The aim of studying and bibliography

The main aim of study: The student should have a theoretical knowledge and practical skills from the area of the classic chemical analysis methods.

The general information about the module: Classification of analytical chemistry, scale, accuracy and precision of a method. Analytical errors, statistical evaluation of results. General scheme of quantitative analysis. Classification and characteristics of methods of chemical analysis. Theoretical basis of volumetric analysis. Calculations and analysis in the field of volumetric analysis and gravimetric methods.

Teaching materials: Instrukcje do ćwiczeń.

Bibliography required to complete the module

Bibliography used during lectures

1	D. Kealey, P.J. Haines	Chemia analityczna, krótkie wykłady	PWN, Warszawa.	2006.
2	J. Minczewski, Z. Marczenko	Chemia analityczna, t. I i II	PWN, Warszawa .	1997.
3	M. Kopacz	Chemia analityczna, podstawy teoretyczne analizy ilościowej	Oficyna Wydawnicza Politechniki Rzeszowskiej, Rzeszów.	1997.

Bibliography used during classes/laboratories/others

1	J. Minczewski, Z. Marczenko	, Chemia analityczna, t. II.	PWN, Warszawa.	1997.
2	Praca zbiorowa pod red. Z. Galusa	Ćwiczenia rachunkowe z chemii analitycznej	PWN, Warszawa.	1996.

Basic requirements in category knowledge/skills/social competences

Formal requirements: Registration for the given semester.

Basic requirements in category knowledge: Basic theoretical and practical knowledge in the area of general and inorganic chemistry.

Basic requirements in category skills: Basic manual skills necessary to the realization of simple chemical analyses. The knowledge of basic equipment applied in the chemical laboratory.

Basic requirements in category social competences: The knowledge of the basic of BHP and anti-fire rules in the chemical laboratory. Consciousness of the dangerous influences of chemical substances on organism and natural environment.

Module outcomes

MEK	The student who completed the module	Types of classes / teaching methods leading to achieving a given outcome of teaching	Methods of verifying every mentioned outcome of teaching	Relationships with KEK	Relationships with PRK
01	The student should have a theoretical knowledge in the area of the classic methods of chemical analysis: volumetric methods and gravimetric analysis.	lecture	the written test	K_W04++ K_U06++ K_K01++	P6S_KK P6S_KR P6S_UU P6S_WG
02	Student should perform the analysis according to the definite analytic procedure in the area of the classic chemical analysis.	laboratory	the colloquium
03	Student should know how to calculate and interpret the results of analyse.	lecture, laboratory	the colloquium
04	Student be able to co-operate and work in the laboratory group in the studio of analytic chemistry.	laboratory	observation of performance	K_K03++	P6S_KR

Attention: Depending on the epidemic situation, verification of the achieved learning outcomes specified in the study program, in particular credits and examinations at the end of specific classes, can be implemented remotely (real-time meetings).

The syllabus of the module

Sem.	TK	The content	realized in	MEK
3	TK01	Classification of analytical chemistry, scale, accuracy and precision of a method. Analytical errors, statistical evaluation of results. General scheme of quantitative analysis. Classification and characteristics of methods of chemical analysis. Theoretical basis of volumetric analysis. Alkacymetric. Reductometry and oxidimetry. Complexometry. Precipitation analysis, effects accompanying solid product separation. Chemical calculations and analyses in the field of volumetric and gravimetric methods.	wykład, laboratorium	MEK01
3	TK02	Alkacymetric: determination of sulphuric acid concentration.	L01,L02	MEK02 MEK04
3	TK03	Redox: determination of Fe(II) in Mohr’s salt, determination of Cu(II) concentration.	L03,L04	MEK02 MEK04
3	TK04	Complexometry: determination of Ca(II) or Mg(II) ionic concentrations.	L05	MEK02 MEK04
3	TK05	Precipitation analysis: determination of Cl- ions concentration.	L06	MEK02 MEK04
3	TK06	Chemical calculations in the field of volumetric analysis and gravimetric methods.	L01,L02,L03,L04,L05,L06	MEK03

The student's effort

The type of classes	The work before classes	The participation in classes	The work after classes
Lecture (sem. 3)	The preparation for a test: 15.00 hours/sem.	contact hours: 9.00 hours/sem.	complementing/reading through notes: 5.00 hours/sem. Studying the recommended bibliography: 10.00 hours/sem.
Laboratory (sem. 3)		contact hours: 18.00 hours/sem.
Advice (sem. 3)		The participation in Advice: 2.00 hours/sem.
Credit (sem. 3)	The preparation for a Credit: 15.00 hours/sem.	The written credit: 1.00 hours/sem.

The way of giving the component module grades and the final grade

The type of classes	The way of giving the final grade
Lecture
Laboratory
The final grade	The final score from the object (K) is counted according to the example K = 0,5wW + 0,5wL; where w-factor related w=1,0 (first term), w=0,9 (second term), w=0,8 (third term). The grade is rounded according to WKZJK.

Sample problems

Required during the exam/when receiving the credit
(-)

Realized during classes/laboratories/projects
Analiza objętościowa-zagadnienuia do kolokwium.pdf

Others
(-)

Can a student use any teaching aids during the exam/when receiving the credit : no

The contents of the module are associated with the research profile: yes

1	Ł. Byczyński; M. Kosińska-Pezda; E. Woźnicka; L. Zapała; W. Zapała	Synteza oraz badania składu i właściwości związków: 3-hydroksyflawonu, chryzyny oraz sulfonowych pochodnych chryzyny i kwercetyny z jonami Mn(II)	2023
2	E. Ciszkowicz; M. Kosińska-Pezda; K. Lecka-Szlachta; A. Miłoś; E. Woźnicka; L. Zapała	Analiza właściwości antybakteryjnych oraz cytotoksyczności kompleksów jonów Co(II), Mn(II) oraz Zn(II) z chryzyną oraz 3-hydroksyflawonem	2022
3	M. Kosińska-Pezda; E. Woźnicka; L. Zapała	Synteza i charakterystyka spektroskopowa kompleksów jonów lantanowców ciężkich z 3-hydroksyflawonem	2022
4	M. Kosińska-Pezda; U. Maciołek; E. Woźnicka; L. Zapała	Kompleksy 3-hydroksyflawonu z jonami Zn(II) - synteza i właściwości związków	2022
5	M. Kosińska-Pezda; U. Maciołek; E. Woźnicka; L. Zapała; W. Zapała	Synteza, badania składu i właściwości spektroskopowych kompleksów wybranych jonów metali przejściowych z kwasem niflumowym	2022
6	A. Kuźniar; U. Maciołek; E. Pieniążek; J. Pusz; E. Sočo; E. Woźnicka	Związek kwasu kwercetyno-5’-sulfonowego z jonami sodu. Synteza, właściwości, zastosowanie	2021
7	E. Ciszkowicz; K. Lecka-Szlachta; J. Pusz; E. Woźnicka	Antybakteryjna aktywność sulfonowych pochodnych chryzyny	2021
8	E. Ciszkowicz; M. Kosińska-Pezda; A. Kuźniar; K. Lecka-Szlachta; E. Pieniążek; E. Woźnicka; L. Zapała	Synteza, charakterystyka i właściwości biologiczne kompleksów jonów antanowców lekkich z 3-hydroksyflawonem	2021
9	J. Kalembkiewicz; M. Kosińska-Pezda; J. Pusz; E. Woźnicka; L. Zapała	Badania równowagi reakcji kompleksowania chryzyny z jonami Er(III) w układach: woda - metanol i woda - metanol - 1,4-dioksan	2021
10	Ł. Byczyński; E. Ciszkowicz; M. Kosińska-Pezda; K. Lecka-Szlachta; U. Maciołek; E. Woźnicka; L. Zapała; W. Zapała	Green synthesis of niflumic acid complexes with some transition metal ions (Mn(II), Fe(III), Co(II), Ni(II), Cu(II) and Zn(II)). Spectroscopic, thermoanalytical and antibacterial studies	2021
11	Ł. Byczyński; M. Kosińska-Pezda; U. Maciołek; E. Woźnicka; L. Zapała; W. Zapała	Thermal study, temperature diffraction patterns and evolved gas analysis during pyrolysis and oxidative decomposition of novel ternary complexes of light lanthanides with mefenamic acid and 1,10-phenanthroline	2021
12	J. Kalembkiewicz; A. Kuźniar; B. Papciak; J. Pusz; E. Sitarz-Palczak; E. Sočo; E. Woźnicka	Pierwiastki i związki chemiczne	2020
13	J. Kalembkiewicz; A. Kuźniar; E. Pieniążek; E. Sočo; E. Woźnicka	Aktywność biochemiczna sulfonowych pochodnych moryny	2020
14	J. Kalembkiewicz; B. Papciak; J. Pusz; E. Sitarz-Palczak; E. Woźnicka	Roztwory i procesy w roztworach	2020
15	M. Kopacz; A. Kuźniar; B. Papciak; J. Pusz; E. Woźnicka	Badania reakcji kompleksowania chryzyny z jonami Nd(III), Tb(III) i Dy(III) w roztworach wodno-metanolowych	2020
16	M. Kosińska-Pezda; E. Pieniążek; E. Woźnicka; L. Zapała	Badania stałych produktów reakcji jonów Ag(I) i Cu(II) z 3-hydroksyflawonem i moryną	2020
17	M. Kosińska; E. Woźnicka; L. Zapała; W. Zapała	Response of the DFT study to the calculations of selected microdissociation constants of anthranilic acid and its derivatives	2019
18	Ł. Byczyński; M. Chutkowski; E. Ciszkowicz; M. Kosińska; K. Lecka-Szlachta; E. Woźnicka; L. Zapała; W. Zapała	Comparison of spectral and thermal properties and antibacterial activity of new binary and ternary complexes of Sm(III), Eu(III) and Gd (III) ions with N-phenylanthranilic acid and 1,10-phenanthroline	2019