Analytical chemistry
Some basic information about the module
Cycle of education:
2022/2023
The name of the faculty organization unit:
The faculty Chemistry
The name of the field of study:
Pharmaceutical engineering
The area of study:
technical/biological sciences
The profile of studing:
The level of study:
first degree study
Type of study:
full time
discipline specialities :
The degree after graduating from university:
Bachelor of Science (BSc)
The name of the module department :
Department of Inorganic and Analytical Chemistry
The code of the module:
12679
The module status:
mandatory for teaching programme
The position in the studies teaching programme:
sem: 3 / W15 L30 / 3 ECTS / Z
The language of the lecture:
Polish
The name of the coordinator:
Anna Kuźniar, PhD, Eng.
The aim of studying and bibliography
The main aim of study:
A student should obtain theoretical and practical knowledge about classic and some instrumental analytic methods. During the laboratory a student is required to perform accurate analysis according to analytical formula, carry out right calculations and statistical evaluation of results.
The general information about the module:
Division of analytical chemistry, scale, accuracy and precision of the methods. Analytical errors, statistical evaluation of the results. General scheme of quantitative analysis. Division and characteristics of chemical analysis methods and selected instrumental methods. Theoretical bases of volumetric analysis. Precipitation analysis, effects accompanying solid product separation. Chemical calculations in the field of volumetric, potentiometric and spectrophotometric analysis and gravimetric methods.
Teaching materials:
Instrukcje do ćwiczeń laboratoryjnych
others:
Materiały pomocnicze do wykładów udostępniane na stronie internetowej koordynatora.
Bibliography required to complete the module
| 1 | Skoog D.A., West D.M., Holler F.J., Crouch S.R. | Podstawy chemii analitycznej | PWN Warszawa . | 2007 |
| 2 | Kopacz M. | Chemia analityczna, podstawy teoretyczne analizy ilościowej | Oficyna Wydawnicza Politechniki Rzeszowskiej, Rzeszów. | 1997 |
| 3 | Minczewski J., Marczenko Z. | Chemia analityczna, t. I i II. | PWN, Warszawa. | 1997 |
| 1 | Minczewski J., Marczenko Z. | Chemia analityczna t. II | PWN Warszawa. | 1997 |
| 2 | Praca zbiorowa pod red. Z. Galusa | Ćwiczenia rachunkowe z chemii analitycznej | PWN, Warszawa. | 1996 |
| 3 | Praca zbiorowa pod red. M. Kopacz | Ćwiczenia laboratoryjne i rachunkowe z analizy ilościowej | Oficyna Wydawnicza Politechniki Rzeszowskiej, Rzeszów. | 1999 |
| 1 | Kealey D. , Haines P.J. | Chemia analityczna, krótkie wykłady | PWN, Warszawa . | 2006 |
Basic requirements in category knowledge/skills/social competences
Formal requirements:
Registration for semester 3
Basic requirements in category knowledge:
Basic knowledge of general and inorganic chemistry and mathematics.
Basic requirements in category skills:
Manual skills necessary to execution of simple chemical analyses. Knowledge of basic laboratory equipment.
Basic requirements in category social competences:
Knowledge of basic in health and safety-at-work legislation and fire regulations currently in force in chemical laboratory. Awareness of harmful influence of chemicals on human body and the environmen
Module outcomes
| MEK | The student who completed the module | Types of classes / teaching methods leading to achieving a given outcome of teaching | Methods of verifying every mentioned outcome of teaching | Relationships with KEK | Relationships with PRK |
|---|---|---|---|---|---|
| MEK01 | Has a knowledge in chemical analysis methods: volumetric and precipitation analysis. | lecture, laboratory | written tests, evaluation of accuracy performed determinations |
K-W01+++ K-W08++ |
P6S-WG |
| MEK02 | Has a knowledge in division of analytical chemistry, general scheme of quantitative analysis, division and characteristics of chemical analysis methods and selected instrumental methods. | lecture | written test |
K-W02+++ |
P6S-WG |
| MEK03 | Can characterize accuracy and precision of the analytical methods, estimates analytical errors and makes statistical evaluation of the results. | lecture, laboratory | written test, report |
K-U05+++ K-K03+++ |
P6S-KR P6S-UW |
| MEK04 | Student is knowledgeable about contemporary theories of acids and bases, protolytic solvents, equilibrium constants. solubility and solubility product; effects accompanying solid product separation. | lecture | written test |
K-W01+++ |
P6S-WG |
| MEK05 | Has basic knowledge about selected instrument al methods. | lecture, laboratory | test |
K-U05+++ |
P6S-UW |
| MEK06 | Has ability to work in a small, laboratory team. | laboratory | observation |
K-K03+++ |
P6S-KR |
| MEK07 | Student should to comply with principles of safety in chemical laboratory, especially with toxic, caustic and flammable chemicals. | laboratory | observation |
K-U14++ K-K02+++ |
P6S-KO P6S-KR P6S-UO |
| MEK08 | Can carry out a chemical experiment, perform calculations and is able to describe the results and conclusions. | laboratory | observation, written report, written test |
K-U06+ K-U14+++ K-K03+++ |
P6S-KR P6S-UO P6S-UW |
The syllabus of the module
| Sem. | TK | The content | realized in | MEK |
|---|---|---|---|---|
| 3 | TK01 | wykład | MEK01 MEK02 MEK03 MEK04 MEK05 | |
| 3 | TK02 | L01, L02, L03 | MEK01 MEK06 MEK07 MEK08 | |
| 3 | TK03 | L04, L05 | MEK01 MEK06 MEK07 MEK08 | |
| 3 | TK04 | L06 | MEK01 MEK06 MEK07 MEK08 | |
| 3 | TK05 | L7, L8 | MEK05 MEK06 MEK07 MEK08 | |
| 3 | TK06 | L01-L8 | MEK03 MEK08 |
The student's effort
| The type of classes | The work before classes | The participation in classes | The work after classes |
|---|---|---|---|
| Lecture (sem. 3) | contact hours:
15.00 hours/sem. |
complementing/reading through notes:
5.00 hours/sem. Studying the recommended bibliography: 8.00 hours/sem. |
|
| Laboratory (sem. 3) | The preparation for a Laboratory:
5.00 hours/sem. The preparation for a test: 10.00 hours/sem. |
contact hours:
30.00 hours/sem. |
Finishing/Making the report:
5.00 hours/sem. |
| Advice (sem. 3) | |||
| Credit (sem. 3) |
The way of giving the component module grades and the final grade
| The type of classes | The way of giving the final grade |
|---|---|
| Lecture | written test (OW) |
| Laboratory | five written tests during semester. Evaluation of accuracy performed determinations - OL. OL depends on test evaluations (50%) and determinations (50%) |
| The final grade | final grade OK = 0,4 wOW + 0,6wOL Where:OW and OL - positive evaluation of the lecture and lab; w - factor related to the time of credit or examination, w= 1.0 first term, w = 0.9 second term , w = 0.8 third term. The grade is rounded according to WKZJK |
Sample problems
Required during the exam/when receiving the credit
(-)
Realized during classes/laboratories/projects
(-)
Others
(-)
Can a student use any teaching aids during the exam/when receiving the credit : no
The contents of the module are associated with the research profile yes
| 1 | B. Guratowska; A. Kuźniar; J. Nizioł; A. Nowak; M. Okrasa; T. Ruman; M. Ryngajłło; J. Szulc | Uncontrolled Post-Industrial Landfill—Source of Metals, Potential Toxic Compounds, Dust, and Pathogens in Environment—A Case Study | 2024 |
| 2 | J. Kalembkiewicz; A. Kuźniar; B. Papciak; E. Sočo | Zastosowanie materiału krzemionkowego modyfikowanego surfaktantem do immobilizacji moryny | 2023 |
| 3 | S. Kuberski; A. Kuźniar; J. Nizioł; A. Nowak; I. Nowak; M. Okrasa; T. Ruman; B. Szponar; J. Szulc | Biological and chemical contamination of illegal, uncontrolled refuse storage areas in Poland | 2023 |
| 4 | Ł. Byczyński; M. Huta; A. Kuźniar; E. Sočo | Badania produktów sulfonowania kwercetyny | 2023 |
| 5 | M. Dranka; J. Kalembkiewicz; D. Kamiński; A. Kozioł; A. Kuźniar; U. Maciołek; L. Mazur; E. Mendyk | Structural and spectroscopic studies of Na+ – Quercetin-5′-sulfonic acid polymeric complexes obtained via solvothermal synthesis | 2022 |
| 6 | A. Hałoń; D. Ksiądzyna; A. Kuźniar; A. Matuszewska; A. Merwid-Ląd; B. Nowak; T. Sozański; M. Szandruk-Bender; A. Szeląg; D. Szkudlarek; M. Trocha | Morin-5′-Sulfonic Acid Sodium Salt (NaMSA) Attenuates Cyclophosphamide-Induced Histological Changes in Genitourinary Tract in Rats—Short Report | 2021 |
| 7 | A. Kuźniar; U. Maciołek; E. Pieniążek; J. Pusz; E. Sočo; E. Woźnicka | Związek kwasu kwercetyno-5’-sulfonowego z jonami sodu. Synteza, właściwości, zastosowanie | 2021 |
| 8 | E. Ciszkowicz; M. Kosińska-Pezda; A. Kuźniar; K. Lecka-Szlachta; E. Pieniążek; E. Woźnicka; L. Zapała | Synteza, charakterystyka i właściwości biologiczne kompleksów jonów antanowców lekkich z 3-hydroksyflawonem | 2021 |
| 9 | A. Czerwonka; J. Kafałut; A. Kuźniar; U. Maciołek; E. Mendyk; W. Rzeski | Anticancer effects of sodium and potassium quercetin-5’-sulfonates through inhibition of proliferation, induction of apoptosis, and cell cycle arrest in the HT-29 human adenocarcinoma cell line | 2020 |
| 10 | J. Kalembkiewicz; A. Kuźniar; B. Papciak; J. Pusz; E. Sitarz-Palczak; E. Sočo; E. Woźnicka | Pierwiastki i związki chemiczne | 2020 |
| 11 | J. Kalembkiewicz; A. Kuźniar; E. Pieniążek; E. Sočo; E. Woźnicka | Aktywność biochemiczna sulfonowych pochodnych moryny | 2020 |
| 12 | M. Kopacz; A. Kuźniar; B. Papciak; J. Pusz; E. Woźnicka | Badania reakcji kompleksowania chryzyny z jonami Nd(III), Tb(III) i Dy(III) w roztworach wodno-metanolowych | 2020 |