Item card
Methods of analysis of organic compounds
Some basic information about the module
Cycle of education:
2022/2023
The name of the faculty organization unit:
The faculty Chemistry
The name of the field of study:
Chemical Technology
The area of study:
technical sciences
The profile of studing:
The level of study:
second degree study
Type of study:
past time
discipline specialities :
Chemical analysis in industry and environment, Engineering of polymer materials, Organic and polymer technology , Product and ecological process engineering, Technology of medicinal products
The degree after graduating from university:
Master of Science (MSc)
The name of the module department :
Department of Organic Chemistry
The code of the module:
10504
The module status:
mandatory for the speciality Chemical analysis in industry and environment
The position in the studies teaching programme:
sem: 2 / W18 L27 / 5 ECTS / E
The language of the lecture:
Polish
The name of the coordinator:
Elżbieta Chmiel-Szukiewicz, PhD, Eng.
The aim of studying and bibliography
The main aim of study:
The students should obtain knowledge of chemical and instrumental methods of analysis of organic compounds.
The general information about the module:
The module is implemented in the second semester. There are 18 hours of lectures and 27 hours laboratory. Module ends with an exam.
Bibliography required to complete the module
| 1 | Vogel A. I. i inni | Preparatyka organiczna | WNT, Warszawa. | 1984 |
| 2 | Chmiel-Szukiewicz E., Kijowska D., Zarzyka-Niemiec I. | Laboratorium chemii organicznej. Metody syntezy i analizy jakościowej związków organicznych | Wydawnictwo Oświatowe FOSZE, Rzeszów. | 2010 |
| 3 | Jerzmanowska Z. | Analiza jakościowa związków organicznych | PZWL, Warszawa. | 1975 |
| 4 | Wolinski J., Terpiński J. | Organiczna analiza jakościowa | PWN, Warszawa. | 1973 |
| 5 | Praca zbiorowa | Metody spektroskopowe i ich zastosowanie do identyfikacji związków organicznych | WNT, Warszawa. | 1995 |
| 6 | Silverstein R. i inni | Spektroskopowe metody identyfikacji zwiazków organicznych | Wydawnictwo Naukowe PWN, Warszawa. | 2007 |
| 7 | Kazicyna L.A., Kupletska W.B. | Metody spektroskopowe wyznaczania struktury związków organicznych | PWN, Warszawa. | 1974 |
| 1 | Vogel A. I. i inni | Preparatyka organiczna | WNT, Warszawa. | 1984 |
| 2 | Chmiel-Szukiewicz E., Kijowska D., Zarzyka-Niemiec I. | Laboratorium chemii organicznej. Metody syntezy i analizy jakościowej związków organicznych | Wydawnictwo Oświatowe FOSZE, Rzeszów. | 2010 |
| 3 | Jerzmanowska Z. | Analiza jakościowa związków organicznych | PZWL, Warszawa. | 1975 |
| 4 | Wolinski J., Terpiński J. | Organiczna analiza jakościowa | PWN, Warszawa. | 1973 |
| 5 | Praca zbiorowa | Metody spektroskopowe i ich zastosowanie do identyfikacji związków organicznych | WNT, Warszawa. | 1995 |
| 6 | Silverstein R. i inni | Spektroskopowe metody identyfikacji zwiazków organicznych | Wydawnictwo Naukowe PWN, Warszawa. | 2007 |
| 7 | Kazicyna L.A., Kupletska W.B. | Metody spektroskopowe wyznaczania struktury związków organicznych | PWN, Warszawa. | 1974 |
| 1 | Vogel A. I. i inni | Preparatyka organiczna | WNT, Warszawa. | 1984 |
| 2 | Jerzmanowska Z. | Analiza jakościowa związków organicznych | PZWL, Warszawa. | 1975 |
| 3 | Wolinski J., Terpiński J. | Organiczna analiza jakościowa | PWN, Warszawa. | 1973 |
| 4 | Praca zbiorowa | Metody spektroskopowe i ich zastosowanie do identyfikacji związków organicznych | WNT, Warszawa. | 1995 |
| 5 | Silverstein R. i inni | Spektroskopowe metody identyfikacji zwiazków organicznych | Wydawnictwo Naukowe PWN, Warszawa. | 2010 |
| 6 | Kazicyna L.A., Kupletska W.B. | Metody spektroskopowe wyznaczania struktury związków organicznych | PWN, Warszawa. | 1974 |
Basic requirements in category knowledge/skills/social competences
Formal requirements:
Registration for semester II
Basic requirements in category knowledge:
Knowledge of the nomenclature, structure, preparation methods, physical and chemical properties of the basic classes of organic compounds and basic knowlegde of the spectral techniques.
Basic requirements in category skills:
Ability to name and to predict a chemical properties of organic compounds based on the structure and the effects of electron transfer, ability to work in a laboratory.
Basic requirements in category social competences:
Ability to work in a team in the synthesis, isolation of simple organic compounds.
Module outcomes
| MEK | The student who completed the module | Types of classes / teaching methods leading to achieving a given outcome of teaching | Methods of verifying every mentioned outcome of teaching | Relationships with KEK | Relationships with PRK |
|---|---|---|---|---|---|
| MEK01 | has a basic knowledge of the purity tests, of the techniques of separation and purification of organic compounds | lecture | written exam |
K-W01++ |
P7S-WG |
| MEK02 | has knowledge of chemical methods determining qualitative and quantitative composition of organic compounds | lecture, laboratory | written exam, written test, written report |
K-W01++ K-W08++ |
P7S-WG |
| MEK03 | has knowledge of instrumental methods determining structure of organic compounds | lecture, laboratory | written exam, written test, written report |
K-W01++ K-W08++ |
P7S-WG |
| MEK04 | can propose chemical methods to identification of organic compounds and can identify a simple organic compounds using chemical methods | lecture, laboratory | written exam, written test, performance monitoring, written report |
K-U14++ K-U15+ |
P7S-UW |
| MEK05 | can propose a spectral method to identify organic compounds and identify simple organic compounds using spectral methods | lecture, laboratory | written exam, written test, performance monitoring, written report |
K-U14++ K-U15++ |
P7S-UW |
| MEK06 | can individually expand their knowledge in the analysis of the organic compounds | lecture | written exam |
K-K01+ |
P7S-KK |
The syllabus of the module
| Sem. | TK | The content | realized in | MEK |
|---|---|---|---|---|
| 2 | TK01 | W01, W02 | MEK01 MEK06 | |
| 2 | TK02 | W03 - W06, L01 - L08 | MEK02 MEK04 MEK06 | |
| 2 | TK03 | W07 - W15, L09 - L15 | MEK03 MEK05 MEK06 |
The student's effort
| The type of classes | The work before classes | The participation in classes | The work after classes |
|---|---|---|---|
| Lecture (sem. 2) | contact hours:
18.00 hours/sem. |
Studying the recommended bibliography:
10.00 hours/sem. |
|
| Laboratory (sem. 2) | The preparation for a Laboratory:
5.00 hours/sem. The preparation for a test: 20.00 hours/sem. |
contact hours:
27.00 hours/sem. |
Finishing/Making the report:
15.00 hours/sem. |
| Advice (sem. 2) | |||
| Exam (sem. 2) | The preparation for an Exam:
28.00 hours/sem. |
The written exam:
2.00 hours/sem. |
The way of giving the component module grades and the final grade
| The type of classes | The way of giving the final grade |
|---|---|
| Lecture | Written exam including the whole scope of material. The final exam grade depends on the amount of points : 3.0 52.0%-62.0% ; 3.5 62.1%-72.0%; 4.0 72.1%-81.0%; 4.5 81.1%-90.5%; 5.0 90.6%-100%. |
| Laboratory | Each laboratory exercise must be positively included. The final grade of the exercise is a weighted average; the weight of a written test is twice greater than a weight of a grade for experiment and report. The final grade of the laboratory is an arithmetic average from all exercise included in the curriculum. |
| The final grade | Final grade (K): K = 0,4 w L + 0,6 w E; where: L, E - positive evaluation of the lab and exam; w - factor related to the time of credit, w= 1.0 first term, w = 0.9 second term , w = 0.8 third term. The grade is rounded according to WKZJK. |
Sample problems
Required during the exam/when receiving the credit
(-)
Realized during classes/laboratories/projects
(-)
Others
(-)
Can a student use any teaching aids during the exam/when receiving the credit : yes
Available materials : spectroscopic correlation tables
The contents of the module are associated with the research profile yes
| 1 | E. Chmiel-Szukiewicz; M. Szpiłyk; Ł. Uram; M. Zaręba | Sposób otrzymywania materiału porowatego oraz zastosowanie tego materiału porowatego | 2025 |
| 2 | E. Chmiel-Szukiewicz; M. Szukiewicz | Carbon dioxide methanation in PtG technology | 2025 |
| 3 | E. Chmiel-Szukiewicz; N. Patulska; M. Szukiewicz | A Fast and Efficient Response Surface Approach for the Optimization of the Gas-Phase Hydrogenation of Carbon Dioxide on Nickel-Based Catalysts | 2025 |
| 4 | E. Chmiel-Szukiewicz; A. Szałek; M. Szukiewicz | Graph Theory in Chemical Kinetics Practice Problems | 2024 |
| 5 | E. Chmiel-Szukiewicz; J. Noga; M. Rzepna; Ł. Uram; S. Wołowiec; M. Zaręba | A Novel PAMAM G3 Dendrimer-Based Foam with Polyether Polyol and Castor Oil Components as Drug Delivery System into Cancer and Normal Cells | 2024 |
| 6 | E. Chmiel-Szukiewicz; M. Szukiewicz | Generalized Linear Driving Force Formulas for Diffusion and Reaction in Porous Catalysts | 2024 |
| 7 | E. Chmiel-Szukiewicz; M. Szukiewicz; L. Zaręba | Application of the kinetic polynomial idea to describecatalytic hydrogenation of propene | 2024 |
| 8 | E. Chmiel-Szukiewicz; P. Cieciński; M. Drajewicz; J. Pieniążek; T. Rogalski; R. Smusz; M. Szukiewicz | Fire Test of an Equipment for Hydrogen Powered Aircraft | 2024 |
| 9 | E. Chmiel-Szukiewicz | Hardly Flammable Polyurethane Foams with 1,3-Pyrimidine Ring and Boron Atoms | 2021 |
| 10 | E. Chmiel-Szukiewicz; A. Szałek; M. Szukiewicz | Kinetic investigations of heterogeneous reactor processes – Optimization of experiments | 2021 |