The aim of studying and bibliography

The main aim of study: The student should obtain knowledge about theoretical and practical skills for analysis of traces in industrial and environmental materials and use the analytical data.

The general information about the module: Module implemented as a lecture (30 hours) and laboratory (45 hours) in the second semester. The module ends with an exam.

Bibliography required to complete the module

Basic requirements in category knowledge/skills/social competences

Formal requirements: Registration for the semester

Basic requirements in category knowledge: Knowledge of analytical chemistry and instrumental analysis at the basic level.

Basic requirements in category skills: Ability to perform an experiment at the basic level

Basic requirements in category social competences: The ability to cooperate and work in a group

Module outcomes

MEK	The student who completed the module	Types of classes / teaching methods leading to achieving a given outcome of teaching	Methods of verifying every mentioned outcome of teaching	Relationships with KEK	Relationships with PRK
01	It has an extended knowledge of trace analytes, methods of their detection and analysis, special techniques and evaluation of the analytical result.	lecture	written exam	K_W01+++ K_U15+++	P7S_UW P7S_WG
02	Has the ability to prepare and perform trace analysis, calculation and evaluation of the impurity content in samples.	Laboratory	written test	K_K01+++ K_K02++	P7S_KK P7S_KO

Attention: Depending on the epidemic situation, verification of the achieved learning outcomes specified in the study program, in particular credits and examinations at the end of specific classes, can be implemented remotely (real-time meetings).

The syllabus of the module

Sem.	TK	The content	realized in	MEK
2	TK01	Fundamental problems of trace analysis. Techniques and analytical methods in trace analysis. Separation and concentration of traces. Derivatization. Sources of errors. Quality assurance and control quality of results. Trace analysis of products and waste industrials, water and sewage, soils and plants, atmospheric air, pharmaceutical and food products. Speciation analysis.	W18	MEK01
2	TK02	1. Analysis of the selected elements in water. 2. Analysis of oxalate in the foodstuffs 3. Analysis of mefenamic acid in pharmaceuticals and its different forms in aqueous solution. 4. Analysis of heavy metals and trace elements in soil. 5. Analysis of formaldehyde in package materials. 6. Analysis of chromium(VI) in soil eluates. 7. Analysis of the chemical fraction of manganese in industrial ash. 8. Analysis of the content of nitrate(III) and nitrate(V) in food products. 9. Speciation analysis of iron in mineral water.	L27	MEK02

The student's effort

The type of classes	The work before classes	The participation in classes	The work after classes
Lecture (sem. 2)		contact hours: 18.00 hours/sem.	complementing/reading through notes: 5.00 hours/sem. Studying the recommended bibliography: 25.00 hours/sem.
Laboratory (sem. 2)	The preparation for a Laboratory: 5.00 hours/sem. The preparation for a test: 15.00 hours/sem.	contact hours: 27.00 hours/sem.	Finishing/Making the report: 10.00 hours/sem.
Advice (sem. 2)	The preparation for Advice: 5.00 hours/sem.	The participation in Advice: 5.00 hours/sem.
Exam (sem. 2)	The preparation for an Exam: 20.00 hours/sem.	The written exam: 2.00 hours/sem.

The way of giving the component module grades and the final grade

The type of classes	The way of giving the final grade
Lecture	Lecture – written examination - OW.
Laboratory	Laboratory – written test, each classes - OL.
The final grade	The final note (OK) is calculated according to the formula: OK = 50%OW+ 50%OL

Sample problems

Required during the exam/when receiving the credit
(-)

Realized during classes/laboratories/projects
(-)

Others
(-)

Can a student use any teaching aids during the exam/when receiving the credit : no

The contents of the module are associated with the research profile: yes

1	J. Kalembkiewicz; A. Kuźniar; B. Papciak; E. Sočo	Zastosowanie materiału krzemionkowego modyfikowanego surfaktantem do immobilizacji moryny	2023
2	J. Kalembkiewicz; M. Kopacz; J. Pusz	Współczesne metody badań i zastosowań flawonoidów: praca zbiorowa	2023
3	D. Galas; J. Kalembkiewicz; E. Sitarz-Palczak	Study of the Adsorption of Cu(II), Mn(II), Pb(II), and Zn(II) Ions on Geopolymers Obtained from Ashes from Biomass Combustion	2022
4	J. Kalembkiewicz; E. Pieniążek; J. Pusz; E. Sitarz-Palczak; E. Sočo	Badania właściwości kwercetyny i jej sulfonowych pochodnych w układach z fluoroforem	2022
5	J. Kalembkiewicz; M. Kopacz; J. Pusz	Flawonoidy i ich pochodne w badaniach naukowych i praktyce	2022
6	M. Dranka; J. Kalembkiewicz; D. Kamiński; A. Kozioł; A. Kuźniar; U. Maciołek; L. Mazur; E. Mendyk	Structural and spectroscopic studies of Na+ – Quercetin-5′-sulfonic acid polymeric complexes obtained via solvothermal synthesis	2022
7	J. Kalembkiewicz; B. Papciak; E. Pieniążek; E. Sočo	Stałe związki kompleksowe jonów tytanu(IV) z sulfonową pochodną moryny	2021
8	J. Kalembkiewicz; E. Pieniążek; E. Sočo	Adsorpcja flawonoidów na uporządkowanych mezoporowych materiałach krzemionkowych	2021
9	J. Kalembkiewicz; E. Sitarz-Palczak	Application of halloysite geopolymers to removal of methyl blue from aqueous solution	2021
10	J. Kalembkiewicz; E. Sitarz-Palczak	The Influence of Physical Modification on the Sorption Properties of Geopolymers Obtained from Halloysite	2021
11	J. Kalembkiewicz; M. Kopacz; J. Pusz	Badania naukowe i aplikacyjne flawonoidów	2021
12	J. Kalembkiewicz; M. Kopacz; J. Pusz	Nauka i praktyka w świecie flawonoidów	2021
13	J. Kalembkiewicz; M. Kosińska-Pezda; J. Pusz; E. Woźnicka; L. Zapała	Badania równowagi reakcji kompleksowania chryzyny z jonami Er(III) w układach: woda - metanol i woda - metanol - 1,4-dioksan	2021
14	J. Kalembkiewicz	Surowce i produkty nieorganiczne	2020
15	J. Kalembkiewicz	Uzupełnienia	2020
16	J. Kalembkiewicz; A. Kuźniar; B. Papciak; J. Pusz; E. Sitarz-Palczak; E. Sočo; E. Woźnicka	Pierwiastki i związki chemiczne	2020
17	J. Kalembkiewicz; A. Kuźniar; E. Pieniążek; E. Sočo; E. Woźnicka	Aktywność biochemiczna sulfonowych pochodnych moryny	2020
18	J. Kalembkiewicz; B. Papciak	Chemia ogólna i nieorganiczna. Pierwiastki i związki chemiczne. Surowce i produkty nieorganiczne: obliczenia chemiczne i problemy	2020
19	J. Kalembkiewicz; B. Papciak	Chemia ogólna i nieorganiczna. Podstawy chemii. Roztwory i procesy w roztworach: obliczenia chemiczne i problemy	2020
20	J. Kalembkiewicz; B. Papciak	Uzupełnienia	2020
21	J. Kalembkiewicz; B. Papciak; E. Pieniążek; J. Pusz; P. Skitał; E. Sočo; L. Zapała	Podstawy chemii	2020
22	J. Kalembkiewicz; B. Papciak; J. Pusz; E. Sitarz-Palczak; E. Woźnicka	Roztwory i procesy w roztworach	2020
23	J. Kalembkiewicz; D. Pająk; E. Sočo	Multi-component sorption and utilization of solid waste to simultaneous removing basic dye and heavy metal from aqueous system	2020
24	J. Kalembkiewicz; E. Sočo	Characterisation and utilisation of solid waste from coal combustion to modelling of sorption equilibrium in a bi-component system metal-dye	2020
25	J. Kalembkiewicz; E. Sočo	Immobilizing and Removal of Cadmium and Rhodamine B from an Aqueous System by Converting Solid Waste from Poland; Studies of Equilibrium and Kinetic Sorption	2020
26	J. Kalembkiewicz; M. Kopacz; J. Pusz	Świat flawonoidów w badaniach naukowych	2020
27	J. Kalembkiewicz; R. Rawski; P. Sanecki	Units and Methods of Proteolytic Activity Determination	2020
28	D. Galas; J. Kalembkiewicz; E. Sitarz-Palczak	Comparative study on the characteristics of coal fly ash and biomass ash geopolymers	2019
29	D. Galas; J. Kalembkiewicz; E. Sitarz-Palczak	Study of potential availability of heavy metals to phytoremediation to use of ash from biomass combustion	2019
30	J. Kalembkiewicz; D. Saletnik; P. Sanecki; P. Skitał	Electrodeposition of nickel from alkaline NH4OH/NH4Cl buffer solutions	2019
31	J. Kalembkiewicz; E. Sočo	Enhanced sorption capacity of a metal-dye system from water effluents by using activated industrial waste	2019