Methods of analysis of organic compounds
Some basic information about the module
Cycle of education: 2022/2023
The name of the faculty organization unit: The faculty Chemistry
The name of the field of study: Chemical Technology
The area of study: technical sciences
The profile of studing:
The level of study: second degree study
Type of study: past time
discipline specialities : Chemical analysis in industry and environment, Engineering of polymer materials, Organic and polymer technology , Product and ecological process engineering, Technology of medicinal products
The degree after graduating from university: Master of Science (MSc)
The name of the module department : Department of Organic Chemistry
The code of the module: 10529
The module status: mandatory for the speciality Organic and polymer technology
The position in the studies teaching programme: sem: 2 / W9 L9 / 2 ECTS / Z
The language of the lecture: Polish
The name of the coordinator: Prof. Jacek Lubczak, DSc, PhD, Eng.
The aim of studying and bibliography
The main aim of study: The students should obtain knowledge of instrumental methods of analysis of organic compounds.
The general information about the module: The module is implemented in the second semester. There are 9 hours of lectures and 9 hours laboratory. Module ends with a credit.
Bibliography required to complete the module
| 1 | Praca zbiorowa | Metody spektralne i ich zastosowanie do identyfikacji związków organicznych | WNT, Warszawa. | 1995 |
| 2 | Silverstein R. i inni | Spektroskopowe metody identyfikacji zwiazków organicznych | Wydawnictwo Naukowe PWN, Warszawa. | 2007 |
| 3 | Kazicyna L.A., Kupletska W.B. | Metody spektroskopowe wyznaczania struktury związków organicznych | PWN, Warszawa. | 1974 |
| 1 | Praca zbiorowa | Metody spektralne i ich zastosowanie do identyfikacji związków organicznych | WNT, Warszawa. | 1995 |
| 2 | Silverstein R. i inni | Spektroskopowe metody identyfikacji zwiazków organicznych | Wydawnictwo Naukowe PWN, Warszawa. | 2007 |
| 3 | Kazicyna L.A., Kupletska W.B. | Metody spektroskopowe wyznaczania struktury związków organicznych | PWN, Warszawa. | 1974 |
| 1 | Praca zbiorowa | Metody spektralne i ich zastosowanie do identyfikacji związków organicznych | WNT, Warszawa. | 1995 |
| 2 | Silverstein R. i inni | Spektroskopowe metody identyfikacji zwiazków organicznych | Wydawnictwo Naukowe PWN, Warszawa. | 2007 |
| 3 | Kazicyna L.A., Kupletska W.B. | Metody spektroskopowe wyznaczania struktury związków organicznych | PWN, Warszawa. | 1974 |
Basic requirements in category knowledge/skills/social competences
Formal requirements: Registration for semester II
Basic requirements in category knowledge: Knowledge of the nomenclature, structure, preparation methods, physical and chemical properties of the basic classes of organic compounds and basic knowlegde of the spectral techniques.
Basic requirements in category skills: Ability to name and to predict a chemical properties of organic compounds based on the structure and the effects of electron transfer, ability to work in a laboratory.
Basic requirements in category social competences: Ability to work in a team.
Module outcomes
| MEK | The student who completed the module | Types of classes / teaching methods leading to achieving a given outcome of teaching | Methods of verifying every mentioned outcome of teaching | Relationships with KEK | Relationships with PRK |
|---|---|---|---|---|---|
| 01 | has knowledge of instrumental methods determining structure of organic compounds | lecture, laboratory | colloquium, written test, written report |
K_W01++ K_W08++ |
P7S_WG |
| 02 | can propose a spectral method to identify organic compounds and identify simple organic compounds using spectral methods | lecture, laboratory | colloquium, written test, written report |
K_U14++ K_U15++ |
P7S_UW |
| 03 | can individually expand their knowledge in the analysis of the organic compounds | performance monitoring |
K_K01+ |
P7S_KK |
Attention: Depending on the epidemic situation, verification of the achieved learning outcomes specified in the study program, in particular credits and examinations at the end of specific classes, can be implemented remotely (real-time meetings).
The syllabus of the module
| Sem. | TK | The content | realized in | MEK |
|---|---|---|---|---|
| 2 | TK01 | W01 - W15, L01 - L10 | MEK01 MEK02 MEK03 |
The student's effort
| The type of classes | The work before classes | The participation in classes | The work after classes |
|---|---|---|---|
| Lecture (sem. 2) | contact hours:
9.00 hours/sem. |
Studying the recommended bibliography:
4.00 hours/sem. |
|
| Laboratory (sem. 2) | The preparation for a Laboratory:
1.00 hours/sem. The preparation for a test: 10.00 hours/sem. |
contact hours:
9.00 hours/sem. |
Finishing/Making the report:
4.00 hours/sem. |
| Advice (sem. 2) | |||
| Credit (sem. 2) | The preparation for a Credit:
10.00 hours/sem. |
The written credit:
3.00 hours/sem. |
The way of giving the component module grades and the final grade
| The type of classes | The way of giving the final grade |
|---|---|
| Lecture | The final grade depends on the basis of 2 written tests including the whole scope of material. The final test grade depends on the amount of points : 3.0 52.0%-62.0% ; 3.5 62.1%-72.0%; 4.0 72.1%-81.0%; 4.5 81.1%-90.5%; 5.0 90.6%-100%. |
| Laboratory | Each laboratory exercise must be positively included. The final grade of the exercise is an arithmetic average from written test and properly performed exercise. The final grade of the laboratory is an arithmetic average from all exercise included in the curriculum. |
| The final grade | Final grade (K): K = 0,4 w L + 0,6 w Z; where: L, Z - positive evaluation of the lab and lecture; w - factor related to the time of credit, w= 1.0 first term, w = 0.9 second term , w = 0.8 third term. The grade is rounded according to WKZJK. |
Sample problems
Required during the exam/when receiving the credit
(-)
Realized during classes/laboratories/projects
(-)
Others
(-)
Can a student use any teaching aids during the exam/when receiving the credit : yes
Available materials : spectroscopic correlation tables
The contents of the module are associated with the research profile: yes
| 1 | B. Dębska; J. Lubczak; A. Strzałka | Polyols and polyurethane foams based on chitosans of various molecular weights | 2024 |
| 2 | E. Chmiel-Bator; J. Lubczak; R. Lubczak; M. Szpiłyk | Sposób otrzymywania poliolu | 2024 |
| 3 | J. Lubczak; A. Strzałka | Sposób wytwarzania wielofunkcyjnych polioli z wykorzystaniem chitozanu | 2024 |
| 4 | J. Lubczak; A. Strzałka | Polyols and Polyurethane Foams Based on Water-Soluble Chitosan | 2023 |
| 5 | J. Lubczak; A. Strzałka | Polyurethane foams with hydroxylated chitosan units | 2023 |
| 6 | J. Lubczak; A. Strzałka | Sposób wytwarzania wielofunkcyjnych polioli | 2023 |
| 7 | J. Lubczak; A. Strzałka | Sposób wytwarzania wielofunkcyjnych polioli z wykorzystaniem chitozanu | 2023 |
| 8 | J. Lubczak; R. Lubczak | Oligoetherols and polyurethane foams based on cyclotriphosphazene of reduced fammability | 2023 |
| 9 | J. Lubczak; R. Lubczak; A. Strzałka | Chitosan Oligomer as a Raw Material for Obtaining Polyurethane Foams | 2023 |
| 10 | J. Lubczak; R. Lubczak; A. Strzałka | Polyols obtained from chitosan | 2023 |
| 11 | J. Lubczak; R. Lubczak; M. Szpiłyk | Sposób wytwarzania mieszaniny polioli | 2023 |
| 12 | J. Lubczak; R. Lubczak; M. Szpiłyk | Sposób wytwarzania wielofunkcyjnych polieteroli | 2023 |
| 13 | E. Chmiel-Bator; J. Lubczak; R. Lubczak; M. Szpiłyk | Polyols and Polyurethane Foams Obtained from Mixture of Metasilicic Acid and Cellulose | 2022 |
| 14 | J. Lubczak; M. Walczak | e-caprolactone and pentaerythritol derived oligomer for rigid polyurethane foams preparation | 2022 |
| 15 | J. Lubczak; R. Lubczak | Increased Thermal Stability and Reduced Flammability of Polyurethane Foams with an Application of Polyetherols | 2022 |
| 16 | D. Broda; B. Dębska; M. Kus-Liśkiewicz; J. Lubczak; R. Lubczak; D. Szczęch; R. Wojnarowska-Nowak | Polyetherols and polyurethane foams from starch | 2021 |
| 17 | E. Bobko; D. Broda; B. Dębska; M. Kus-Liśkiewicz; J. Lubczak; R. Lubczak; D. Szczęch; M. Szpiłyk | Flame retardant polyurethane foams with starch unit | 2021 |
| 18 | J. Lubczak; R. Lubczak; D. Szczęch | Sposób otrzymywania mieszaniny wielofunkcyjnych polieteroli | 2021 |
| 19 | J. Lubczak; R. Lubczak; M. Szpiłyk | Polyetherols and polyurethane foams with cellulose subunits | 2021 |
| 20 | J. Lubczak; R. Lubczak; M. Szpiłyk | Sposób wytwarzania wielofunkcyjnych polieteroli | 2021 |
| 21 | J. Lubczak; R. Lubczak; M. Szpiłyk | The biodegradable cellulose-derived polyol and polyurethane foam | 2021 |
| 22 | J. Lubczak; R. Lubczak; M. Szpiłyk; M. Walczak | Polyol and polyurethane foam from cellulose hydrolysate | 2021 |
| 23 | M. Borowicz; E. Chmiel; J. Lubczak; J. Paciorek-Sadowska | Use of a Mixture of Polyols Based on Metasilicic Acid and Recycled PLA for Synthesis of Rigid Polyurethane Foams Susceptible to Biodegradation | 2021 |
| 24 | E. Chmiel; J. Lubczak | Polyurethane foams with 1,3,5-triazine ring, boron and silicon | 2020 |
| 25 | J. Lubczak; M. Szpiłyk | Sposób wytwarzania oligoeterolu z pierścieniem azafosfacyklicznym | 2020 |
| 26 | J. Lubczak; R. Lubczak; D. Szczęch | From starch to oligoetherols and polyurethane foams | 2020 |
| 27 | B. Dębska; J. Duliban; K. Hęclik; J. Lubczak | Analysis of the Possibility and Conditions of Application of Methylene Blue to Determine the Activity of Radicals in Model System with Preaccelerated Cross-Linking of Polyester Resins | 2019 |
| 28 | E. Chmiel; J. Lubczak | Polyurethane foams with 1,3,5-triazine ring and silicon atoms | 2019 |
| 29 | E. Chmiel; J. Lubczak | Sposób otrzymywania termoodpornych i niepalnych pianek poliuretanowych | 2019 |
| 30 | E. Chmiel; J. Lubczak | Synthesis of oligoetherols from mixtures of melamine and boric acid and polyurethane foams formed from these oligoetherols | 2019 |
| 31 | E. Chmiel; J. Lubczak; R. Oliwa | Boron-containing non-flammable polyurethane foams | 2019 |
| 32 | J. Lubczak; R. Lubczak; D. Szczęch | Sposób otrzymywania mieszaniny wielofunkcyjnych polieteroli | 2019 |
| 33 | J. Lubczak; R. Lubczak; I. Zarzyka | Sposób otrzymywania polieteroli z pierścieniami azacyklicznymi | 2019 |
| 34 | M. Borowicz; B. Czupryński; J. Lubczak; J. Paciorek-Sadowska | Biodegradable, Flame-retardant, and Bio-Based rigid Polyurethane/Polyisocyanurate Foams for Thermal Insulation Application | 2019 |