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Surfactants and detergents in pharmaceutical industry

Some basic information about the module

Cycle of education: 2022/2023

The name of the faculty organization unit: The faculty Chemistry

The name of the field of study: Chemical Technology

The area of study: technical sciences

The profile of studing:

The level of study: second degree study

Type of study: past time

discipline specialities : Chemical analysis in industry and environment, Engineering of polymer materials, Organic and polymer technology , Product and ecological process engineering, Technology of medicinal products

The degree after graduating from university: Master of Science (MSc)

The name of the module department : Department of Technology and Materials Chemistry

The code of the module: 10542

The module status: mandatory for the speciality Technology of medicinal products

The position in the studies teaching programme: sem: 2 / W9 L9 / 2 ECTS / Z

The language of the lecture: Polish

The name of the coordinator: Prof. Wiktor Bukowski, DSc, PhD, Eng.

semester 2: Agnieszka Bukowska, DSc, PhD, Eng.

The aim of studying and bibliography

The main aim of study: Familiarizing students with the problems of production of surface-active substances and their use in pharmaceutical industry.

The general information about the module: The module is carried out in the secondsemester. It includes 15 hours of lecture and 15 hours laboratory.

Teaching materials: Instrukcje laboratoryjne

Bibliography required to complete the module
Bibliography used during lectures
1 Farn R. (ed.) Chemistry and Technology of Surfactants Blackwell Publishing. 2006
2 Tadros T.F. Applied Surfactants Wiley-VCH. 2005
3 Ogonowski J., Tomaszkiewicz-Potępa Związki powierzchniowo czynne Wydawnictwo Politechniki Krakowskiej. 1999

Basic requirements in category knowledge/skills/social competences

Formal requirements: Registration for the second semester.

Basic requirements in category knowledge: Knowledge of the basic technological operations. Knowledge of the fundamentals of organic and physical chemistry.

Basic requirements in category skills: Ability to apply basic laboratory techniques.

Basic requirements in category social competences: Awareness of the need to work in teams of 2-3 people.

Module outcomes

MEK The student who completed the module Types of classes / teaching methods leading to achieving a given outcome of teaching Methods of verifying every mentioned outcome of teaching Relationships with KEK Relationships with PRK
01 Student has a basic knowledge of the raw materials used for production of surface-active agents and their processing to produce different classes of surfactants. lecture, laboratory written test, oral test K_W05+
K_W07+
K_W09+
P7S_WG
02 Student has basic knowledge of the physical and chemical phenomena carrying out with surfactants participation. lecture, laboratory written test, oral test K_W05+
P7S_WG
03 Student knows basic directions of the use of surfactants in pharmaceutical industry. lecture, laboratory written test, oral test, written report K_W05+
P7S_WG
04 Student is able to perform an experiment with surfactants, in particular those which are prepared from natural raw materials, characterize the selected surface active compounds and apply their in an composition. laboratory observation of performance, written report K_U03+
K_U06+
P7S_UK
P7S_UW
05 Student is able to work in a team conducting experiments with surfactants. laboratory observation of performance K_K02+
P7S_KO

Attention: Depending on the epidemic situation, verification of the achieved learning outcomes specified in the study program, in particular credits and examinations at the end of specific classes, can be implemented remotely (real-time meetings).

The syllabus of the module

Sem. TK The content realized in MEK
2 TK01 Introduction to surfactant chemistry. Basic terminology and surfactant clasification, Surfactant market. W01, W02 MEK01 MEK02
2 TK02 Selected topics from the theory of surfactants. Micelles and critical micelle concentration. Micellar systems in pharmaceutical industry. W03, W04 MEK02
2 TK03 Raw materials and methods of production of ionic surfactants (anionic, cationic and amphoteric). W05-W07 MEK01
2 TK04 Nonionic surfactants. W08 MEK01 MEK03
2 TK05 Microemulsions and emulsions. W09-W11 MEK01 MEK02 MEK03
2 TK06 Aerosols. W12 MEK01 MEK02 MEK03
2 TK07 Foams. W13 MEK01 MEK02 MEK03
2 TK08 Polymers and polymer gels. W14 MEK02 MEK03
2 TK09 Exercises selected from the topics: Emulsions o/w and w/o. Production of medicinal soaps. Exploration of foaming properties of pharmaceutical preparations, Medicinal liniments L01-L03 MEK04 MEK05

The student's effort

The type of classes The work before classes The participation in classes The work after classes
Lecture (sem. 2) contact hours: 9.00 hours/sem.
complementing/reading through notes: 5.00 hours/sem.
Studying the recommended bibliography: 5.00 hours/sem.
Laboratory (sem. 2) The preparation for a Laboratory: 2.00 hours/sem.
The preparation for a test: 6.00 hours/sem.
contact hours: 9.00 hours/sem.
Finishing/Making the report: 5.00 hours/sem.
Advice (sem. 2)
Credit (sem. 2) The preparation for a Credit: 15.00 hours/sem.
The written credit: 1.00 hours/sem.

The way of giving the component module grades and the final grade

The type of classes The way of giving the final grade
Lecture Positive mark of the written test. 0-50% point.- 2,0, 50-60% point.. – 3.0, 60-70% point. 3.5, 70-80% point. – 4.0, 80-90% point. – 4.5, 90-100% point. – 5.0
Laboratory Student must conduct all of the planed experiments, prepare and pass written reports, pass tests from theoretical information connected with exepriments.
The final grade The final grade (K): K = 0.5E + 0.5wL where E, L - positive grade of the exam and laboratory, respectively w – a coefficient, w = 1.0 for the first term, 0.9 for the second term and 0.8 for the third term.

Sample problems

Required during the exam/when receiving the credit
(-)

Realized during classes/laboratories/projects
(-)

Others
(-)

Can a student use any teaching aids during the exam/when receiving the credit : no

The contents of the module are associated with the research profile: yes

1 K. Bester; A. Bukowska; W. Bukowski; A. Kawka; M. Pytel Salophen chromium(III) complexes functionalized with pyridinium salts as catalysts for carbon dioxide cycloaddition to epoxides 2024
2 K. Bester; A. Bukowska; W. Bukowski; M. Drajewicz; K. Dychtoń; R. Ostatek; P. Szałański Sposób wytwarzania salofenowego kompleksu chromu(III) 2024
3 K. Bester; A. Bukowska; W. Bukowski; S. Flaga Reactive Polymer Composite Microparticles Based on Glycidyl Methacrylate and Magnetite Nanoparticles 2024
4 K. Bester; A. Bukowska; W. Bukowski; M. Drajewicz; K. Dychtoń; R. Ostatek; P. Szałański Ligand salphenowy oraz sposób syntezy tego ligandu salphenowego 2023
5 K. Bester; W. Bukowski; M. Kaczmarek; D. Tomczyk Electrocatalytic Properties of Ni(II) Schiff Base Complex Polymer Films 2022
6 K. Bester; W. Bukowski; P. Seliger; D. Tomczyk The Influence of Electrolyte Type on Kinetics of Redox Processes in the Polymer Films of Ni(II) Salen-Type Complexes 2022
7 K. Bester; A. Bukowska; W. Bukowski Homogeniczny katalizator chromowy, sposób jego wytwarzania, układ katalityczny zawierający ten katalizator oraz zastosowanie tego układu katalitycznego 2021
8 K. Bester; A. Bukowska; W. Bukowski; M. Pytel Polymer Beads Decorated with Dendritic Systems as Supports for A3 Coupling Catalysts 2021
9 K. Bester; A. Bukowska; W. Bukowski; M. Pytel; A. Sobota Copolymerization of Phthalic Anhydride with Epoxides Catalyzed by Amine-Bis(Phenolate) Chromium(III) Complexes 2021
10 K. Bester; A. Bukowska; W. Bukowski Homogeniczny katalizator chromowy, sposób jego wytwarzania, układ katalityczny zawierający ten katalizator oraz zatosowanie tego układu katalitycznego 2019
11 K. Bester; W. Bukowski; D. Tomczyk Kinetics of Redox Processes in the Polymer Films of Ni(II) Salen Type Complexes 2019