The aim of studying and bibliography

The main aim of study: The students should obtain knowledge of chemical and instrumental methods of analysis of organic compounds.

The general information about the module: The module is implemented in the second semester. There are 18 hours of lectures and 27 hours laboratory. Module ends with an exam.

Bibliography required to complete the module

Bibliography used during lectures

1	Vogel A. I. i inni	Preparatyka organiczna	WNT, Warszawa.	1984
2	Chmiel-Szukiewicz E., Kijowska D., Zarzyka-Niemiec I.	Laboratorium chemii organicznej. Metody syntezy i analizy jakościowej związków organicznych	Wydawnictwo Oświatowe FOSZE, Rzeszów.	2010
3	Jerzmanowska Z.	Analiza jakościowa związków organicznych	PZWL, Warszawa.	1975
4	Wolinski J., Terpiński J.	Organiczna analiza jakościowa	PWN, Warszawa.	1973
5	Praca zbiorowa	Metody spektroskopowe i ich zastosowanie do identyfikacji związków organicznych	WNT, Warszawa.	1995
6	Silverstein R. i inni	Spektroskopowe metody identyfikacji zwiazków organicznych	Wydawnictwo Naukowe PWN, Warszawa.	2007
7	Kazicyna L.A., Kupletska W.B.	Metody spektroskopowe wyznaczania struktury związków organicznych	PWN, Warszawa.	1974

Bibliography used during classes/laboratories/others

1	Vogel A. I. i inni	Preparatyka organiczna	WNT, Warszawa.	1984
2	Chmiel-Szukiewicz E., Kijowska D., Zarzyka-Niemiec I.	Laboratorium chemii organicznej. Metody syntezy i analizy jakościowej związków organicznych	Wydawnictwo Oświatowe FOSZE, Rzeszów.	2010
3	Jerzmanowska Z.	Analiza jakościowa związków organicznych	PZWL, Warszawa.	1975
4	Wolinski J., Terpiński J.	Organiczna analiza jakościowa	PWN, Warszawa.	1973
5	Praca zbiorowa	Metody spektroskopowe i ich zastosowanie do identyfikacji związków organicznych	WNT, Warszawa.	1995
6	Silverstein R. i inni	Spektroskopowe metody identyfikacji zwiazków organicznych	Wydawnictwo Naukowe PWN, Warszawa.	2007
7	Kazicyna L.A., Kupletska W.B.	Metody spektroskopowe wyznaczania struktury związków organicznych	PWN, Warszawa.	1974

Bibliography to self-study

1	Vogel A. I. i inni	Preparatyka organiczna	WNT, Warszawa.	1984
2	Jerzmanowska Z.	Analiza jakościowa związków organicznych	PZWL, Warszawa.	1975
3	Wolinski J., Terpiński J.	Organiczna analiza jakościowa	PWN, Warszawa.	1973
4	Praca zbiorowa	Metody spektroskopowe i ich zastosowanie do identyfikacji związków organicznych	WNT, Warszawa.	1995
5	Silverstein R. i inni	Spektroskopowe metody identyfikacji zwiazków organicznych	Wydawnictwo Naukowe PWN, Warszawa.	2010
6	Kazicyna L.A., Kupletska W.B.	Metody spektroskopowe wyznaczania struktury związków organicznych	PWN, Warszawa.	1974

Basic requirements in category knowledge/skills/social competences

Formal requirements: Registration for semester II

Basic requirements in category knowledge: Knowledge of the nomenclature, structure, preparation methods, physical and chemical properties of the basic classes of organic compounds and basic knowlegde of the spectral techniques.

Basic requirements in category skills: Ability to name and to predict a chemical properties of organic compounds based on the structure and the effects of electron transfer, ability to work in a laboratory.

Basic requirements in category social competences: Ability to work in a team in the synthesis, isolation of simple organic compounds.

Module outcomes

MEK	The student who completed the module	Types of classes / teaching methods leading to achieving a given outcome of teaching	Methods of verifying every mentioned outcome of teaching	Relationships with KEK	Relationships with PRK
01	has a basic knowledge of the purity tests, of the techniques of separation and purification of organic compounds	lecture	written exam	K_W01++	P7S_WG
02	has knowledge of chemical methods determining qualitative and quantitative composition of organic compounds	lecture, laboratory	written exam, written test, written report	K_W01++ K_W08++	P7S_WG
03	has knowledge of instrumental methods determining structure of organic compounds	lecture, laboratory	written exam, written test, written report	K_W01++ K_W08++	P7S_WG
04	can propose chemical methods to identification of organic compounds and can identify a simple organic compounds using chemical methods	lecture, laboratory	written exam, written test, performance monitoring, written report	K_U14++ K_U15+	P7S_UW
05	can propose a spectral method to identify organic compounds and identify simple organic compounds using spectral methods	lecture, laboratory	written exam, written test, performance monitoring, written report	K_U14++ K_U15++	P7S_UW
06	can individually expand their knowledge in the analysis of the organic compounds	lecture	written exam	K_K01+	P7S_KK

Attention: Depending on the epidemic situation, verification of the achieved learning outcomes specified in the study program, in particular credits and examinations at the end of specific classes, can be implemented remotely (real-time meetings).

The syllabus of the module

Sem.	TK	The content	realized in	MEK
2	TK01	The types of methods of analysis of organic compounds. Methods separation and purification of organic compounds: crystallization, sublimation, extraction, distillation and chromatography. Determination of physical properties of the compounds.	W01, W02	MEK01 MEK06
2	TK02	Qualitative and quantitative methods for determining the composition of the compounds. Chemical methods: elemental analysis, detection and determination of the elements in the organic compounds, group reactions. Analysis of mixtures of organic compounds.	W03 - W06, L01 - L08	MEK02 MEK04 MEK06
2	TK03	Instrumental methods: elemental analysis, mass spectrometry, spectral methods: UV-VIS, IR, NMR and EPR. Study of the composition of mixtures of tautomers. Analysis of the steric structure of enantiomers and diastereomers.	W07 - W15, L09 - L15	MEK03 MEK05 MEK06

The student's effort

The type of classes	The work before classes	The participation in classes	The work after classes
Lecture (sem. 2)		contact hours: 18.00 hours/sem.	Studying the recommended bibliography: 10.00 hours/sem.
Laboratory (sem. 2)	The preparation for a Laboratory: 5.00 hours/sem. The preparation for a test: 20.00 hours/sem.	contact hours: 27.00 hours/sem.	Finishing/Making the report: 15.00 hours/sem.
Advice (sem. 2)
Exam (sem. 2)	The preparation for an Exam: 28.00 hours/sem.	The written exam: 2.00 hours/sem.

The way of giving the component module grades and the final grade

The type of classes	The way of giving the final grade
Lecture	Written exam including the whole scope of material. The final exam grade depends on the amount of points : 3.0 52.0%-62.0% ; 3.5 62.1%-72.0%; 4.0 72.1%-81.0%; 4.5 81.1%-90.5%; 5.0 90.6%-100%.
Laboratory	Each laboratory exercise must be positively included. The final grade of the exercise is a weighted average; the weight of a written test is twice greater than a weight of a grade for experiment and report. The final grade of the laboratory is an arithmetic average from all exercise included in the curriculum.
The final grade	Final grade (K): K = 0,4 w L + 0,6 w E; where: L, E - positive evaluation of the lab and exam; w - factor related to the time of credit, w= 1.0 first term, w = 0.9 second term , w = 0.8 third term. The grade is rounded according to WKZJK.

Sample problems

Required during the exam/when receiving the credit
(-)

Realized during classes/laboratories/projects
(-)

Others
(-)

Can a student use any teaching aids during the exam/when receiving the credit : yes

Available materials : spectroscopic correlation tables

The contents of the module are associated with the research profile: yes

1	E. Chmiel-Szukiewicz; A. Szałek; M. Szukiewicz	Graph Theory in Chemical Kinetics Practice Problems	2024
2	E. Chmiel-Szukiewicz; M. Szukiewicz	Generalized Linear Driving Force Formulas for Diffusion and Reaction in Porous Catalysts	2024
3	E. Chmiel-Szukiewicz; M. Szukiewicz; L. Zaręba	Application of the kinetic polynomial idea to describecatalytic hydrogenation of propene	2024
4	E. Chmiel-Szukiewicz	Hardly Flammable Polyurethane Foams with 1,3-Pyrimidine Ring and Boron Atoms	2021
5	E. Chmiel-Szukiewicz; A. Szałek; M. Szukiewicz	Kinetic investigations of heterogeneous reactor processes – Optimization of experiments	2021
6	E. Chmiel-Szukiewicz	Improved thermally stable oligoetherols from 6-aminouracil, ethylene carbonate and boric acid	2019
7	E. Chmiel-Szukiewicz; K. Kaczmarski; A. Szałek; M. Szukiewicz	Dead zone for hydrogenation of propylene reaction carried out on commercial catalyst pellets	2019